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EPRI/NRC fire human reliability analysis guidelines

American Nuclear Society - International Topical Meeting on Probabilistic Safety Assessment and Analysis, PSA 2008

Cooper, Susan E.; Hill, Kendra; Julius, Jeff; Grobbelaar, Jan; Kohlhepp, Kaydee; Forester, John A.; Hendrickson, Stacey M.; Hannaman, Bill; Najafi, Bijan

During the 1990's the Electric Power Research Institute (EPRI) developed methods for fire risk analysis to support its utility members in the preparation of responses to Generic Letter 88-20, Supplement 4, "Individual Plant Examination - External Events" (IPEEE). This effort produced a Fire Risk Assessment methodology for at-power that was used by the majority of US Nuclear Power Plants (NPPs) in support of the IPEEE program and several NPPs oversees. Although these methods were acceptable for accomplishing the objectives of the IPEEE, EPRI and the U.S. Nuclear Regulatory Commission (NRC) recognized that these methods require upgrades to support current requirements for Risk-Informed/Performance-Based (RI/PB) applications. In 2001 EPRI and the NRC Office of Nuclear Regulatory Research (RES) embarked on a cooperative project to improve the state-of-the-art in fire risk assessment to support this new risk-informed environment in fire protection. This project produced a consensus document, NUREG/CR-6850 (EPRI 1011989), entitled "Fire PRA Methodology for Nuclear Power Facilities" which addresses fire risk for at-power operations. This report developed: 1) the process for identification and inclusion of the post-fire Human Failure Events (HFEs), 2) the methodology for assigning quantitative screening values to these HFEs, and 3) the initial considerations of performance shaping factors (PSFs) and related fire effects that may need to be addressed in developing best-estimate Human Error Probabilities (HEPs). However, this document does not describe a methodology to develop these best-estimate HEPs given the PSFs and the fire-related effects. In 2007 EPRI and NRC's RES embarked on another cooperative project to develop explicit guidance for estimating HEPs for human error events under fire generated conditions, building upon existing human reliability analysis (HRA) methods. This paper will describe the progress to date on the development and testing of the fire HRA methodology, which includes addressing the range of fire procedures used in existing plants, the range of strategies for main control room abandonment, and the potential impact of fire-induced spurious electrical effects on crew performance. In addition to developing a detailed HRA approach, one goal of the project is to develop a fire HRA scoping quantification approach that allows derivation of more realistic HEPs than those in the screening approach from NUREG/CR-6850 (EPRI 1011989), while requiring less analytic resources than a detailed HRA. In this approach, detailed HRA will be used only for the more complex actions that cannot meet the criteria for the scoping approach.

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Controlling across complex networks - Emerging links between networks and control

Annual Reviews in Control

Clauset, A.; Tanner, H.G.; Abdallah, C.T.; Byrne, R.H.

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A family of energy minimizing coarse spaces for overlapping schwarz preconditioners

Lecture Notes in Computational Science and Engineering

Dohrmann, Clark R.; Klawonn, Axel; Widlund, Olof B.

A simple and effective approach is presented to construct coarse spaces for overlapping Schwarz preconditioners. The approach is based on energy minimizing extensions of coarse trace spaces, and can be viewed as a generalization of earlier work by Dryja, Smith, and Widlund. The use of these coarse spaces in overlapping Schwarz preconditioners leads to condition numbers bounded by C(1 + H/δ)(1 + log(H/h)) for certain problems when coefficient jumps are aligned with subdomain boundaries. For problems without coefficient jumps, it is possible to remove the log(H/h) factor in this bound by a suitable enrichment of the coarse space. Comparisons are made with the coarse spaces of two other substructuring preconditioners. Numerical examples are also presented for a variety of problems.

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Strip transect sampling to estimate object abundance in homogeneous and non-homogeneous poisson fields: A simulation study of the effects of changing transect width and number

Progress in Geomathematics

Coburn, Timothy C.; Mckenna, Sean A.; Saito, Hirotaka

This paper investigates the use of strip transect sampling to estimate object abundance when the underlying spatial distribution is assumed to be Poisson. A design-rather than model-based approach to estimation is investigated through computer simulation, with both homogeneous and non-homogeneous fields representing individual realizations of spatial point processes being considered. Of particular interest are the effects of changing the number of transects and transect width (or alternatively, coverage percent or fraction) on the quality of the estimate. A specific application to the characterization of unexploded ordnance (UXO) in the subsurface at former military firing ranges is discussed. The results may be extended to the investigation of outcrop characteristics as well as subsurface geological features. © 2008 Springer-Verlag Berlin Heidelberg.

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Reduced-Volume horn antennas with integrated high-impedance electromagnetic surfaces

Proceedings of 2008 Asia Pacific Microwave Conference, APMC 2008

Forman, Michael F.

Several antennas with integrated high-impedance surfaces are presented. The high-impedance surface is implemented as a composite right/left-handed (CRLH) metamaterial fabricated from a periodic structure characterized by a substrate, filled with an array of vertical vias and capped by capacitive patches. Omnidirectional antennas placed in close proximity to the high-impedance surface radiate hemispherically with an increase in boresight far-field pattern gain of up to 10 dB and a front-to-back ratio as high as 13 dB at 2.45 GHz. Several TEM rectangular horn antennas are realized by replacing conductor walls with high-impedance surfaces. The TEM horn antennas are capable of operating below the TE{sub 1,0} cutoff frequency of a standard all-metal horn antenna, enabling a reduction in antenna volume. Above the cutoff frequency the TEM horn antennas function similarly to standard rectangular horn antennas.

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Modeling an unstructured driving domain: A comparison of two cognitive frameworks

2008 BRIMS Conference - Behavior Representation in Modeling and Simulation

Best, Bradley J.; Dixon, Kevin R.; Speed, Ann; Fleetwood, Michael D.

This paper outlines a comparison between two cognitive modeling frameworks: Atomic Components of Thought - Rational (ACT-R; Anderson & Lebiere, 1998) and a framework under development at Sandia National Laboratories. Both frameworks are based on the cognitive psychological literature, although they represent different theoretical perspectives on cognition, with ACT-R being a production-rule-based system and the Sandia framework being a dynamical-systems or connectionist-type approach. This comparison involved a complex driving domain in which both the car being driven and the driver were equipped with sensors that provided information to each framework. The output of each framework was a classification of the real-world situation that the driver was in, e.g., being overtaken on the autobahn. Comparisons between the two frameworks included validation against human ratings of the driving situations via videotapes of driving sessions, along with twelve creation and performance metrics regarding the method and ease of framework population, processor requirements, and maximum real-time data sampling rate.

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Discussion tracking in enron email using PARAFAC

Survey of Text Mining II: Clustering, Classification, and Retrieval

Bader, Brett W.; Berry, Michael W.; Browne, Murray

In this chapter, we apply a nonnegative tensor factorization algorithm to extract and detect meaningful discussions from electronic mail messages for a period of one year. For the publicly released Enron electronic mail collection, we encode a sparse term-author-month array for subsequent three-way factorization using the PARAllel FACtors (or PARAFAC) three-way decomposition first proposed by Harshman. Using nonnegative tensors, we preserve natural data nonnegativity and avoid subtractive basis vector and encoding interactions present in techniques such as principal component analysis. Results in thread detection and interpretation are discussed in the context of published Enron business practices and activities, and benchmarks addressing the computational complexity of our approach are provided. The resulting tensor factorizations can be used to produce Gantt-like charts that can be used to assess the duration, order, and dependencies of focused discussions against the progression of time. © 2008 Springer-Verlag London.

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Laboratory simulation of drill bit dynamics using a model-based servohydraulic controller

Journal of Energy Resources Technology, Transactions of the ASME

Raymond, David W.; Elsayed, M.A.; Polsky, Yarom P.; Kuszmaul, Scott S.

Drilling costs are significantly influenced by bit performance when drilling in offshore formations. Retrieving and replacing damaged downhole tools is an extraordinarily expensive and time-intensive process, easily costing several hundred thousand dollars of offshore rig time plus the cost of damaged components. Dynamic behavior of the drill string can be particularly problematic when drilling high strength rock, where the risk of bit failure increases dramatically. Many of these dysfunctions arise due to the interaction between the forces developed at the bit-rock interface and the modes of vibration of the drill string. Although existing testing facilities are adequate for characterizing bit performance in various formations and operating conditions, they lack the necessary drill string attributes to characterize the interaction between the bit and the bottom hole assembly (BHA). A facility that includes drill string compliance and yet allows real-rock/ bit interaction would provide an advanced practical understanding of the influence of drill string dynamics on bit life and performance. Such a facility can be used to develop new bit designs and cutter materials, qualify downhole component reliability, and thus mitigate the harmful effects of vibration. It can also serve as a platform for investigating process-related parameters, which influence drilling performance and bit-induced vibration to develop improved practices for drilling operators. The development of an advanced laboratory simulation capability is being pursued to allow the dynamic properties of a BHA to be reproduced in the laboratory. This simulated BHA is used to support an actual drill bit while conducting drilling tests in representative rocks in the laboratory. The advanced system can be used to model the response of more complex representations of a drill string with multiple modes of vibration. Application of the system to field drilling data is also addressed. Copyright © 2008 by ASME.

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Finite element solution of optimal control problems arising in semiconductor modeling

Lecture Notes in Computer Science (including subseries Lecture Notes in Artificial Intelligence and Lecture Notes in Bioinformatics)

Bochev, Pavel B.; Ridzal, Denis R.

Optimal design, parameter estimation, and inverse problems arising in the modeling of semiconductor devices lead to optimization problems constrained by systems of PDEs. We study the impact of different state equation discretizations on optimization problems whose objective functionals involve flux terms. Galerkin methods, in which the flux is a derived quantity, are compared with mixed Galerkin discretizations where the flux is approximated directly. Our results show that the latter approach leads to more robust and accurate solutions of the optimization problem, especially for highly heterogeneous materials with large jumps in material properties. © 2008 Springer.

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New applications of the verdict library for standardized mesh verification pre, post, and end-to-end processing

Proceedings of the 16th International Meshing Roundtable, IMR 2007

Pébay, Philippe P.; Thompson, David; Shepherd, Jason F.; Knupp, Patrick K.; Lisle, Curtis; Magnotta, Vincent A.; Grosland, Nicole M.

Verdict is a collection of subroutines for evaluating the geometric qualities of triangles, quadrilaterals, tetrahedra, and hexahedra using a variety of functions. A quality is a real number assigned to one of these shapes depending on its particular vertex coordinates. These functions are used to evaluate the input to finite element, finite volume, boundary element, and other types of solvers that approximate the solution to partial differential equations defined over regions of space. This article describes the most recent version of Verdict and provides a summary of the main properties of the quality functions offered by the library. It finally demonstrates the versatility and applicability of Verdict by illustrating its use in several scientific applications that pertain to pre, post, and end-to-end processing.

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A selective approach to conformal refinement of unstructured hexahedral finite element meshes

Proceedings of the 16th International Meshing Roundtable, IMR 2007

Parrish, Michael; Borden, Michael; Staten, Matthew; Benzley, Steven

Hexahedral refinement increases the density of an all-hexahedral mesh in a specified region, improving numerical accuracy. Previous research using solely sheet refinement theory made the implementation computationally expensive and unable to effectively handle concave refinement regions and self-intersecting hex sheets. The Selective Approach method is a new procedure that combines two diverse methodologies to create an efficient and robust algorithm able to handle the above stated problems. These two refinement methods are: 1) element by element refinement and 2) directional refinement. In element by element refinement, the three inherent directions of a Hex are refined in one step using one of seven templates. Because of its computational superiority over directional refinement, but its inability to handle concavities, element by element refinement is used in all areas of the specified region except regions local to concavities. The directional refinement scheme refines the three inherent directions of a hexahedron separately on a hex by hex basis. This differs from sheet refinement which refines hexahedra using hex sheets. Directional refinement is able to correctly handle concave refinement regions. A ranking system and propagation scheme allow directional refinement to work within the confines of the Selective Approach Algorithm.

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Methods and applications of generalized sheet insertion for hexahedral meshing

Proceedings of the 16th International Meshing Roundtable, IMR 2007

Merkley, Karl; Ernst, Corey; Shepherd, Jason F.; Borden, Michael J.

This paper presents methods and applications of sheet insertion in a hexahedral mesh. A hexahedral sheet is dual to a layer of hexahedra in a hexahedral mesh. Because of symmetries within a hexahedral element, every hexahedral mesh can be viewed as a collection of these sheets. It is possible to insert new sheets into an existing mesh, and these new sheets can be used to define new mesh boundaries, refine the mesh, or in some cases can be used to improve quality in an existing mesh. Sheet insertion has a broad range of possible applications including mesh generation, boundary refinement, R-adaptivity and joining existing meshes. Examples of each of these applications are demonstrated.

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pCAMAL: An embarrassingly parallel hexahedral mesh generator

Proceedings of the 16th International Meshing Roundtable, IMR 2007

Pébay, Philippe P.; Stephenson, Michael B.; Fortier, Leslie A.; Owen, Steven J.; Melander, Darryl J.

This paper describes a distributed-memory, embarrassingly parallel hexahedral mesh generator, pCAMAL (parallel CUBIT Adaptive Mesh Algorithm Library). pCAMAL utilizes the sweeping method following a serial step of geometry decomposition conducted in the CUBIT geometry preparation and mesh generation tool. The utility of pCAMAL in generating large meshes is illustrated, and linear speed-up under load-balanced conditions is demonstrated.

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Performance of a pulsed ion beam with a renewable cryogenically cooled ion source

Laser and Particle Beams

Renk, T.J.; Mann, Gregory A.; Torres, G.A.

For operation of an ion source in an intense ion beam diode, it is desirable to form a localized and robust source of high purity. A cryogenically operated ion source has great promise, since the ions are formed from a condensed high-purity gas, which has been confined to a relatively thin ice layer on the anode surface. Previous experiments have established the principles of operation of such an ion source, but have been limited in repetitive duration due to the use of short-lived liquid He cooling of the anode surface. We detail here the successful development of a Cryo-Diode in which the cooling was achieved with a closed-cycle cryo-pump. This results in an ion source design that can potentially be operated for an indefinite duration. Time-of-flight measurements with Faraday cups indicate that the resultant ion beam is of high-purity, and composed of singly charged ions formed out of the gas frozen out on the anode surface. © 2008 Copyright Cambridge University Press 2008.

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Distance-avoiding sequences for extremely low-bandwidth authentication

Lecture Notes in Computer Science (including subseries Lecture Notes in Artificial Intelligence and Lecture Notes in Bioinformatics)

Collins, Michael J.; Mitchell, Scott A.

We develop a scheme for providing strong cryptographic authentication on a stream of messages which consumes very little bandwidth (as little as one bit per message) and is robust in the presence of dropped messages. Such a scheme should be useful for extremely low-power, low-bandwidth wireless sensor networks and "smart dust" applications. The tradeoffs among security, memory, bandwidth, and tolerance for missing messages give rise to several new optimization problems. We report on experimental results and derive bounds on the performance of the scheme. © 2008 Springer-Verlag Berlin Heidelberg.

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A wet chemistry approach to sub-micron removable flip chip interconnects

Proceedings of SPIE - The International Society for Optical Engineering

Orendorff, Christopher O.; Barker, Joy M.; Rowen, Adam M.; Yelton, W.G.; Arrington, Christian L.; Gillen, J.R.

Higher performance is the main driver in the integrated circuit (IC) market, but along with added function comes the cost of increased input/output connections and larger die sizes. Space saving approaches aimed at solving these challenges includes two technologies; 3D stacking (3D-ICs) and flip chip assemblies. Emerging ICs require sub-micron scale interconnects which include vias for 3D-ICs and bump bonds for flip chips. Photolithographic techniques are commonly used to prepare templates followed by metal vapor deposition to create flip chip bump bonds. Both the lithography step and the metal properties required for bump bonding contribute to limiting this approach to a minimum bump size of ∼10 μm. Here, we present a wet chemistry approach to fabricating uniform bump bonds of tunable size and height down to the nanoscale. Nanosphere lithography (NSL), a "soft" lithographic technique, is used to create a bump bond template or mask for nanoscale bumps. Electrochemical deposition is also used through photoresist templates to create uniform bump bonds across large area wafers or dies. This template approach affords bumps with tunable diameters from 100s of nanometers to microns (allowing for tunable interconnect pitch and via diameters) while the use of constant current electoplating gives uniform bump height over large areas (>1 cm2).

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Ultralow power silicon microdisk modulators and switches

2008 5th International Conference on Group IV Photonics, GFP

Watts, Michael W.; Trotter, Douglas C.; Young, Ralph W.; Lentine, Anthony L.

We demonstrate a 4μm silicon microdisk modulator with a power consumption of 85fJ/bit. The modulator utilizes a reverse-biased. vertical p-n junction to achieve 10Gb/s data transmission, with 3.5V drive voltage, BER<10-12, and without signal pre-emphasis. High-speed silicon bandpass switches are constructed from pairs of modulators. © 2008 IEEE Institute of Electrical and Electronics Engineers.

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A molecular dynamics study of alkaline earth metal-chloride complexation in aqueous solution

Journal of Physical Chemistry B

Larentzos, James P.; Criscenti, Louise J.

The relative stability of alkaline earth metals (M2+ = Mg 2+, Ca2+, Sr2+, and Ba2+) and their chloride complexes in aqueous solution is examined through molecular dynamics simulations using a flexible SPC water model with an internally consistent set of metal ion force field parameters. For each metal-chloride ion pair in aqueous solution, the free energy profile was calculated via potential of mean force simulations. The simulations provide detailed thermodynamic information regarding the relative stability of the different types of metal-chloride pairs. The free energy profiles indicate that the preference for contact ion pair formation increases with ionic radius and is closely related to the metal hydration free energies. The water residence times within the first hydration shells are in agreement with residence times reported in other computational studies. Calculated association constants suggest an increase in metal-chloride complexation with increasing cation radii that is inconsistent with experimentally observed trends. Possible explanations for this discrepancy are discussed. © 2008 American Chemical Society.

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Design, fabrication, and characterization of metal micromachined rectangular waveguides at 3 THz

2008 IEEE International Symposium on Antennas and Propagation and USNC/URSI National Radio Science Meeting, APSURSI

Nordquist, Christopher D.; Wanke, Michael W.; Rowen, Adam M.; Arrington, Christian L.; Lee, Mark L.; Grine, Albert D.

Single-mode 75 μm × 37 μm rectangular waveguide components, including horn antennas, couplers, and bends, for operation at 3 THz have been designed and fabricated using thick gold micromachining. THz transmission through these waveguides has been quasi-optically measured at 2.92 THz. This technology offers the potential for realizing miniature integrated systems operating in the 3 THz frequency range. © 2008 IEEE.

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VHF and UHF mechanically coupled aluminum nitride MEMS filters

2008 IEEE International Frequency Control Symposium, FCS

Olsson, Roy H.; Washburn, Cody M.; Stevens, James E.; Tuck, Melanie R.; Nordquist, Christopher N.

This paper reports the development of narrow-bandwidth, post-CMOS compatible aluminum nitride (AlN) MEMS filters operating in the very (VHF) and ultra (UHF) high frequency bands. Percent bandwidths less than 0.1% are achieved utilizing a mechanically coupled filter architecture, where a quarter wavelength beam attached in low velocity coupling locations is used to connect two AlN ring resonators. The filter bandwidth has been successfully varied from 0.09% to 0.2% by moving the attachment of the coupling beam on the ring to locations with different velocity at resonance. Insertion losses of 11 dB are obtained for filters centered at 99.5 MHz with low termination impedances of 200 &Omega. Utilizing a passive temperature compensation technique, the temperature coefficient of frequency (TCF) for these filters has been reduced from -21 ppm/C to 2.5 ppm/C. The reduced TCF is critical for narrow bandwidth filters, requiring only 13% of the filter bandwidth to account for military range (-55 to 125 C) temperature variations compared to 100% for uncompensated filters. Filters operating at 557 MHz are realized using overtone operation of the ring resonators and coupling beam where higher insertion losses of 32 dB into 50 ω are seen due to the finite resonator quality factor and narrow bandwidth design. Overtone operation allows for the implementation of fully differential and balun type filters where the stop-band rejection is as high as 38 dB despite the increased Insertion loss. © 2008 IEEE.

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Characterization and modeling of a bulk acoustic wave particle focusing device

2008 IEEE International Frequency Control Symposium, FCS

Ravula, Surendra K.; Branch, Darren W.; Westlake, Karl W.; Brener, Igal B.

In this paper, we discuss our work in the modeling and characterization of an acousdc-microfluidlc focusing device that uses standing bulk acoustic waves to focus particles under flow. Modeling was done using Comsol Multiphysics® (Comsol, Los Angeles, CA), a multiphysics FEM tool, and the performance of the device was assessed through coefficient of variance (CV) measurements using a confocal microscope. © 2008 IEEE.

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VHF and UHF mechanically coupled aluminum nitride MEMS filters

2008 IEEE International Frequency Control Symposium, FCS

Olsson, Roy H.; Washburn, Cody M.; Stevens, James E.; Tuck, Melanie R.; Nordquist, Christopher N.

This paper reports the development of narrow-bandwidth, post-CMOS compatible aluminum nitride (AlN) MEMS filters operating in the very (VHF) and ultra (UHF) high frequency bands. Percent bandwidths less than 0.1% are achieved utilizing a mechanically coupled filter architecture, where a quarter wavelength beam attached in low velocity coupling locations is used to connect two AlN ring resonators. The filter bandwidth has been successfully varied from 0.09% to 0.2% by moving the attachment of the coupling beam on the ring to locations with different velocity at resonance. Insertion losses of 11 dB are obtained for filters centered at 99.5 MHz with low termination impedances of 200 &Omega. Utilizing a passive temperature compensation technique, the temperature coefficient of frequency (TCF) for these filters has been reduced from -21 ppm/C to 2.5 ppm/C. The reduced TCF is critical for narrow bandwidth filters, requiring only 13% of the filter bandwidth to account for military range (-55 to 125 C) temperature variations compared to 100% for uncompensated filters. Filters operating at 557 MHz are realized using overtone operation of the ring resonators and coupling beam where higher insertion losses of 32 dB into 50 ω are seen due to the finite resonator quality factor and narrow bandwidth design. Overtone operation allows for the implementation of fully differential and balun type filters where the stop-band rejection is as high as 38 dB despite the increased Insertion loss. © 2008 IEEE.

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Fiber-optic current sensors based on polarization coherence and power scattering in magneto-optical films

Proceedings of SPIE - The International Society for Optical Engineering

Hsu, Alan Y.; Robinson, Alex L.; Cernosek, R.W.

Fiber-optic sensors for sensing electrical current are attractive due to their inherent immunity to electromagnetic interference. Several groups have shown the use of Faraday rotation in magneto-optical materials as a function of current-induced magnetic field. In this work, fiber-optic sensors based on different mechanisms such as magnetic-fielddependent polarization coherence and power scattering effects in magneto-optical materials are demonstrated. These novel sensor configurations can have advantages in that they exhibit power-independent or polarization-independent operation which can ultimately lead to fewer components and relaxed light source requirements compared to fiber-optic current sensor systems based on Faraday rotation.

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Variable-angle directional emissometer for moderate-temperature emissivity measurements

Proceedings of SPIE - The International Society for Optical Engineering

Ellis, A.R.; Graham, H.M.; Sinclair, Michael B.; Verley, Jason V.

We have developed a system to measure the directional thermal emission from a surface, and in turn, calculate its emissivity. This approach avoids inaccuracies sometimes encountered with the traditional method for calculating emissivity, which relies upon subtracting the measured total reflectivity and total transmissivity from unity. Typical total reflectivity measurements suffer from an inability to detect backscattered light, and may not be accurate for high angles of incidence. Our design allows us to vary the measurement angle (θ) from near-normal to ∼80°, and can accommodate samples as small as 7 mm on a side by controlling the sample interrogation area. The sample mount is open-backed to eliminate shine-through, can be heated up to 200°C, and is kept under vacuum to avoid oxidizing the sample. A cold shield reduces the background noise and stray signals reflected off the sample. We describe the strengths, weaknesses, trade-offs, and limitations of our system design, data analysis methods, the measurement process, and present the results of our validation of this Variable-Angle Directional Emissometer.

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Temperature and dose-rate effects in gamma irradiated rare-earth doped fibers

Proceedings of SPIE - The International Society for Optical Engineering

Fox, B.P.; Simmons-Potter, K.; Thomes, W.J.; Meister, Dorothy C.; Bambha, R.P.; Kliner, D.A.V.

Rare-earth-doped fibers, such as Er3+- and Yb3+-doped aluminosilicates can be advantageous in space-based systems due to their stability, their high-bandwidth transmission properties and their lightweight, small-volume properties. In such environments the effect of ionizing-radiation on the optical transmission of these fibers is of paramount importance. For the present work, gamma-radiation experiments were conducted in which un-pumped Yb3+ and Er3+ doped sample fibers were irradiated with a Cobalt-60 source under different dose-rate and temperature conditions. In-situ spectral transmittance data over the near IR was monitored during the irradiations for total doses of up to tens of krad (Si). It was found that there was a dose-rate dependence in which higher rates resulted in more photodarkening. Higher temperatures were not found to significantly affect the rate of photodarkening at the dose rates used.

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IR spectrometer using 90-degree off-axis parabolic mirrors

Proceedings of SPIE - The International Society for Optical Engineering

Malone, Robert M.; Dolan, Daniel H.; Hacking, Richard G.; McKenna, Ian J.

A gated spectrometer has been designed for real-time, pulsed infrared (IR) studies at the National Synchrotron Light Source at the Brookhaven National Laboratory. A pair of 90-degree, off-axis parabolic mirrors are used to relay the light from an entrance slit to an output IR recording camera. With an initial wavelength range of 1500-4500 nm required, gratings could not be used in the spectrometer because grating orders would overlap. A magnesium oxide prism, placed between these parabolic mirrors, serves as the dispersion element. The spectrometer is doubly telecentric. With proper choice of the air spacing between the prism and the second parabolic mirror, any spectral region of interest within the InSb camera array's sensitivity region can be recorded. The wavelengths leaving the second parabolic mirror are collimated, thereby relaxing the camera positioning tolerance. To set up the instrument, two different wavelength (visible) lasers are introduced at the entrance slit and made collinear with the optical axis via flip mirrors. After dispersion by the prism, these two laser beams are directed to tick marks located on the outside housing of the gated IR camera. This provides first-order wavelength calibration for the instrument. Light that is reflected off the front prism face is coupled into a high-speed detector to verify steady radiance during the gated spectral imaging. Alignment features include tick marks on the prism and parabolic mirrors. This instrument was designed to complement singlepoint pyrometry, which provides continuous time histories of a small collection of spots from shock-heated targets.

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Waste package corrosion studies using small mockup experiments

Materials Research Society Symposium Proceedings

Anderson, B.E.; Helean, Katheryn B.; Bryan, Charles R.; Brady, Patrick V.; Ewing, R.C.

Understanding the corrosion of spent nuclear fuel (SNF) and the subsequent mobilization of released radionuclides, particularly under oxidizing conditions, is one of the key issues in evaluating the long-term performance of a nuclear waste repository. However, the large amounts of iron in the metal waste package may create locally reducing conditions that would lower corrosion rates for the SNF, as well as reduce the solubility of some key radionuclides, e.g., Tc and Np. In order to investigate the interactions among SNF-waste package-fluids, four smallscale (∼1:40 by length) waste package mockups were constructed using metals similar to those proposed for use in waste packages at the proposed repository at Yucca Mountain. Each mockup experiment differed with respect to water input, exposure to the atmosphere, and temperature. Simulated Yucca Mountain process water (YMPW) was injected into three of the mockups at a rate of 200 μL per day for five days a week using a calibrated needle syringe. The YMPW was prepared by equilibrating 50 mg/L silica as sodium metasilicate with air, and adding enough HC1 to lower the pH to 7.6 in contact with an excess of powdered calcite. X-ray powder diffraction and scanning electron microscopy confirm that, where corrosion occurred, the dominant corrosion product in all cases was magnetite. In the high temperature (60°C) experiment, hematite and a fibrous, Fe-O-Cl phase were also identified. The Fe(II)/Fe(III) ratios measured in the corrosion products using a wet chemistry technique indicate extremely low oxygen fugacities (10-36 bar). Experiments are in progress in which 0.1g powdered UO2 was included in the mock-up in order to investigate the relative kinetics of Fe and U oxidation and to identify the U corrosion products formed under these conditions. © 2008 Materials Research Society.

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X-ray diagnostics of imploding plasmas from planar wire arrays composed of Cu and few tracer Al wires on the 1MA pulsed power generator at UNR

Review of Scientific Instruments

Safronova, A.S.; Kantsyrev, V.L.; Esaulov, A.A.; Ouart, N.D.; Yilmaz, M.F.; Williamson, K.M.; Shlyaptseva, V.; Shrestha, I.; Osborne, G.C.; Coverdale, Christine A.; Jones, Brent M.; Deeney, C.

Tracer aluminum alloyed wires (Al5056) are used to provide additional information for x-ray diagnostics of implosions of Cu planar wire arrays (PWAs). Specifically, the analysis of combined PWA experiments using the extensive set of x-ray diagnostics is presented. In these experiments, which were conducted at the 1MA pulsed power generator at University of Nevada, Reno, the Z-pinch load consisted of several (eight) Cu alloyed (main material) and one to two Al alloyed (tracer) wires mounted in a single plane row or double parallel plane rows, single planar wire array (SPWA) or double planar wire array (DPWA), respectively. The analysis of x-ray spatially resolved spectra from the main material indicates the increase in the electron temperature Te near the cathode. In general, the axial gradients in Te are more pronounced for SPWA than for DPWA due to the more "columnlike" plasma formation for SPWA compared to "hot-spot-like" plasma formation for DPWA. In addition, x-ray spectra from tracer wires are studied, and estimated plasma parameters are compared with those from the main material. It is observed that the x-ray K -shell Al spectra manifest more opacity features for the case of SPWA with about 18% of Al mass (to the total load mass) compared to the case of DPWA with about 11% of Al mass. The analysis of time-gated spectra shows that the relative intensity of the most intense K -shell Al line, small before the x-ray burst, increases with time and peaks close to the maximum of the sub-keV signal. © 2008 American Institute of Physics.

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Scenario discovery using nonnegative tensor factorization

Lecture Notes in Computer Science (including subseries Lecture Notes in Artificial Intelligence and Lecture Notes in Bioinformatics)

Bader, Brett W.; Puretskiy, Andrey A.; Berry, Michael W.

In the relatively new field of visual analytics there is a great need for automated approaches to both verify and discover the intentions and schemes of primary actors through time. Data mining and knowledge discovery play critical roles in facilitating the ability to extract meaningful information from large and complex textual-based (digital) collections. In this study, we develop a mathematical strategy based on nonnegative tensor factorization (NTF) to extract and sequence important activities and specific events from sources such as news articles. The ability to automatically reconstruct a plot or confirm involvement in a questionable activity is greatly facilitated by our approach. As a variant of the PARAFAC multidimensional data model, we apply our NTF algorithm to the terrorism-based scenarios of the VAST 2007 Contest data set to demonstrate how term-by-entity associations can be used for scenario/plot discovery and evaluation. © 2008 Springer-Verlag Berlin Heidelberg.

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CMOS Integrated single electron transistor electrometry (CMOS-SET) circuit design for nanosecond quantum-bit read-out

2008 8th IEEE Conference on Nanotechnology, IEEE-NANO

Gurrieri, Thomas G.; Carroll, Malcolm; Lilly, Michael L.; Levy, James E.

Novel single electron transistor (SET) read-out circuit designs are described. The circuits use a silicon SET interfaced to a CMOS voltage mode or current mode comparator to obtain a digital read-out of the state of the qubit. The design assumes standard submicron (0.35um) CMOS SOI technology using room temperature SPICE models. Implications and uncertainties related to the temperature scaling of these models to 100mK operation are discussed. Using this technology, the simulations predict a read-out operation speed of approximately 1ns and a power dissipation per cell as low as 2nW for single-shot read-out, which is a significant advantage over currently used radio frequency SET (RF-SET) approaches. © 2008 IEEE.

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Inexact newton dogleg methods

SIAM Journal on Numerical Analysis

Pawlowski, Roger P.; Simonis, Joseph P.; Walker, Homer F.; Shadid, John N.

The dogleg method is a classical trust-region technique for globalizing Newton's method. While it is widely used in optimization, including large-scale optimization via truncated-Newton approaches, its implementation in general inexact Newton methods for systems of nonlinear equations can be problematic. In this paper, we first outline a very general dogleg method suitable for the general inexact Newton context and provide a global convergence analysis for it. We then discuss certain issues that may arise with the standard dogleg implementational strategy and propose modified strategies that address them. Newton-Krylov methods have provided important motivation for this work, and we conclude with a report on numerical experiments involving a Newton-GMRES dogleg method applied to benchmark CFD problems. © 2008 Society for Industrial and Applied Mathematics.

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Solving elliptic finite element systems in near-linear time with support preconditioners

SIAM Journal on Numerical Analysis

Boman, Erik G.; Hendrickson, Bruce A.; Vavasis, Stephen

We consider linear systems arising from the use of the finite element method for solving scalar linear elliptic problems. Our main result is that these linear systems, which are symmetric and positive semidefinite, are well approximated by symmetric diagonally dominant matrices. Our framework for defining matrix approximation is support theory. Significant graph theoretic work has already been developed in the support framework for preconditioners in the diagonally dominant case, and, in particular, it is known that such systems can be solved with iterative methods in nearly linear time. Thus, our approximation result implies that these graph theoretic techniques can also solve a class of finite element problems in nearly linear time. We show that the support number bounds, which control the number of iterations in the preconditioned iterative solver, depend on mesh quality measures but not on the problem size or shape of the domain. © 2008 Society for Industrial and Applied Mathematics.

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Multispace and multilevel BDDC

Computing (Vienna/New York)

Mandel, Jan; Sousedík, Bedřich; Dohrmann, Clark R.

The Balancing Domain Decomposition by Constraints (BDDC) method is the most advanced method from the Balancing family of iterative substructuring methods for the solution of large systems of linear algebraic equations arising from discretization of elliptic boundary value problems. In the case of many substructures, solving the coarse problem exactly becomes a bottleneck. Since the coarse problem in BDDC has the same structure as the original problem, it is straightforward to apply the BDDC method recursively to solve the coarse problem only approximately. In this paper, we formulate a new family of abstract Multispace BDDC methods and give condition number bounds from the abstract additive Schwarz preconditioning theory. The Multilevel BDDC is then treated as a special case of the Multispace BDDC and abstract multilevel condition number bounds are given. The abstract bounds yield polylogarithmic condition number bounds for an arbitrary fixed number of levels and scalar elliptic problems discretized by finite elements in two and three spatial dimensions. Numerical experiments confirm the theory. © 2008 Springer-Verlag.

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Model validation of a complex aerospace structure

Sound and Vibration

Rice, Amy E.; Carne, Thomas G.; Kelton, David W.

A series of modal tests were performed to validate a finite-element model of a complex aerospace structure. Data were measured using various excitation methods to extract clean modes and damping values for a lightly damped system. Model validation was performed for one subassembly as well as for the full assembly to pinpoint the areas of the model that required updating and to better ascertain the quality of the joint models connecting the various components and subassemblies. After model updates were completed using the measured modal data, the model was validated using frequency response functions (FRFs) as the independent validation metric. Test and model FRFs were compared to determine the validity of the finite-element model.

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An argument for proof testing brittle microsystems in high-reliability applications

Journal of Micromechanics and Microengineering

Boyce, B.L.; Ballarini, R.; Chasiotis, I.

The vast majority of microelectromechanical systems (MEMS) for sensor and actuator applications are fabricated from brittle materials, such as Si, SiC and diamond. Numerous prior studies have shown that the structural reliability of these flaw-intolerant materials is governed by processing-induced critical defects, and that their failure strengths have a wide dispersion associated with a low Weibull modulus. This broad distribution of critical failure conditions creates an uncertainty that cannot be tolerated in high-risk or high-consequence applications. This note presents arguments for the adoption of proof testing methodologies which will provide a statistically-sound basis for certifying MEMS component reliability. © 2008 IOP Publishing Ltd.

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Quantitative chemical analysis of fluorite-to-perovskite transformations in (Pb,La) (Zr,Ti)O3 PLZT thin films

Journal of Materials Research

Parish, Chad M.; Brennecka, Geoffrey L.; Tuttle, Bruce T.; Brewer, Luke N.

Lead loss during processing of solution-derived Pb(Zr,Ti)O3 (PZT)-based thin-films can result in the formation of a Pb-deficient, nonferroelectric fluorite phase that is detrimental to dielectric properties. It has recently been shown that this nonferroelectric fluorite phase can be converted to the desired perovskite phase by postcrystallization treatment. Here, quantitative standard-based energy-dispersive x-ray spectrometry (EDS) in a scanning transmission electron microscope (STEM) is used to study cation distribution before and after this fluorite-to-perovskite transformation. Single-phase perovskite PbZr0.53 Ti0.47O3 (PZT 53 /47) and Pb0.88 La0.12 Zr0.68 Ti0.29O3 (PLZT 12/70/30) specimens that underwent this treatment were found to be chemically indistinguishable from the perovskite present in the multiphase specimens prior to the fluorite-to-perovskite transformation. Significant Zr-Ti segregation is found in PLZT 12/70/30, but not in PZT 53/47. Slight La-segregation was seen in rapidly crystallized PLZT, but not in more slowly crystallized PLZT.

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Quantitative X-Ray spectrum imaging of lead lanthanum zirconate titanate PLZT thin-films

Journal of the American Ceramic Society

Parish, Chad M.; Brennecka, Geoffrey L.; Tuttle, Bruce T.; Brewer, Luke N.

The high permittivity of Pb(Zr,Ti)O3 and (Pb,La)(Zr,Ti)O 3 - PZT and PLZT, respectively - thin films and the flexibility of chemical solution deposition (CSD) make solution-derived P(L)ZT thin films extremely attractive for integrated capacitor applications. However, Pb-loss or cation segregation during processing results in degraded properties of the final film. Here, we have extended the use of multivariate statistical analysis (MSA) of energy-dispersive spectroscopy (EDS) spectrum images (SIs) in scanning transmission electron microscopy (STEM) to allow the two-dimensional (2D) quantitative analysis of cation segregation and depletion in P(L)ZT thin films. Quantified STEM-EDS SIs allow high-resolution (< ≈10 nm) quantification of these cation distributions. Surface Pb depletion is found after crystallization and is replenished by a unique post-crystallization PbO overcoat+anneal processes. Zr/Ti and La segregation are found to develop in a decidedly nonplanar fashion during crystallization, especially in PLZT 12/70/30 material, highlighting the need for 2D analysis. Quantitative 2D chemical information is essential for improved processing of homogeneous P(L)ZT films with optimal electrical properties. © 2008 Sandia Corporation. Journal compilation © 2008 The American Ceramic Society.

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Doppler electron velocimetry : notes on creating a practical tool

Reu, Phillip L.

The Doppler electron velocimeter (DEV) has been shown to be theoretically possible. This report attempts to answer the next logical question: Is it a practical instrument? The answer hinges upon whether enough electrons are available to create a time-varying Doppler current to be measured by a detector with enough sensitivity and bandwidth. The answer to both of these questions is a qualified yes. A target Doppler frequency of 1 MHz was set as a minimum rate of interest. At this target a theoretical beam current signal-to-noise ratio of 25-to-1 is shown for existing electron holography equipment. A detector is also demonstrated with a bandwidth of 1-MHz at a current of 10 pA. Additionally, a Linnik-type interferometer that would increase the available beam current is shown that would offer a more flexible arrangement for Doppler electron measurements over the traditional biprism.

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The Arctic as a test case for an assessment of climate impacts on national security

Boslough, Mark B.; Taylor, Mark A.; Zak, Bernard D.; Backus, George A.

The Arctic region is rapidly changing in a way that will affect the rest of the world. Parts of Alaska, western Canada, and Siberia are currently warming at twice the global rate. This warming trend is accelerating permafrost deterioration, coastal erosion, snow and ice loss, and other changes that are a direct consequence of climate change. Climatologists have long understood that changes in the Arctic would be faster and more intense than elsewhere on the planet, but the degree and speed of the changes were underestimated compared to recent observations. Policy makers have not yet had time to examine the latest evidence or appreciate the nature of the consequences. Thus, the abruptness and severity of an unfolding Arctic climate crisis has not been incorporated into long-range planning. The purpose of this report is to briefly review the physical basis for global climate change and Arctic amplification, summarize the ongoing observations, discuss the potential consequences, explain the need for an objective risk assessment, develop scenarios for future change, review existing modeling capabilities and the need for better regional models, and finally to make recommendations for Sandia's future role in preparing our leaders to deal with impacts of Arctic climate change on national security. Accurate and credible regional-scale climate models are still several years in the future, and those models are essential for estimating climate impacts around the globe. This study demonstrates how a scenario-based method may be used to give insights into climate impacts on a regional scale and possible mitigation. Because of our experience in the Arctic and widespread recognition of the Arctic's importance in the Earth climate system we chose the Arctic as a test case for an assessment of climate impacts on national security. Sandia can make a swift and significant contribution by applying modeling and simulation tools with internal collaborations as well as with outside organizations. Because changes in the Arctic environment are happening so rapidly, a successful program will be one that can adapt very quickly to new information as it becomes available, and can provide decision makers with projections on the 1-5 year time scale over which the most disruptive, high-consequence changes are likely to occur. The greatest short-term impact would be to initiate exploratory simulations to discover new emergent and robust phenomena associated with one or more of the following changing systems: Arctic hydrological cycle, sea ice extent, ocean and atmospheric circulation, permafrost deterioration, carbon mobilization, Greenland ice sheet stability, and coastal erosion. Sandia can also contribute to new technology solutions for improved observations in the Arctic, which is currently a data-sparse region. Sensitivity analyses have the potential to identify thresholds which would enable the collaborative development of 'early warning' sensor systems to seek predicted phenomena that might be precursory to major, high-consequence changes. Much of this work will require improved regional climate models and advanced computing capabilities. Socio-economic modeling tools can help define human and national security consequences. Formal uncertainty quantification must be an integral part of any results that emerge from this work.

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Medically relevant ElectroNeedle technology development

Achyuthan, Komandoor A.; Harper, Jason C.; McClain, Jaime L.; Ten Eyck, Gregory A.; Thomas, Michael L.

ElectroNeedles technology was developed as part of an earlier Grand Challenge effort on Bio-Micro Fuel Cell project. During this earlier work, the fabrication of the ElectroNeedles was accomplished along with proof-of-concept work on several electrochemically active analytes such as glucose, quinone and ferricyanide. Additionally, earlier work demonstrated technology potential in the field of immunosensors by specifically detecting Troponin, a cardiac biomarker. The current work focused upon fabrication process reproducibility of the ElectroNeedles and then using the devices to sensitively detect p-cresol, a biomarker for kidney failure or nephrotoxicity. Valuable lessons were learned regarding fabrication assurance and quality. The detection of p-cresol was accomplished by electrochemistry as well as using fluorescence to benchmark ElectroNeedles performance. Results from these studies will serve as a guide for the future fabrication processes involving ElectroNeedles as well as provide the groundwork necessary to expand technology applications. One paper has been accepted for publication acknowledging LDRD funding (K. E. Achyuthan et al, Comb. Chem. & HTS, 2008). We are exploring the scope for a second paper describing the applications potential of this technology.

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The Sandia MEMS passive shock sensor : FY08 design summary

Wittwer, Jonathan W.; Baker, Michael S.; Mitchell, John A.; Epp, David E.; Clemens, Rebecca C.; Brake, Matthew R.; Walraven, J.A.

This report summarizes design and modeling activities for the MEMS passive shock sensor. It provides a description of past design revisions, including the purposes and major differences between design revisions but with a focus on Revisions 4 through 7 and the work performed in fiscal year 2008 (FY08). This report is a reference for comparing different designs; it summarizes design parameters and analysis results, and identifies test structures. It also highlights some of the changes and or additions to models previously documented [Mitchell et al. 2006, Mitchell et al. 2008] such as the way uncertainty thresholds are analyzed and reported. It also includes dynamic simulation results used to investigate how positioning of hard stops may reduce vibration sensitivity.

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In vivo collection of rare proteins using kinesin-based "nano-harvesters"

Bachand, George B.; Greene, Adrienne C.

In this project, we have developed a novel platform for capturing, transport, and separating target analytes using the work harnessed from biomolecular transport systems. Nanoharvesters were constructed by co-organizing kinesin motor proteins and antibodies on a nanocrystal quantum dot (nQD) scaffold. Attachment of kinesin and antibodies to the nQD was achieved through biotin-streptavidin non-covalent bonds. Assembly of the nanoharvesters was characterized using a modified enzyme-linked immunosorbent assay (ELISA) that confirmed attachment of both proteins. Nanoharvesters selective against tumor necrosis factor-{alpha} (TNF-{alpha}) and nuclear transcription factor-{kappa}B (NF-{kappa}B) were capable of detecting target antigens at <100 ng/mL in ELISAs. A motility-based assay was subsequently developed using an antibody-sandwich approach in which the target antigen (TNF-{alpha}) formed a sandwich with the red-emitting nanoharvester and green-emitting detection nQD. In this format, successful sandwich formation resulted in a yellow emission associated with surface-bound microtubules. Step-wise analysis of sandwich formation suggested that the motility function of the kinesin motors was not adversely affected by either antigen capture or the subsequent binding of the detection nQDs. TNF-{alpha} was detected as low as {approx}1.5 ng/mL TNF-{alpha}, with 5.2% of the nanoharvesters successfully capturing the target analyte and detection nQDs. Overall, these results demonstrate the ability to capture target protein analytes in vitro using the kinesin-based nanoharvesters in nanofluidic environments. This system has direct relevance for lab-on-a-chip applications where pressure-driven or electrokinetic movement of fluids is impractical, and offers potential application for in vivo capture of rare proteins within the cytoplasmic domain of live cells.

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Preliminary systems engineering evaluations for the National Ecological Observatory Network

Kottenstette, Richard K.; Heller, Edwin J.; Ivey, Mark D.; Brocato, Robert W.; Zak, Bernard D.; Zirzow, Jeffrey A.; Schubert, William K.; Crouch, Shannon M.; Dishman, James L.; Robertson, Perry J.; Osborn, Thor D.

The National Ecological Observatory Network (NEON) is an ambitious National Science Foundation sponsored project intended to accumulate and disseminate ecologically informative sensor data from sites among 20 distinct biomes found within the United States and Puerto Rico over a period of at least 30 years. These data are expected to provide valuable insights into the ecological impacts of climate change, land-use change, and invasive species in these various biomes, and thereby provide a scientific foundation for the decisions of future national, regional, and local policy makers. NEON's objectives are of substantial national and international importance, yet they must be achieved with limited resources. Sandia National Laboratories was therefore contracted to examine four areas of significant systems engineering concern; specifically, alternatives to commercial electrical utility power for remote operations, approaches to data acquisition and local data handling, protocols for secure long-distance data transmission, and processes and procedures for the introduction of new instruments and continuous improvement of the sensor network. The results of these preliminary systems engineering evaluations are presented, with a series of recommendations intended to optimize the efficiency and probability of long-term success for the NEON enterprise.

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Nanomechanical switch for integration with CMOS logic

Proposed for publication in the Journal of Microelectronics and Micromechanics.

Czaplewski, David A.; Patrizi, G.A.; Kraus, Garth K.; Wendt, J.R.; Nordquist, Christopher N.; Wolfley, Steven L.; De Boer, Maarten P.

We designed, fabricated and measured the performance of nanoelectromechanical (NEMS) switches. Initial data are reported with one of the switch designs having a measured switching time of 400 ns and an operating voltage of 5 V. The switches operated laterally with unmeasurable leakage current in the 'off' state. Surface micromachining techniques were used to fabricate the switches. All processing was CMOS compatible. A single metal layer, defined by a single mask step, was used as the mechanical switch layer. The details of the modeling, fabrication and testing of the NEMS switches are reported.

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Problems encountered in fluctuating flame temperature measurements by thermocouple

Proposed for publication in Sensors.

Gill, Walt; Donaldson, Arlie B.

Some thermocouple experiments were carried out in order to obtain sensitivity of thermocouple readings to fluctuations in flames and to determine if the average thermocouple reading was representative of the local volume temperature for fluctuating flames. The thermocouples considered were an exposed junction thermocouple and a fully sheathed thermocouple with comparable time constants. Either the voltage signal or indicated temperature for each test was recorded at sampling rates between 300-4,096 Hz. The trace was then plotted with respect to time or sample number so that time variation in voltage or temperature could be visualized and the average indicated temperature could be determined. For experiments where high sampling rates were used, the signal was analyzed using Fast Fourier Transforms (FFT) to determine the frequencies present in the thermocouple signal. This provided a basic observable as to whether or not the probe was able to follow flame oscillations. To enhance oscillations, for some experiments, the flame was forced. An analysis based on thermocouple time constant, coupled with the transfer function for a sinusoidal input was tested against the experimental results.

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Molecular models and simulations of layered materials

Proposed for publication in the Journal of Materials Chemistry.

Greathouse, Jeffery A.; Cygan, Randall T.

The micro- to nano-sized nature of layered materials, particularly characteristic of naturally occurring clay minerals, limits our ability to fully interrogate their atomic dispositions and crystal structures. The low symmetry, multicomponent compositions, defects, and disorder phenomena of clays and related phases necessitate the use of molecular models and modern simulation methods. Computational chemistry tools based on classical force fields and quantum-chemical methods of electronic structure calculations provide a practical approach to evaluate structure and dynamics of the materials on an atomic scale. Combined with classical energy minimization, molecular dynamics, and Monte Carlo techniques, quantum methods provide accurate models of layered materials such as clay minerals, layered double hydroxides, and clay-polymer nanocomposites.

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Safety analysis of high pressure 3He-filled micro-channels for thermal neutron detection

Renzi, Ronald F.; Ferko, Scott M.; Galambos, Paul; Derzon, Mark S.

This document is a safety analysis of a novel neutron detection technology developed by Sandia National Laboratories. This technology is comprised of devices with tiny channels containing high pressure {sup 3}He. These devices are further integrated into large scale neutron sensors. Modeling and preliminary device testing indicates that the time required to detect the presence of special nuclear materials may be reduced under optimal conditions by several orders of magnitude using this approach. Also, these devices make efficient use of our {sup 3}He supply by making individual devices more efficient and/or extending the our limited {sup 3}He supply. The safety of these high pressure devices has been a primary concern. We address these safety concerns for a flat panel configuration intended for thermal neutron detection. Ballistic impact tests using 3 g projectiles were performed on devices made from FR4, Silicon, and Parmax materials. In addition to impact testing, operational limits were determined by pressurizing the devices either to failure or until they unacceptably leaked. We found that (1) sympathetic or parasitic failure does not occur in pressurized FR4 devices (2) the Si devices exhibited benign brittle failure (sympathetic failure under pressure was not tested) and (3) the Parmax devices failed unacceptably. FR4 devices were filled to pressures up to 4000 + 100 psig, and the impacts were captured using a high speed camera. The brittle Si devices shattered, but were completely contained when wrapped in thin tape, while the ductile FR4 devices deformed only. Even at 4000 psi the energy density of the compressed gas appears to be insignificant compared to the impact caused by the incoming projectile. In conclusion, the current FR4 device design pressurized up to 4000 psi does not show evidence of sympathetic failure, and these devices are intrinsically safe.

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Radioluminescence and scintillation results of horizontal gradient freeze grown aliovalently-doped CeBr3

Proposed for publication in IEEE Transactions on Nuclear Science.

Doty, Fred P.

Strengthening the crystal lattice of lanthanide halides, which are brittle, anisotropic, ionic crystals, may prove to increase the availability and ruggedness of these scintillators for room-temperature gamma-ray spectroscopy applications. Eight aliovalent dopants for CeBr{sub 3} were explored in an effort to find the optimal aliovalent strengthening agent. Eight dopants, CaBr{sub 2}, SrBr{sub 2}, BaBr{sub 2}, ZrBr{sub 4}, HfBr{sub 4}, ZnBr{sub 2}, CdBr[sub 2}, and PbBr{sub 2}, were explored at two levels of doping, 500 and 1000 ppm. From each ingot, samples were harvested for radioluminescence spectrum measurement and scintillation testing. Of the eight dopants explored, only BaBr{sub 2} and PbBr{sub 2} were found to clearly decrease total light yield. ZnBr{sub 2} and CdBr{sub 2} dopants both affected the radioluminescence emission spectrum very little as compared to undoped CeBr{sub 3}. HfBr{sub 2}- and ZnBr{sub 4}-doped CeBr{sub 3} exhibited the highest light yields.

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Treatment of acoustic fluid-structure interaction by Localized Lagrange Multipliers and comparison to alternative interface coupling methods

Computer Methods in Applied Mechanics and Engineering

This paper is a sequel on the topic of localized Lagrange multipliers (LLM) for applications of fluid-structure interaction (FSI) between finite-element models of an acoustic fluid and an elastic structure. The prequel paper formulated the spatial-discretization methods, the LLM interface treatment, the time-marching partitioned analysis procedures, and the application to 1D benchmark problems. Here, we expand on formulation aspects required for successful application to more realistic 2D and 3D problems. Additional topics include duality relations at the fluid-structure interface, partitioned vibration analysis, reduced-order modeling, handling of curved interface surfaces, and comparison of LLM with other coupling methods. Emphasis is given to non-matching fluid-structure meshes. We present benchmark examples that illustrate the benefits and drawbacks of competing interface treatments. Realistic application problems involving the seismic response of two existing dams are considered. These include 2D modal analyses of the Koyna gravity dam, transient-response analyses of that dam with and without reduced-order modeling, incorporation of nonlinear cavitation effects, and the 3D transient-response analysis of the Morrow Point arch dam.

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Predicting the lifetime of fluorosilicone O-rings

Proposed for publication in Polymer Degradation and Stability.

Long-term (up to 1000 days) accelerated oven-aging studies on a commercial fluorosilicone o-ring seal are used to predict the sealing lifetime at room temperature (23 C). The study follows force decay (relaxation) on squeezed o-ring material using isothermal compression stress relaxation (CSR) techniques. The relaxation is normally a complex mix of reversible physical effects and non-reversible chemical effects but we utilize an over-strain approach to quickly achieve physical equilibrium. This allows us to concentrate the measurements on the chemical relaxation effects of primary interest to lifetime assessment. The long-term studies allow us to access a fairly broad temperature range (80-138 C) which results in improved modeling of the temperature dependence of the accelerated data. Non-Arrhenius behavior is observed with evidence of a significant lowering of the activation energy at the lowest accelerated aging temperature (80 C). This observation is consistent with numerous recent accelerated aging studies that probed temperature ranges large enough to observe similar non-Arrhenius behavior. The extrapolated predictions imply that significant loss of sealing force requires on the order of 50-100 years at 23 C. Field aging results out to 25 years at 23 C are shown to be in reasonable accord with the significant change in Arrhenius slope observed from the accelerated aging study.

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Shaping the output pulse of a linear-transformer-driver module

Proposed for publication in Physical Review Special Topics: Accelerators and Beams.

Stygar, William A.; Stoltzfus, Brian S.; Woodworth, Joseph R.; Fowler, William E.; LeChien, Keith R.; Long, Finis W.; Mazarakis, Michael G.; McKee, George R.; Mckenney, John M.; Savage, Mark E.

We demonstrate that a wide variety of current-pulse shapes can be generated using a linear-transformer-driver (LTD) module that drives an internal water-insulated transmission line. The shapes are produced by varying the timing and initial charge voltage of each of the module's cavities. The LTD-driven accelerator architecture outlined in [Phys. Rev. ST Accel. Beams 10, 030401 (2007)] provides additional pulse-shaping flexibility by allowing the modules that drive the accelerator to be triggered at different times. The module output pulses would be combined and symmetrized by water-insulated radial-transmission-line impedance transformers [Phys. Rev. ST Accel. Beams 11, 030401 (2008)].

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Report of tritide study at the Responsive Neutron Generator Product Deployment Center

Coffey, Jamie C.

This report documents a study of sample counting results for wipes from routine surface area monitoring conducted at the Responsive Neutron Generator Product Deployment Center (RNGPDC) at Sandia National Laboratories (SNL). The study was initiated in November 2006, with two samples suspected of containing erbium tritide, after some samples were found to exhibit higher tritium counting rates upon recount at a later time. The main goal of the study was to determine whether the current practice of analyzing tritium wipe samples once, within a few days of sample collection, is adequate to accurately quantify the amount of tritium on the sample when tritides may be present. Recommendations are made toward routine recounting of vials suspected of containing particulate forms of tritium.

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Computational and experimental study of nanoporous membranes for water desalination and decontamination

Debusschere, Bert D.; Zendejas, Frank Z.; Adalsteinsson, Helgi A.; Tran, Huu T.; Najm, H.N.; Chinn, Douglas A.; Kent, Michael S.; Simmons, Blake S.

Fundamentals of ion transport in nanopores were studied through a joint experimental and computational effort. The study evaluated both nanoporous polymer membranes and track-etched nanoporous polycarbonate membranes. The track-etched membranes provide a geometrically well characterized platform, while the polymer membranes are more closely related to ion exchange systems currently deployed in RO and ED applications. The experimental effort explored transport properties of the different membrane materials. Poly(aniline) membranes showed that flux could be controlled by templating with molecules of defined size. Track-etched polycarbonate membranes were modified using oxygen plasma treatments, UV-ozone exposure, and UV-ozone with thermal grafting, providing an avenue to functionalized membranes, increased wettability, and improved surface characteristic lifetimes. The modeling effort resulted in a novel multiphysics multiscale simulation model for field-driven transport in nanopores. This model was applied to a parametric study of the effects of pore charge and field strength on ion transport and charge exclusion in a nanopore representative of a track-etched polycarbonate membrane. The goal of this research was to uncover the factors that control the flux of ions through a nanoporous material and to develop tools and capabilities for further studies. Continuation studies will build toward more specific applications, such as polymers with attached sulfonate groups, and complex modeling methods and geometries.

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Results 74601–74800 of 96,771
Results 74601–74800 of 96,771