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Shock margin testing of a one-axis MEMS accelerometer

Tanner, Danelle M.; Parson, Ted B.; Buchheit, Thomas E.

Shock testing was performed on a selected commercial-off-the-shelf - MicroElectroMechanical System (COTS-MEMS) accelerometer to determine the margin between the published absolute maximum rating for shock and the 'measured' level where failures are observed. The purpose of this testing is to provide baseline data for isolating failure mechanisms under shock and environmental loading in a representative device used or under consideration for use within systems and assemblies of the DOD/DOE weapons complex. The specific device chosen for this study was the AD22280 model of the ADXL78 MEMS Accelerometer manufactured by Analog Devices Inc. This study focuses only on the shock loading response of the device and provides the necessary data for adding influence of environmental exposure to the reliability of this class of devices. The published absolute maximum rating for acceleration in any axis was 4000 G for this device powered or unpowered. Results from this study showed first failures at 8000 G indicating a margin of error of two. Higher shock level testing indicated that an in-plane, but off-axis acceleration was more damaging than one in the sense direction.

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Predicting the Hall-Petch effect in fcc metals using non-local crystal plasticity

International Journal of Plasticity

Counts, William A.; Braginsky, Michael V.; Battaile, Corbett C.; Holm, Elizabeth A.

Many conventional continuum approaches to solid mechanics do not address the size sensitivity of deformation to microstructural features like grain boundaries, and are therefore unable to capture much of the experimentally observed behavior of polycrystal deformation. We propose a non-local crystal plasticity model, in which the geometrically necessary dislocation (GND) density is calculated using a non-local integral approach. The model is based on augmented FeFp kinematics, which account for the initial microstructure (primarily grain boundaries) present in the polycrystal. With the augmented kinematics, the initial GND and the evolving GND state are determined in a consistent manner. The expanded kinematics and the non-local crystal plasticity model are used to simulate the tensile behavior in copper polycrystals with different grain sizes ranging from 14 μm to 244 μm. The simulation results show a grain size dependence on the polycrystal's yield strength, which are in good agreement with the experimental data. © 2007 Elsevier Ltd. All rights reserved.

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Analysis of flow-cytometer scattering and fluorescence data to identify particle mixtures

Proceedings of SPIE - The International Society for Optical Engineering

Reichardt, Thomas A.; Bisson, Scott E.; Crocker, Robert W.; Kulp, Thomas J.

As part of the U.S. Department of Homeland Security Detect-to-Protect program, a multilab [Sandia National Laboratories (SNL), Lawrence Livermore National Laboratories (LLNL), Pacific Northwest National Laboratory (PNNL), Oak Ridge National Laboratory (ORNL), and Los Alamos National Laboratory (LANL)] effort is addressing the need for useable detect-to-warn bioaerosol sensors for public facility protection. Towards this end, the SNL team is employing rapid fluorogenic staining to infer the protein content of bioaerosols. This is being implemented in a flow cytometry platform wherein each particle detected generates coincident signals of forward scatter, side scatter, and fluorescence. Several thousand such coincident signal sets are typically collected to generate a probability distribution over the scattering and fluorescence values. A linear unmixing analysis is performed to differentiate components in the mixture. After forming a library of pure component distributions from measured pure material samples, the distribution of an unknown mixture of particles is treated as a linear combination of the pure component distributions. The scattering/fluorescence probability distribution data vector a is considered the product of two vectors, the fractional profile f and the scattering/ fluorescence distributions from pure components P. A least squares procedure minimizes the magnitude of the residual vector e in the expression a = fP T + e. The profile f designates a weighting fraction for each particle type included in the set of pure components, providing the composition of the unknown mixture. We discuss testing of this analysis approach and steps we have taken to evaluate the effect of interferents, both known and unknown.

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Beamforming as a foundation for spotlight-mode SAR image formation by backprojection

Proceedings of SPIE - The International Society for Optical Engineering

Jakowatz, Charles V.; Wahl, Daniel E.; Yocky, David A.

In this paper we show that the technique for spotlight-mode SAR image formation generally known as "backprojection" or "time- domain" is most easily derived and described in terms of the well-known methods of phased-array beamforming. By contrast, backprojection has been typically developed via analogy to tomographic imaging [1], which restricts this technique to the case of planar wavefronts. We demonstrate how the very simple notion of delay-and-sum beamforming leads directly to the backprojection algorithm for SAR, including the case for curved wavefronts. We further explain why backprojection offers a certain elegant simplicity for SAR imaging, and allows direct one-step computation of several useful SAR products, including an orthographically correct image free of any geometric or defocus effects from wavefront curvature and also free of the effects of terrain-elevation-induced defocus. (This product requires as an input a pre-existing digital elevation map (DEM) of the scene to be imaged.) In addition, we'll demonstrate why beamforming yields a mode-independent SAR image formation algorithm, i.e. one that can just as easily accommodate strip-map or spotlight-mode phase histories collected on an arbitrary flight path.

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Fiber faceplates to mitigate diffraction effects in an imaging snapshot polarimeter

Proceedings of SPIE - The International Society for Optical Engineering

Cruz-Cabrera, A.A.; Kemme, S.A.; Carter, T.R.

We investigate the advantages of employing a fiber faceplate in a snapshot polarimetry system. Our previous work at Sandia National Laboratories indicates that diffraction and propagation between the micropolarizer array, the micro-waveplate array, and the Focal Plane Array (FPA) degrade performance, as quantified by the extinction ratio1,2. Crosstalk between adjacent pixels due to diffraction increases uncertainty of the measured polarization states in a scene of interest. These issues are exacerbated in the long-wavelength regime and as FPA pixel dimensions decrease. One solution, since it minimizes propagation distance, is to construct the micropolarizer and micro-waveplate arrays on a single substrate surface and to place this combination on the FPA3. This solution is a significant fabrication challenge and decreases yield due to its serial assembly nature. An alternative solution that would improve yield is to fabricate the micropolarizer on top of a fiber faceplate, place the faceplate on the FPA with the micropolarizer facing away, then place the waveplate array on top of the micropolarizer. The optical field that passes through the plane of the microwaveplate array and the micropolarizer array is guided to the FPA plane, without suffering diffraction effects associated with free-space propagation. We will quantify the utility of these proposed configurations with predicted imaging polarimetric system extinction ratios.

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Confirmatory measurement channels for LIF-based bioaerosol instrumentation

Proceedings of SPIE - The International Society for Optical Engineering

Bisson, Scott E.; Crocker, Robert W.; Kulp, Thomas J.; Reichardt, Thomas A.; Reilly, Peter T.A.; Whitten, William B.

As part of the U.S. Department of Homeland Security Detect-to-Protect (DTP) program, a multilab [Sandia National Laboratories (SNL), Lawrence Livermore National Laboratories (LLNL), Pacific Northwest National Laboratory (PNNL), Oak Ridge National Laboratory (ORNL), and Los Alamos National Laboratory (LANL)] effort is addressing the need for useable detect-to-warn bioaerosol sensors for public facility protection. Towards this end, the SNL team is investigating the use of rapid fluorogenic staining to infer the protein content of bioaerosols. This is being implemented in a flow cytometer wherein each particle detected generates coincident signals of correlated forward scatter, side scatter, and fluorescence. Several thousand such coincident signal sets are typically collected to generate a distribution describing the probability of observing a particle with certain scattering and fluorescence values. These data are collected for sample particles in both a stained and unstained state. A linear unmixing analysis is performed to differentiate components in the mixture. In this paper, we discuss the implementation of the staining process and the cytometric measurement, the results of their application to the analysis of known and blind samples, and a potential instrumental implementations that would use staining.

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Approximate constitutive relation for lap joints using a tribo-mechanical approach

2007 Proceedings of the ASME International Design Engineering Technical Conferences and Computers and Information in Engineering Conference, DETC2007

Farhang, K.; Segalman, Daniel J.; Starr, M.

Energy dissipation in mechanical joints occurs as a result of micro-slip motion between contacting rough surfaces. An account of this phenomenon is especially challenging due to the vast differences in the length and time scale differences between the macro-mechanical structure and the micron-scale events at the joint interface. This paper considers the contact between two nominally flat surfaces containing micron-scale roughness. The rough surface interaction is viewed as a multi-sphere elastic interaction subject to a periodic tangential force. It combines the Mindlin's formulation [1,2] for the elastic interaction of two spheres with the Greenwood and Williamson's [3] statistical approach for the contact of two nominally flat rough surfaces so as to develop a model for multi-sphere problem in which sphere radii, contact load and the number of spheres in contact can only be known in a statistical sense and not deterministically. Copyright © 2007 by ASME.

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Theory of enhancement of thermoelectric properties of materials with nanoinclusions

Physical Review B - Condensed Matter and Materials Physics

Faleev, Sergey V.; Leonard, Francois L.

Based on the concept of band bending at metal/semiconductor interfaces as an energy filter for electrons, we present a theory for the enhancement of the thermoelectric properties of semiconductor materials with metallic nanoinclusions. We show that the Seebeck coefficient can be significantly increased due to a strongly energy-dependent electronic scattering time. By including phonon scattering, we find that the enhancement of ZT due to electron scattering is important for high doping, while at low doping it is primarily due to a decrease in the phonon thermal conductivity. © 2008 The American Physical Society.

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A beryllium dome specimen holder for XRD analysis of air sensitive materials

Powder Diffraction

Rodriguez, Marko A.; Boyle, Timothy J.; Yang, Pin Y.; Harris, Damon L.

A specially designed specimen holder employing a beryllium dome has been fabricated for collection of X-ray diffraction (XRD) data from highly reactive materials. The specimen holder has a robust O-ring type seal (< 10-9 Torr) and no observed intensity artifacts in the 1° to 150° 2θ range. The design also minimizes specimen displacement errors and allows for analysis of both powders and bulk specimens (i.e., pellets). The simple design makes for straightforward assembly of the holder within the confines of a glove box. XRD analysis of hygroscopic LaBr3 powders collected with this holder are suitable for Rietveld structure refinement, yielding unit cell lattice parameters of a=7.9703(6) Å and c=4.5122(6) Å cell volume= 248.44(6) Å3; Rp =7.70%. © 2008 International Centre for Diffraction Data.

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Three-dimensional effects in trailing mass in the wire-array Z pinch

Physics of Plasmas

Yu, Edmund Y.; Cuneo, M.E.; Desjarlais, Michael P.; Lemke, Raymond W.; Sinars, Daniel S.; Haill, Thomas A.; Waisman, E.M.; Bennett, G.R.; Jennings, C.A.; Mehlhorn, T.A.; Brunner, T.A.; Hanshaw, H.L.; Porter, J.L.; Stygar, W.A.; Rudakov, L.I.

The implosion phase of a wire-array Z pinch is investigated using three-dimensional (3D) simulations, which model the mass ablation phase and its associated axial instability using a mass injection boundary condition. The physical mechanisms driving the trailing mass network are explored, and it is found that in 3D the current paths though the trailing mass can reduce bubble growth on the imploding plasma sheath, relative to the 2D (r,z) equivalent. Comparison between the simulations and a high quality set of experimental radiographs is presented. © 2008 American Institute of Physics.

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A hybrid constraint programming / local search approach to the job-shop scheduling problem

Lecture Notes in Computer Science (including subseries Lecture Notes in Artificial Intelligence and Lecture Notes in Bioinformatics)

Watson, Jean-Paul W.; Beck, J.C.

Since their introduction, local search algorithms - and in particular tabu search algorithms - have consistently represented the state-of-the-art in solution techniques for the classical job-shop scheduling problem. This is despite the availability of powerful search and inference techniques for scheduling problems developed by the constraint programming community. In this paper, we introduce a simple hybrid algorithm for job-shop scheduling that leverages both the fast, broad search capabilities of modern tabu search and the scheduling-specific inference capabilities of constraint programming. The hybrid algorithm significantly improves the performance of a state-of-the-art tabu search for the job-shop problem, and represents the first instance in which a constraint programming algorithm obtains performance competitive with the best local search algorithms. Further, the variability in solution quality obtained by the hybrid is significantly lower than that of pure local search algorithms. As an illustrative example, we identify twelve new best-known solutions on Taillard's widely studied benchmark problems. © 2008 Springer-Verlag Berlin Heidelberg.

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Lithographically defined carbon growth templates for ELOG of GaN

Journal of Crystal Growth

Burckel, D.B.; Fan, Hongyou F.; Thaler, Gerald T.; Koleske, Daniel K.

We report the initial use of lithographically defined carbon growth templates for use as an epitaxial lateral overgrowth (ELOG) mask for metalorganic chemical vapor deposition (MOCVD) heteroepitaxial GaN on sapphire. Interferometric lithography is used to define high aspect ratio structures in SU-8, which are then pyrolyzed in a reducing atmosphere up to 1200 °C. The resist structures convert to amorphous carbon, shrinking 80% in the vertical direction and 53% in the horizontal direction, but maintain their pattern geometry and adhesion to the substrate. These templates are capable of surviving GaN nucleation layer growth temperatures (∼530 °C), GaN crystal growth and high-temperature annealing up to 1050 °C. This new approach to ELOG offers several advantages, requiring fewer processing steps, and favorable selectivity tendencies as well as the capability to create growth masks which are difficult or impossible to fabricate using a top-down etching approach. © 2008 Elsevier B.V. All rights reserved.

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Tunable arrays of ZnO nanorods and nanoneedles via seed layer and solution chemistry

Crystal Growth and Design

Lee, Yun J.; Sounart, Thomas L.; Liu, Jun; Spoerke, Erik D.; McKenzie, Bonnie B.; Hsu, Julia W.; Voigt, James A.

We have systematically studied the effect of pH and 1,3-diaminopropane additive concentration on the morphology of ZnO nanorod and nanoneedle arrays grown in aqueous solution using a variety of seed layers. Increase in the growth solution pH from 6.8 to 13.2 resulted in a near doubling of the growth rate in the [0001] direction possibly due to attractive interaction between the zinc species and the growth surface at high pH, leading to nanorod arrays with reduced faceting and higher aspect ratios. Increases in 1,3-diaminopropane concentration initially enhanced and subsequently inhibited growth of tapered ZnO nanoneedles on seed layers consisting of ZnO nanoparticles, oriented ZnO films, or columnar facets of ZnO microrods. The final nanoneedle dimensions, packing density, and alignment were strongly affected by 1,3-diaminopropane concentration and seed layer type, which can be explained in terms of the relative strength of zinc chelation by 1,3-diaminopropane, the areal density of seeds, and other factors. The precise tuning of ZnO crystalline morphology via the control of seeding and growth conditions may be beneficial to many potential applications that require these aligned crystalline nanostructures. © 2008 American Chemical Society.

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Site Environmental Report for 2007: Sandia National Laboratories, California

Larsen, Barbara L.

Sandia National Laboratories, California (SNL/CA) is a government-owned/contractor-operated laboratory. Sandia Corporation, a Lockheed Martin Company, operates the laboratory for the Department of Energy’s National Nuclear Security Administration (NNSA). The NNSA Sandia Site Office oversees operations at the site, using Sandia Corporation as a management and operating contractor. This Site Environmental Report for 2007 was prepared in accordance with DOE Order 231.1A (DOE 2004a). The report provides a summary of environmental monitoring information and compliance activities that occurred at SNL/CA during calendar year 2007. General site and environmental program information is also included.

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On the secure obfuscation of deterministic finite automata

Anderson, William E.

In this paper, we show how to construct secure obfuscation for Deterministic Finite Automata, assuming non-uniformly strong one-way functions exist. We revisit the software protection approaches originally proposed by [5, 10, 12, 17] and revise them to the current obfuscation setting of Barak et al. [2]. Under this model, we introduce an efficient oracle that retains some 'small' secret about the original program. Using this secret, we can construct an obfuscator and two-party protocol that securely obfuscates Deterministic Finite Automata against malicious adversaries. The security of this model retains the strong 'virtual black box' property originally proposed in [2] while incorporating the stronger condition of dependent auxiliary inputs in [15]. Additionally, we show that our techniques remain secure under concurrent self-composition with adaptive inputs and that Turing machines are obfuscatable under this model.

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Reduced-order model-based feedback control of flow over an obstacle using center manifold methods

Proposed for publication in the American Society of Mechanical Engineers publication.

Camphouse, Russell C.

In this paper, we consider a boundary control problem governed by the two-dimensional Burgers equation for a configuration describing convective flow over an obstacle. Flows over obstacles are important as they arise in many practical applications. Burgers equations are also significant as they represent a simpler form of the more general Navier-Stokes momentum equation describing fluid flow. The aim of the work is to develop a reduced-order boundary control-oriented model for the system with subsequent nonlinear control law design. The control objective is to drive the full order system to a desired 2D profile. Reduced-order modeling involves the application of an L{sub 2} optimization based actuation mode expansion technique for input separation, demonstrating how one can obtain a reduced-order Galerkin model in which the control inputs appear as explicit terms. Controller design is based on averaging and center manifold techniques and is validated with full order numerical simulation. Closed-loop results are compared to a standard linear quadratic regulator design based on a linearization of the reduced-order model. The averaging/center manifold based controller design provides smoother response with less control effort and smaller tracking error.

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In-situ time-of-flight neutron diffraction of ErD2 (beta phase) formation during D2 loading

Rodriguez, M.A.; Snow, Clark S.; Wixom, Ryan R.

In an effort to better understand the structural changes occurring during hydrogen loading of erbium target materials, we have performed D{sub 2} loading of erbium metal (powder) with simultaneous neutron diffraction analysis. This experiment tracked the conversion of Er metal to the {alpha} erbium deuteride (solid-solution) phase and then on to the {beta} (fluorite) phase. Complete conversion to ErD{sub 2.0} was accomplished at 10 Torr D{sub 2} pressure with deuterium fully occupying the tetrahedral sites in the fluorite lattice. Increased D{sub 2} pressure (up to 500 Torr at 450 C) revealed {approx}10 % deuterium occupation of the octahedral sites. Subsequent vacuum pumping of the sample at 450 C removed octahedral site occupancy while maintaining tetrahedral deuterium occupancy, thereby yielding stoichiometric ErD{sub 2.0} {beta} phase.

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THRIVE : a data reduction program for three-phase PDV/PDI and VISAR measurements

Dolan, Daniel H.; Jones, Scott C.

THRIVE (THRee Interferometer VElocimetry) is an analysis package for reducing three-phase interferometry measurements. Three-phase displacement interferometry measurements are the primary application of this program, although velocity interferometry is also supported. THRIVE uses a push-pull approach to transform measured signals to a pair of quadrature signals, from which fringe shift, target position, and target velocity are inferred. The program can analyze the signals in an ideal sense or compensate for non-ideal measurement conditions using ellipse characterization. The program can be run in any current version of MATLAB (release 2007a or later) or as a Windows XP executable.

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InGaN/GaN multi-quantum well and LED growth on wafer-bonded sapphire-on-polycrystalline AlN substrates by metalorganic chemical vapor deposition

Proposed for publication in the Journal of Crystal Growth.

Koleske, Daniel K.; Crawford, Mary H.; Thaler, Gerald T.; Russell, Michael J.

We report growth of InGaN/GaN multi-quantum well (MQW) and LED structures on a novel composite substrate designed to eliminate the coefficient of thermal expansion (CTE) mismatch problems which impact GaN growth on bulk sapphire. To form the composite substrate, a thin sapphire layer is wafer-bonded to a polycrystalline aluminum nitride (P-AlN) support substrate. The sapphire layer provides the epitaxial template for the growth; however, the thermo-mechanical properties of the composite substrate are determined by the P-AlN. Using these substrates, thermal stresses associated with temperature changes during growth should be reduced an order of magnitude compared to films grown on bulk sapphire, based on published CTE data. In order to test the suitability of the substrates for GaN LED growth, test structures were grown by metalorganic chemical vapor deposition (MOCVD) using standard process conditions for GaN growth on sapphire. Bulk sapphire substrates were included as control samples in all growth runs. In situ reflectance monitoring was used to compare the growth dynamics for the different substrates. The material quality of the films as judged by X-ray diffraction (XRD), photoluminescence and transmission electron microscopy (TEM) was similar for the composite substrate and the sapphire control samples. Electroluminescence was obtained from the LED structure grown on a P-AlN composite substrate, with a similar peak wavelength and peak width to the control samples. XRD and Raman spectroscopy results confirm that the residual strain in GaN films grown on the composite substrates is dramatically reduced compared to growth on bulk sapphire substrates.

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Results 75801–76000 of 96,771
Results 75801–76000 of 96,771