Publications

Results 5401–5600 of 96,771

Search results

Jump to search filters

Model Evaluation Protocol for Fire Models Involving Fuels at Liquefied Natural Gas Facilities

Luketa, Anay L.

This document provides a description of the model evaluation protocol (MEP) for pool fires, jet fires, and fireballs involving liquefied natural gas (LNG), refrigerant fluids, and byproducts at LNG facilities. The purpose of the MEP is to provide procedures regarding the assessment of a model's suitability to predict heat flux from fires. Three components, namely, a scientific assessment, model verification, and model validation comprise the MEP. The evaluation of a model satisfying these three components is to be documented in the form of a model evaluation report (MER). Discussion of models for the prediction of fire, detailed information on each of the three MEP components, the MEP procedure regarding new versions of previously approved models, and the format of the model evaluation report (MER) are provided.

More Details
TYPE SAND Report YEAR 2022
DOIOSTI

Graph theory and nighttime imagery based microgrid design

Journal of Renewable and Sustainable Energy

Lugo-Alvarez, Melvin; Kleissl, Jan; Khurram, Adil; Lave, Matthew S.; Jones, Christian B.

Reducing the duration and frequency of blackouts in remote communities poses an engineering challenge for grid operators. Outage effects can also be mitigated locally through microgrids. This paper develops a systematic procedure to account for these challenges by creating microgrids prioritizing high value assets within vulnerable communities. Nighttime satellite imagery is used to identify vulnerable communities. Using an asset classification and rating system, multi-Asset clusters within these communities are prioritized. Infrastructure data, geographic information systems, satellite imagery, and spectral clustering are used to form and rank microgrid candidates. A microgrid sizing algorithm is included to guide through the microgrid design process. An application of the methodology is presented using real event, location, and asset data.

More Details
TYPE Journal Article YEAR 2022
DOIOSTIScopus

A Tanks-in-Series Approach to Estimate Parameters for Lithium-Ion Battery Models

Journal of the Electrochemical Society

Kolluri, Suryanarayana; Mittal, Prateek; Subramaniam, Akshay; Preger, Yuliya P.; De Angelis, Valerio D.; Ramadesigan, Venkatasailanathan; Subramanian, Venkat R.

Advanced Battery Management Systems (BMS) play a vital role in monitoring, predicting, and controlling the performance of lithium-ion batteries. BMS employing sophisticated electrochemical models can help increase battery cycle life and minimize charging time. However, in order to realize the full potential of electrochemical model-based BMS, it is critical to ensure accurate predictions and proper model parameterization. The accuracy of the predictions of an electrochemical model is dependent on the accuracy of its parameters, the values of which might change with battery cycling and aging. Parameter estimation for an electrochemical model is generally challenging due to the nonlinear nature and computational complexity of the model equations. To this end, this work utilizes the recently proposed Tanks-in-Series model for Li-ion batteries (J.Electrochem. Soc., 167, 013534 (2020)) to perform parameter estimation. The Tanks-in-Series approach allows for substantially faster parameter estimation compared to the original pseudo two-dimensional (p2D) model. The objective of this work is thus to demonstrate the gain in computational efficiency from the Tanks-in-Series approach. A sensitivity analysis of model parameters is also performed to benchmark the fidelity of the Tanks-in-Series model.

More Details
TYPE Journal Article YEAR 2022
DOIOSTIScopus

A Step Toward Working with Untrusted Ground Stations

Toomey, John T.; Crosby, Sean M.

We are witnessing a shift toward outsourcing satellite and ground station services to third-party commercial entities. As with any enterprise, these third parties can be vulnerable to cyber compromise, including image tampering and deepfake injection. The multimedia community is beginning to establish standards and technology to enable authenticity verification of multimedia created and edited by others. While appealing to the remote sensing domain, the nature of raw satellite imagery is incompatible with the proposed change verification tools, resulting in the need for a means to validate updates made to image products. We present a simple method for verifying a specific class of algorithms. Our inverse processing approach eliminates the need to see the original image as the reversed data can be checked against an original digital signature. We demonstrate our approach on basic image restoration routines and conclude with a discussion on open challenges and next steps.

More Details
TYPE Other Report YEAR 2022
DOIOSTI

Federated Learning and Differential Privacy: What might AI-Enhanced co-design of microelectronics learn?

Eugenio, Evercita

Data is a valuable commodity, and it is often dispersed over multiple entities. Sharing data or models created from the data is not simple due to concerns regarding security, privacy, ownership, and model inversion. This limitation in sharing can hinder model training and development. Federated learning can enable data or model sharing across multiple entities that control local data without having to share or exchange the data themselves. Differential privacy is a conceptual framework that brings strong mathematical guarantee for privacy protection and helps provide a quantifiable privacy guarantee to any data or models shared. The concepts of federated learning and differential privacy are introduced along with possible connections. Lastly, some open discussion topics on how federated learning and differential privacy can tied to AI-Enhanced co-design of microelectronics are highlighted.

More Details
TYPE Other Report YEAR 2022
DOIOSTI

Front-End Design for SiPM-Based Monolithic Neutron Double Scatter Imagers

Sensors

Cates, Joshua W.; Steele, John T.; Balajthy, Jon A.; Negut, Victor; Hausladen, Paul; Ziock, Klaus; Brubaker, Erik B.

Neutron double scatter imaging exploits the kinematics of neutron elastic scattering to enable emission imaging of neutron sources. Due to the relatively low coincidence detection efficiency of fast neutrons in organic scintillator arrays, imaging efficiency for double scatter cameras can also be low. One method to realize significant gains in neutron coincidence detection efficiency is to develop neutron double scatter detectors which employ monolithic blocks of organic scintillator, instrumented with photosensor arrays on multiple faces to enable 3D position and multi-interaction time pickoff. Silicon photomultipliers (SiPMs) have several advantageous characteristics for this approach, including high photon detection efficiency (PDE), good single photon time resolution (SPTR), high gain that translates to single photon counting capabilities, and ability to be tiled into large arrays with high packing fraction and photosensitive area fill factor. However, they also have a tradeoff in high uncorrelated and correlated noise rates (dark counts from thermionic emissions and optical photon crosstalk generated during avalanche) which may complicate event positioning algorithms. We have evaluated the noise characteristics and SPTR of Hamamatsu S13360-6075 SiPMs with low noise, fast electronic readout for integration into a monolithic neutron scatter camera prototype. The sensors and electronic readout were implemented in a small-scale prototype detector in order to estimate expected noise performance for a monolithic neutron scatter camera and perform proof-of-concept measurements for scintillation photon counting and three-dimensional event positioning.

More Details
TYPE Journal Article YEAR 2022
DOIOSTIScopus

Phase transitions in high-purity zirconium under dynamic compression

Physical Review B

Greeff, C.W.; Brown, Justin L.; Velisavljevic, N.; Rigg, P.A.

We present results from ramp compression experiments on high-purity Zr that show the α→ω, ω→β, as well as reverse β→ω phase transitions. Simulations with a multiphase equation of state and phenomenological kinetic model match the experimental wave profiles well. While the dynamic α→ω transition occurs ∼9GPa above the equilibrium phase boundary, the ω→β transition occurs within 0.9 GPa of equilibrium. We estimate that the dynamic compression path intersects the equilibrium ω-β line at P=29.2GPa, and T=490K. The thermodynamic path in the interior of the sample lies ∼100K above the isentrope at the point of the ω→β transition. Approximately half of this dissipative temperature rise is due to plastic work, and half is due to the nonequilibrium α→ω transition. The inferred rate of the α→ω transition is several orders of magnitude higher than that measured in dynamic diamond anvil cell (DDAC) experiments in an overlapping pressure range. We discuss a model for the influence of shear stress on the nucleation rate. We find that the shear stress sji has the same effect on the nucleation rate as a pressure increase δP=cϵijsji/(ΔV/V), where c is a geometric constant ∼1 and ϵij are the transformation shear strains. The small fractional volume change ΔV/V≈0.1 at the α→ω transition amplifies the effect of shear stress, and we estimate that for this case δP is in the range of several GPa. Correcting our transition rate to a hydrostatic rate brings it approximately into line with the DDAC results, suggesting that shear stress plays a significant role in the transformation rate.

More Details
TYPE Journal Article YEAR 2022
DOIOSTIScopus

Model Validation Database for Fires Involving Fuels at Liquefied Natural Gas Facilities

Luketa, Anay L.

This document provides a description of the model evaluation protocol (MEP) database for fires involving liquefied natural gas (LNG) and processing fuels at LNG facilities. The purpose of the MEP is to provide procedures regarding the assessment of a model's suitability to predict thermal exclusion zones resulting from a fire. The database includes measurements from pool fire, jet fire, and fireball experiments which are provided in a spreadsheet. Users are to enter model results into the spreadsheet which automatically generates statistical performance measures and graphical comparisons with the experimental data. The intent of this document is to provide a description of the experiments and of the procedure required to carry out the validation portion of the MEP. In addition, the statistical performance measures, measurements for comparisons, and parameter variation are provided.

More Details
TYPE SAND Report YEAR 2022
DOIOSTI

Molecular Inclusion of Small Aging Products into the Hexanitrohexaazaisowurtzitane (CL-20) Lattice: Part I, Infrared Spectra

Propellants, Explosives, Pyrotechnics

Beste, Ariana B.; Alam, Mary K.

Accelerated aging studies of β CL-20 thin films deposited on glass surfaces in different environments (N2, air, air/water) were conducted. Samples were analyzed with attenuated total reflectance infrared (ATR-IR) spectroscopy. Spectral features of molecular lattice inclusions in CL-20 films aged in an air/water environment were observed. The features occurred after β CL-20 polymorph transformation to α CL-20 and were accompanied by the appearance of lattice water peaks. To assist ATR-IR peak assignment, density functional theory studies were performed, and IR spectra of α CL-20 lattice inclusions of small molecules that were identified as degradation products of CL-20 were computed. Simulated spectra of NO2, HNCO, N2O, and CO2 incorporated into partially hydrated α CL-20 matched the experimental spectrum of β CL-20 thin films aged in air/water.

More Details
TYPE Journal Article YEAR 2022
DOIOSTIScopus

SIESTA a Fatigue Solution: User's and Theory Manual

Ross, Michael R.

This report documents the fatigue code SIESTA that has been used for recently here at Sandia National Laboratories. It is written in two parts: the first as a user manual and the second as a theory manual. Currently employed in SIESTA are stress-life cycle approaches. Clients have requested the use of standards in particular analyses; therefore, the American Society of Mechanical Engineers, Boiler Pressure Vessel Code fatigue standards have been implemented. These include an elastic, an elastic-plastic, and a weld fatigue method. All three methods use a Max-Min cycle counting method that is appropriate for non-proportional loading. A Signed von Mises method that used a Rainflow Cycle Counting Method is also implemented. The Signed von Mises with the Rainflow Cycle Counting Method is appropriate for proportional loading. Several verification examples are noted and include comparisons to experimental data.

More Details
TYPE SAND Report YEAR 2022
DOIOSTI

NNSA Minority Serving Institute Partnership Program (MSIPP)--Indigenous Mutual Partnership to Advanced Cybersecurity Technology (ASPIRE, IMPACT and PAMER); FY22 Q2 Progress Report

Atcitty, Stanley A.; Moriarty, Dylan; Hernandez, Virginia K.

The following report summarizes the status update during this quarter for the National Nuclear Security Agency (NNSA) initiated Minority Serving Institution Partnership Plan's (MSIPP) projects titled, Indigenous Mutual Partnership to Advanced Cybersecurity Technology (ASPIRE), Indigenous Mutual Partnership to Advanced Cybersecurity Technology (IMPACT) and Partnership for Advanced Manufacturing Education and Research (PAMER).

More Details
TYPE SAND Report YEAR 2022
DOIOSTI

Infrasound direction of arrival determination using a balloon-borne aeroseismometer

JASA Express Letters

Bowman, Daniel B.; Rouse, Jerry W.; Krishnamoorthy, Siddharth; Silber, Elizabeth A.

Free-floating balloons are an emerging platform for infrasound recording, but they cannot host arrays sufficiently wide for multi-sensor acoustic direction finding techniques. Because infrasound waves are longitudinal, the balloon motion in response to acoustic loading can be used to determine the signal azimuth. This technique, called “aeroseismometry,” permits sparse balloon-borne networks to geolocate acoustic sources. This is demonstrated by using an aeroseismometer on a stratospheric balloon to measure the direction of arrival of acoustic waves from successive ground chemical explosions. A geolocation algorithm adapted from hydroacoustics is then used to calculate the location of the explosions.

More Details
TYPE Journal Article YEAR 2022
DOIOSTIScopus

GaAs Neutron Response Functions and Radiation Damage Metrics

Griffin, Patrick J.; Asper, Nicholas; Charlton, William

The radiation effects community needs clear, well-documented, neutron energy-dependent responses that can be used in assessing radiation-induced material damage to GaAs semiconductors and for correlating observed radiation-induced changes in the GaAs electronic properties with computed damage metrics. In support of the objective, this document provides: a) a clearly defined set of relevant neutron response functions for use in dosimetry applications; b) clear mathematical expressions for the defined response functions; and c) updated quantitative values for the energy- dependent response functions that reflect the best current nuclear data and modelling. This document recaps the legacy response functions. It then surveys the latest nuclear data and updates the recommended response function to support current GaAs damage studies. A detailed tabulation for six of the energy-dependent response functions is provided in an Appendix.

More Details
TYPE SAND Report YEAR 2022
DOIOSTI

Produced Water-Economic, Socio, Environmental Simulation Model (PW-ESEim) Model: Proof-of-Concept for Southeastern New Mexico

Tidwell, Vincent; Gunda, Thushara G.; Caballero, Mariah D.; Xu, Pei; Xu, Xuesong; Bernknopf, Rich; Broadbent, Craig; Malczynski, Leonard A.; Jacobson, Jake

A proof-of-concept tool, the Produced Water-Economic, Socio, Environmental Simulation model (PW-ESESim), was developed to support ease of analysis. The tool was designed to facilitate head-to-head comparison of alternative produced water source, treatment, and reuse water management strategies. A graphical user interface (GUI) guides the user through the selection and design of alternative produced water treatment and reuse strategies and the associated health and safety risk and economic benefits. At the highest conceptual level, alternative water strategies include the selection of a source water (locally or regionally available produced water), treatment strategy (pre-treatment, physical, chemical, biological, desalination, and post-treatment processes) and product water purpose (e.g., irrigation, industrial processing, environmental). After selection of these details, the PW-ESESim output a number of key economic, societal, environmental, public/ecological health and safety metrics to support user decision-making; specific examples include, cost of treatment, improvements in freshwater availability, human and ecologic health impacts and growth in local jobs and the economy. Through the simulation of different produced water treatment and management strategies, tradeoffs are identified and used to inform fit-for-purpose produced water treatment and reuse management decisions. While the tool was initially designed using Southeastern New Mexico (Permian Basin) as a case study, the general design of the PW-ESESim model can be extended to support other oil and gas regions of the U.S.

More Details
TYPE Other Report YEAR 2022
DOIOSTI

Measurements of Low-Mode Asymmetries in the Areal Density of Laser-Direct- Drive DT Cryogenic Implosions on OMEGA Using Neutron Spectroscopy

Forrest, Chad; Betti, Riccardo; Knauer, James; Glebov, Vladimir; Gopalaswamy, Varchas; Mohamed, Zaarah; Bahukutumbi, Radha; Regan, Sean; Schwemmlein, Arnold; Stoeckl, Christian; Theobald, Wolfgang; Frenje, Johan; Gatu Johnson, Maria; Appelbe, Brian; Crilly, Aidan; Mannion, Owen M.

Abstract not provided.

More Details
TYPE Conference Presenation YEAR 2022
DOIOSTI

Surrogate modeling for efficiently, accurately and conservatively estimating measures of risk

Reliability Engineering and System Safety

Jakeman, John D.; Kouri, Drew P.; Huerta, Jose G.

We present a surrogate modeling framework for conservatively estimating measures of risk from limited realizations of an expensive physical experiment or computational simulation. Risk measures combine objective probabilities with the subjective values of a decision maker to quantify anticipated outcomes. Given a set of samples, we construct a surrogate model that produces estimates of risk measures that are always greater than their empirical approximations obtained from the training data. These surrogate models limit over-confidence in reliability and safety assessments and produce estimates of risk measures that converge much faster to the true value than purely sample-based estimates. We first detail the construction of conservative surrogate models that can be tailored to a stakeholder's risk preferences and then present an approach, based on stochastic orders, for constructing surrogate models that are conservative with respect to families of risk measures. Our surrogate models include biases that permit them to conservatively estimate the target risk measures. We provide theoretical results that show that these biases decay at the same rate as the L2 error in the surrogate model. Numerical demonstrations confirm that risk-adapted surrogate models do indeed overestimate the target risk measures while converging at the expected rate.

More Details
TYPE Journal Article YEAR 2022
DOIOSTIScopus

Entangling-gate error from coherently displaced motional modes of trapped ions

Physical Review A

Ruzic, Brandon R.; Barrick, Todd A.; Hunker, Jeffrey D.; Law, Ryan L.; McFarland, Brian M.; McGuinness, Hayden J.; Parazzoli, L.P.; Sterk, Jonathan D.; Van Der Wall, Jay W.; Stick, Daniel L.

Entangling gates in trapped-ion quantum computers are most often applied to stationary ions with initial motional distributions that are thermal and close to the ground state, while those demonstrations that involve transport generally use sympathetic cooling to reinitialize the motional state prior to applying a gate. Future systems with more ions, however, will face greater nonthermal excitation due to increased amounts of ion transport and exacerbated by longer operational times and variations over the trap array. In addition, pregate sympathetic cooling may be limited due to time costs and laser access constraints. In this paper, we analyze the impact of such coherent motional excitation on entangling-gate error by performing simulations of Mølmer-Sørenson (MS) gates on a pair of trapped-ion qubits with both thermal and coherent excitation present in a shared motional mode at the start of the gate. We quantify how a small amount of coherent displacement erodes gate performance in the presence of experimental noise, and we demonstrate that adjusting the relative phase between the initial coherent displacement and the displacement induced by the gate or using Walsh modulation can suppress this error. We then use experimental data from transported ions to analyze the impact of coherent displacement on MS-gate error under realistic conditions.

More Details
TYPE Journal Article YEAR 2022
DOIOSTIScopus

Bioinspired synthesis of thermally stable and mechanically strong nanocomposite coatings

MRS Advances

Xu, Guangping X.; Fan, Hongyou F.; McCoy, C.A.; Mills, Melissa M.; Schwarz, Jens S.

Abstract: An innovative biomimetic method has been developed to synthesize layered nanocomposite coatings using silica and sugar-derived carbon to mimic the formation of a natural seashell structure. The layered nanocomposites are fabricated through alternate coatings of condensed silica and sugar. Sugar-derived carbon is a cost-effective material as well as environmentally friendly. Pyrolysis of sugar will form polycyclic aromatic carbon sheets, i.e., carbon black. The resulting final nanocomposite coatings can survive temperatures of more than 1150 °C and potentially up to 1650 °C. These coatings have strong mechanical properties, with hardness of more than 11 GPa and elastic modulus of 120 GPa, which are 80% greater than those of pure silica. The layered coatings have many applications, such as shielding in the form of mechanical barriers, body armor, and space debris shields. Graphical abstract: [Figure not available: see fulltext.]

More Details
TYPE Journal Article YEAR 2022
DOIOSTIScopus

Big Hill Geomechanical Analysis Using M-D Viscoplastic Material Model

Park, Byoung P.

The integrity of wellbores at the interbed between the caprock and salt is a serious concern in the Big Hill site. For the remediation and life extension of wellbores, more accurate predictions from the global model are needed. The Big Hill global model is improved using the M-D viscoplastic contact surface model and the mesh containing the interbed layer with contact surfaces between the salt and caprock layers, and fault blocks in overburden and caprock layers. The model calibration has been performed based on the cavern volumetric closures obtained from the Caveman calculations. The results agree well from 1991 to the early 2000s. The difference starts to widen after that, it might be because of frequent fluid movement and raw water injection. Therefore, the predictions from this improved model could be used to examine the structural integrity of caverns in Big Hill salt dome.

More Details
TYPE SAND Report YEAR 2022
DOIOSTI

Hazmat Incident in New Mexico: Sulfur Dioxide Alarm

Fire Engineering

Tinagero, Gary B.; Luna, Philip L.

Sandia National Laboratories (SNL) is a multimission laboratory located in Albuquerque, New Mexico, and is one of three National Nuclear Security Administration research and development laboratories located in the United States. Recently, SNL’s Emergency Response Team (ERT) responded to an incident involving a sulfur dioxide (SO2)-fixed monitor, setting off the alarm inside a laboratory and in the adjacent hallway. The potential sources for the alarm were various experiments involving batteries and an uninterrupted power supply (UPS) in the immediate area.

More Details
TYPE Journal Article YEAR 2022
OSTI

3D Simulations of OMEGA Implosions in Presence of Low Mode Asymmetries: Systematic Flow Anomalies and Impact of Low Modes on Implosion Performance

Colaitis, Arnaud; Igumenschev, Igor; Turnbull, David; Shah, Rahul; Edgell, Dana; Mannion, Owen M.; Stoeckl, Christian; Shvydky, Alex; Janezic, Roger; Kalb, Adam; Coa, Duc; Forrest, Chad; Kwiatkowski, Joe; Regan, Sean; Theobald, Wolfgang; Goncharov, Valeri; Froula, Dustin

Abstract not provided.

More Details
TYPE Conference Presenation YEAR 2022
DOIOSTI

EMP Testing of UL489 Circuit Breakers

Bowman, Tyler B.; Baca, Michael J.; Guttromson, Ross G.

Sandia National Laboratories (SNL) is performing a test campaign for the Department of Energy (DOE) Office of Cybersecurity, Energy Security, and Emergency Response (CESER) to address high-altitude electromagnetic pulse (HEMP) vulnerability of critical components of generation stations, with focus on early-time (E1) HEMP. The campaign seeks to establish response and damage thresholds for these critical elements in response to reasonable HEMP threat levels as a means for determining where vulnerabilities may exist or where mitigations may be needed. This report provides component vulnerability test results that will help to inform site vulnerability assessments and HEMP mitigation planning.

More Details
TYPE Other Report YEAR 2022
DOIOSTI

A study of sacrificial mirrors for use prior to a laser wakefield accelerator driven by the Z-Petawatt laser

Galloway, Benjamin R.; Rambo, Patrick K.; Geissel, Matthias G.; Kimmel, Mark W.; Kellogg, Jeffrey W.; Elle, Jennifer; Garrett, Travis; Porter, John L.; Rochau, G.A.

Many experiments at Sandia’s Z Pulsed Power Facility require x-ray backlighting diagnostics to understand experiment performance. Due to limitations in present-day source/detection modalities, most x-ray diagnostics at Z are restricted to photon energies <20 keV, ultimately limiting the density, amount, and atomic number of targets diagnosable in experiments. These limitations force the use of low-Z materials like Beryllium, and they prevent acquisition of important backlighting data for materials/densities that are opaque to soft x-rays and where background emission from the Z load and transmission lines overwhelm diagnostics. In this LDRD project, we have investigated the design and development of a laser wakefield acceleration platform driven by the Z-Petawatt laser – a platform that would enable the generation of a pulsed, collimated beam of high energy x-rays up to 100 keV. Geometrical considerations for implementation on the Z Machine require the use of sacrificial mirrors, which have been tested in offline experiments in the Chama target chamber in building 983. Our results suggest the use of sacrificial mirrors would not necessarily inhibit the laser wakefield x-ray process, particularly with the benefits stemming from planned laser upgrades. These conclusions support the continuation of laser wakefield source research and the development of the necessary infrastructure to deliver the Z-Petawatt laser to the Z center section along the appropriate lines of sight. Ultimately, this new capability will provide unprecedented views through dense states of matter, enabling the use of previously incompatible target materials/designs, and uncovering a new set of observables accessible through diffraction and spectroscopy in the hard x-ray regime. These will amplify the data return on precious Z shots and enhance Sandia’s ability to investigate fundamental physics in support of national security.

More Details
TYPE SAND Report YEAR 2022
DOIOSTI

Xyce™ Parallel Electronic Simulator Reference Guide, Version 7.5

Keiter, Eric R.; Russo, Thomas V.; Schiek, Richard S.; Thornquist, Heidi K.; Mei, Ting M.; Verley, Jason V.; Aadithya, Karthik V.; Schickling, Joshua D.

This document is a reference guide to the Xyce Parallel Electronic Simulator, and is a companion document to the Xyce Users' Guide. The focus of this document is (to the extent possible) exhaustively list device parameters, solver options, parser options, and other usage details of Xyce. This document is not intended to be a tutorial. Users who are new to circuit simulation are better served by the Xyce Users' Guide.

More Details
TYPE SAND Report YEAR 2022
DOIOSTI

Electrical-Discharge-Machining Contamination Removal from Metal Additively Manufactured Components

Banga, Dhego O.; Chames, Jeffery M.; Yee, Joshua K.; Jankowski, Alan F.

The use of an electrochemical dissolution process is shown to remove the recast layer contamination from the surfaces of electrical-discharge-machining cut components, as well as the interior exposed surfaces of the structure. The solution chemistry, cell potential, and exposure time are all relevant interdependent variables. Optimization of the electrode geometry should be made for each type of component. For the case of Cu-Zn recast contamination of 300-series alloy components, surface composition analysis indicates that complete electrochemical dissolution is achieved using a dilute solution of nitric acid (HNO3). For example, electrochemical dissolution of the Cu-Zn recast is accomplished at 1.2 V cell potential using a 20% nitric solution and an exposure time of 4 h. The use of a nitric acid bath was specifically chosen since it’s chemically compatible and will not degrade the host alloy or the component. In sum, an electrochemically driven dissolution process can be tailored to remove of the recast contamination without affecting the integrity of the host component structure and its dimensional tolerances.

More Details
TYPE SAND Report YEAR 2022
DOIOSTI

DECOVALEX 2023 Task D -- Interim Report from SNL

Jove Colon, Carlos F.; Lopez, Carlos M.; Kuhlman, Kristopher L.

The capability of a 1-D PFLOTRAN model to simulate the S1-3 bentonite saturation experiment has been demonstrated and validated against experimental data. Work remains to be done to refine 1-D PFLOTRAN simulations of the experiment S1-4 which include evaluation of parameter sensitivities on the prediction of material saturation and relative permeabilities. This and further testing of PFLOTRAN capabilities will be done as part of DECOVALEX 2023 Task D contributions by the SNL team in the coming months.

More Details
TYPE Other Report YEAR 2022
DOIOSTI

Impact Response of Control Atmosphere Plasma Spray Deposited Materials

Branch, Brittany A.; McCoy, C.A.; Vackel, Andrew V.

Thermal spray processing of metals and respective blends is becoming increasingly attractive due to the unique properties such as increased yield strength, low ductility, and differences in tensile and compressive strengths that result from microstructural features due to the spray process compared to other additive manufacturing methods. Here we report the results of plate impact experiments applied to Controlled Atmosphere Plasma Spray deposits of tantalum (Ta), niobium (Nb), and a tantalum-niobium blend (TaNb). These methods allowed for definition of the Hugoniot for each material type and the assessment of the Hugoniot Elastic Limit (HEL). Spallation experiments were conducted, and soft recovery of each material type allowed for scanning electron microscopy to characterize the fracture mechanism during tensile loading.

More Details
TYPE SAND Report YEAR 2022
DOIOSTI
Results 5401–5600 of 96,771
Results 5401–5600 of 96,771