Publications

Abstract not provided.

Marine energy generation technologies such as wave and tidal power have great potential in meeting the need for renewable energy in the years ahead. Yet, many challenges remain associated with marine-based systems because of the corrosive environment. Conventional materials like metals are subject to rapid corrosive breakdown, crippling the lifespan of structures in such environments. Fiber-reinforced polymer composites offer an appealing alternative in their strength and corrosion resistance, but can experience degradation of mechanical properties as a result of moisture absorption. An investigation is conducted to test the application of a technique for micromechanical analysis of composites, known as multicontinuum theory and demonstrated in past works, as a mechanism for predicting the effects of prolonged moisture absorption on the performance of fiber-reinforced composites. Experimental tensile tests are performed on composite coupons with and without prolonged exposure to a salt water solution to obtain stiffness and strength properties. Multicontinuum theory is applied in conjunction with micromechanical modeling to deduce the effects of moisture absorption on the behavior of constituent materials within the composites. The results are consistent with experimental observations when guided by known mechanisms and trends from previous studies, indicating multicontinuum theory as a potentially effective tool in predicting the long-term performance of composites in marine environments.

The final version of the above article was posted prematurely on 16 July 2021, owing to a technical error. The final, corrected version of record will be made fully available at a later date.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Knowing when, why, and how materials evolve, degrade, or fail in radiation environments is pivotal to a wide range of fields from semiconductor processing to advanced nuclear reactor design. A variety of methods, including optical and electron microscopy, mechanical testing, and thermal techniques, have been used in the past to successfully monitor the microstructural and property evolution of materials exposed to extreme radiation environments. Acoustic techniques have also been used in the past for this purpose, although most methodologies have not achieved widespread adoption. However, with an increasing desire to understand microstructure and property evolution in situ, acoustic methods provide a promising pathway to uncover information not accessible to more traditional characterization techniques. This work highlights how two different classes of acoustic techniques may be used to monitor material evolution during in situ ion beam irradiation. The passive listening technique of acoustic emission is demonstrated on two model systems, quartz and palladium, and shown to be a useful tool in identifying the onset of damage events such as microcracking. An active acoustic technique in the form of transient grating spectroscopy is used to indirectly monitor the formation of small defect clusters in copper irradiated with self-ions at high temperature through the evolution of surface acoustic wave speeds. Here, these studies together demonstrate the large potential for using acoustic techniques as in situ diagnostics. Such tools could be used to optimize ion beam processing techniques or identify modes and kinetics of materials degradation in extreme radiation environments.

Abstract not provided.

Abstract not provided.

The purpose of this ISRM Suggested Method is to introduce a guideline on determining deformation and failure characteristics of rocks subjected to true triaxial compression on different stress path. The true triaxial testing apparatus was reviewed by means of the function and engineering application. Some key techniques, such as stress and strain measurements, and reduction of end effect between specimen and metal platens, preventing metal platens interference, were stated and suggested in detail. Methodology of specimen processing, specimen shape, and testing procedure are characterized. There is an explanation of the experimental data processing on stress–strain curves, strength, and fracture mode.

Measuring the size and orientation of borehole breakouts is one of the primary methods for determining the orientation and magnitudes of the in situ stresses in the subsurface. To better understand the effects of anisotropy on borehole breakouts, experiments were conducted on Mancos Shale, a finely laminated mudrock. A novel testing configuration was developed to conduct borehole breakout experiments in a standard triaxial vessel and load frame. Samples were prepared at three different orientations and deformed under 6.9 to 20.7 MPa confining pressure. The results show a variation of peak strength and breakout geometry depending on the lamination orientation. Samples deformed parallel to laminations failed at a higher maximum compressive stress than samples deformed perpendicular to laminations, which were stronger than inclined samples. These relationships are quantified by a cosine-based failure envelope. Observed breakout shapes in perpendicular samples are V-shaped and symmetric around the borehole, which advance as a series of fractures of increasing size into the sidewalls. In inclined samples, fractures form along weaker laminations planes and grow in an en echelon pattern towards the axial stress direction. In parallel samples, long fractures grow from the wellbore towards the axial stress direction. The observed geometries highlight potential sources of error in calculating in situ stresses from borehole breakouts.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Following the ISRM Suggested Method on Failure Criteria, ‘A failure criterion for rocks based on true triaxial testing’ by Chang and Haimson (2012), we attempted to obtain experiment-based Nadai (1950) and Mogi (1971) failure criteria for the aforementioned four sandstones: TCDP (Oku et al. 2007), Coconino, Bentheim (Ma and Haimson 2016; Ma et al. 2017a), and Castlegate (Ingraham et al. 2013). Here, the current work extends beyond the scope of Chang and Haimson (2012), to compare σ1 at failure (i.e., σ_1,peak) from test data with predictions based on the experimentally generated Nadai and Mogi criteria. The applicability of Nadai and Mogi criteria to porous sandstones is then evaluated and discussed, considering failure mode evolution in these rocks.

Abstract not provided.

The state of stress in the earth is complicated and it is difficult to determine all three components and directions of the stress. However, the state of stress affects all activities which take place in the earth, from causing earthquakes on critically stressed faults, to affecting production from hydraulically fractured shale reservoirs, to determining closure rates around a subterranean nuclear waste repository. Current state of the art methods commonly have errors in magnitude and direction of up to 40%. This is especially true for the intermediate principal stress. This project seeks to better understand the means which are used to determine the state of stress in the earth and improve upon current methods to decrease the uncertainty in the measurement. This is achieved by a multipronged experimental investigation which is closely coupled with advanced constitutive and numeric modeling.

A critical component of the Underground Nuclear Explosion Signatures Experiment (UNESE) program is a realistic understanding of the post-detonation processes and changes in the environment that produce observable physical and radio-chemical signatures. Rock and fracture properties are essential parameters for any UNESE test bed. In response to the need for accurate modeling scenarios of these observations, an experimental program to determine the permeability and direct shear fracture properties of Barnwell core was developed. Room temperature gas permeability measurements of Barnwell core dried at 50degC yield permeability ranging from 6.24E-02 Darcys to 6.98E-08 Darcys. Friction angles from the direct shear tests vary from 28.1deg to 44.4deg for residual shear strength and average 47.9deg for peak shear strength. Cohesion averaged 3.2 psi and 13.3 psi for residual and peak shear strength values respectively. The work presented herein is the initial determination of an ongoing broader material characterization effort.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Abstract not provided.

Hydrogen effects on small-volume plasticity and elastic stiffness constants are investigated with nanoindentation of Ni-201 and sonic velocity measurements of bulk Ni single crystals. Elastic modulus of Ni-201, calculated from indentation data, decreases ~22% after hydrogen charging. This substantial decrease is independently confirmed by sonic velocity measurements of Ni single crystals; c₄₄ decreases ~20% after hydrogen exposure. Furthermore, clear hydrogen-deformation interactions are observed. The maximum shear stress required to nucleate dislocations in hydrogen-charged Ni-201 is markedly lower than in as-annealed material, driven by hydrogen-reduced shear modulus. Additionally, a larger number of depth excursions are detected prior to general yielding in hydrogen-charged material, suggesting cross-slip restriction. Together, these data reveal direct correlation between hydrogen-affected elastic properties and plastic deformation in Ni alloys.

Abstract not provided.

A novel experimental geometry is combined with acoustic emission monitoring capability to measure crack growth and damage accumulation during laboratory simulations of borehole breakout. Three different experiments are conducted in this study using Sierra White Granite. In the first experiment, the sample is deformed at a constant 17.2 MPa confining pressure without pore fluids; in the second experiment, the sample is held at a constant effective pressure of 17.2 MPa with a constant pore pressure; and in the third experiment, pore pressure is modified to induce failure at otherwise constant stress. The results demonstrate that effective pressure and stress path have controlling influence on breakout initiation and damage accumulation in laboratory simulations of wellbore behavior. Excellent agreement between the dry test and constant pore pressure test verify the application of the effective pressure law to borehole deformation. Located AE events coincide with post-test observations of damage and fracture locations. Comparison of AE behavior between the experiments with pore pressure show that breakouts develop prior to peak stress, and continued loading drives damage further into the formation and generates shear fractures.