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Dynamic response of additively manufactured Ti-5Al-5V-5Mo-3Cr as a function of heat treatment

Journal of Applied Physics

Specht, Paul E.; Ruggles, Timothy; Miers, John C.; Moore, David G.; Brown, Nathan P.; Duwal, Sakun; Branch, Brittany A.

Both shock and shockless compression experiments were performed on laser powder bed fusion (LPBF) Ti-5Al-5V-5Mo-3Cr (Ti-5553) to peak compressive stresses near 15 GPa. Experiments were performed on the as-built material, containing a purely β (body centered cubic) microstructure, and two differing heat treatments resulting in a dual phase α (hexagonal close packed) and β microstructure. The Hugoniot, Hugoniot elastic limit (HEL), and spallation strength were measured and compared to wrought Ti-6Al-4V (Ti-64). The results indicate the LPBF Ti-5553 Hugoniot response is similar between heat treatments and to Ti-64. The HEL stress observed in the LPBF Ti-5553 was considerably higher than Ti-64, with the as-built, fully β alloy exhibiting the largest values. The spallation strength of the LPBF Ti-5553 was also similar to Ti-64. Clear evidence of initial porosity serving as initiation sites for spallation damage was observed when comparing computed tomography measurements before and after loading. Post-mortem scanning electron microscopy images of the recovered spallation samples showed no evidence of retained phase changes near the spall plane. The spall plane was found to have kinks aligned with the loading direction near areas with large concentrations of twin-like, crystallographic defects in the as-built condition. For the heat-treated samples, the concentrations of twin-like, crystallographic defects were absent, and no preference for failure at the interface between the α and β phases was observed.

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Process-structure-property considerations for wire-based directed energy deposition of Ti-6Al-4V

Materials Characterization

Sims, Hannah; Pegues, Jonathan W.; Whetten, Shaun R.; Kustas, Andrew B.; Moore, David G.; Chilson, Tyler W.

Directed energy deposition (DED) is an attractive additive manufacturing (AM) process for large structural components. The rapid solidification and layer-by-layer process associated with DED results in non-ideal microstructures, such as large grains with strong crystallographic textures. These non-ideal microstructures can lead to severe anisotropy in the mechanical properties. Despite these challenges, DED has been identified as a potential solution for the manufacturing of near net shape Ti-6Al-4V preforms, replacing lost casting and forging capabilities. Two popular wire-based directed energy deposition (W-DED) processes were considered for the manufacturing of Ti-6Al-4V with assessments on their respective metallurgical and mechanical properties, as compared to a conventionally processed material. The two W-DED processes explored were wire arc additive manufacturing (WAAM) and electron beam additive manufacturing (EBAM). High throughput inspection and tensile testing procedures were utilized to generate statistically relevant data sets related to each process and sample orientation. The 2 AM technologies produced material with remarkably different microstructures and mechanical properties. Results revealed key differences in strength and ductility for the two disparate processes which were found to be related to differences in the metallurgical properties.

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Understanding Phase and Interfacial Effects of Spall Fracture in Additively Manufactured Ti-5Al-5V-5Mo-3Cr

Branch, Brittany A.; Ruggles, Timothy; Miers, John C.; Massey, Caroline E.; Moore, David G.; Brown, Nathan; Duwal, Sakun; Silling, Stewart; Mitchell, John A.; Specht, Paul E.

Additive manufactured Ti-5Al-5V-5Mo-3Cr (Ti-5553) is being considered as an AM repair material for engineering applications because of its superior strength properties compared to other titanium alloys. Here, we describe the failure mechanisms observed through computed tomography, electron backscatter diffraction (EBSD), and scanning electron microscopy (SEM) of spall damage as a result of tensile failure in as-built and annealed Ti-5553. We also investigate the phase stability in native powder, as-built and annealed Ti-5553 through diamond anvil cell (DAC) and ramp compression experiments. We then explore the effect of tensile loading on a sample containing an interface between a Ti-6Al-V4 (Ti-64) baseplate and additively manufactured Ti-5553 layer. Post-mortem materials characterization showed spallation occurred in regions of initial porosity and the interface provides a nucleation site for spall damage below the spall strength of Ti-5553. Preliminary peridynamics modeling of the dynamic experiments is described. Finally, we discuss further development of Stochastic Parallel PARticle Kinteic Simulator (SPPARKS) Monte Carlo (MC) capabilities to include the integration of alpha (α)-phase and microstructural simulations for this multiphase titanium alloy.

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Understanding the role of segmentation on process-structure–property predictions made via machine learning

International Journal of Advanced Manufacturing Technology

Massey, Caroline E.; Saldana, Christopher J.; Moore, David G.

The present study investigated the effect of porosity surface determination methods on performance of machine learning models used to predict the tensile properties of AlSi10Mg processed by laser powder bed fusion from micro-computed tomography data. Machine learning models applied in this work include support vector machines, neural networks, decision trees, and Bayesian classifiers. The effects of isosurface thresholding and local gradient approaches for porosity segmentation, as well as image filtering schemes, on model precision were evaluated for samples produced under differing levels of global energy density.

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Porosity Determination and Classification of Laser Powder Bed Fusion AlSi10Mg Dogbones Using Machine Learning

Conference Proceedings of the Society for Experimental Mechanics Series

Massey, Caroline E.; Moore, David G.; Saldana, Christopher J.

Metal additive manufacturing allows for the fabrication of parts at the point of use as well as the manufacture of parts with complex geometries that would be difficult to manufacture via conventional methods (milling, casting, etc.). Additively manufactured parts are likely to contain internal defects due to the melt pool, powder material, and laser velocity conditions when printing. Two different types of defects were present in the CT scans of printed AlSi10Mg dogbones: spherical porosity and irregular porosity. Identification of these pores via a machine learning approach (i.e., support vector machines, convolutional neural networks, k-nearest neighbors’ classifiers) could be helpful with part qualification and inspections. The machine learning approach will aim to label the regions of porosity and label the type of porosity present. The results showed that a combination approach of Canny edge detection and a classification-based machine learning model (k-nearest neighbors or support vector machine) outperformed the convolutional neural network in segmenting and labeling different types of porosity.

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Porosity Determination and Classification of Laser Powder Bed Fusion AlSi10Mg Dogbones Using Machine Learning

Conference Proceedings of the Society for Experimental Mechanics Series

Massey, Caroline E.; Moore, David G.; Saldana, Christopher J.

Metal additive manufacturing allows for the fabrication of parts at the point of use as well as the manufacture of parts with complex geometries that would be difficult to manufacture via conventional methods (milling, casting, etc.). Additively manufactured parts are likely to contain internal defects due to the melt pool, powder material, and laser velocity conditions when printing. Two different types of defects were present in the CT scans of printed AlSi10Mg dogbones: spherical porosity and irregular porosity. Identification of these pores via a machine learning approach (i.e., support vector machines, convolutional neural networks, k-nearest neighbors’ classifiers) could be helpful with part qualification and inspections. The machine learning approach will aim to label the regions of porosity and label the type of porosity present. The results showed that a combination approach of Canny edge detection and a classification-based machine learning model (k-nearest neighbors or support vector machine) outperformed the convolutional neural network in segmenting and labeling different types of porosity.

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Evolution of global and local deformation in additively manufactured octet truss lattice structures

Additive Manufacturing Letters

Jost, Elliott W.; Moore, David G.; Saldana, Christopher

Additively manufactured lattice truss structures, often referred to as architected cellular materials, present significant advantages over conventional structures due to their unique characteristics such as high strength-to-weight ratios and surface area-to-volume ratios. These geometrically complex structures, however, come with concomitant challenges for qualification and inspection. In this study, compression testing interrupted with micro-computed tomography inspection was conducted to monitor the evolution of global and local deformation throughout the loading process of 304 L stainless steel octet truss lattice structures. Both two- and three-dimensional image analysis techniques were leveraged to characterize geometric heterogeneities resulting from the laser powder bed fusion manufacturing process as well as track the structure throughout deformation. Variations from model-predicted behavior resulting from these heterogeneities are considered relative to the predicted and actual responses of the structures during compression to better understand, model, and predict the octet truss lattice structure compression response.

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Combining In-situ Diagnostics and Data Analytics for Discovery of Process-Structure-Property Relationships in AM parts – A Step Toward Digital Twins

Heiden, Michael J.; Bolintineanu, Dan S.; Garland, Anthony; Cillessen, Dale; Moore, David G.; Saiz, David J.; Love, Ana S.; Aragon, Matthew

In-situ additive manufacturing (AM) diagnostic tools (e.g., optical/infrared imaging, acoustic, etc.) already exist to correlate process anomalies to printed part defects. This current work aimed to augment existing capabilities by: 1) Incorporating in-situ imaging w/ machine learning (ML) image processing software (ORNL- developed "Peregrine") for AM process anomaly detection 2) Synchronizing multiple in-situ sensors for simultaneous analysis of AM build events 3) Correlating in-situ AM process data, generated part defects and part mechanical properties The key R&D question investigated was to determine if these new combined hardware/software tools could be used to successfully quantify defect distributions for parts build via SNL laser powder bed fusion (LPBF) machines, aiming to better understand data-driven process-structure-property- performance relationships. High resolution optical cameras and acoustic microphones were successfully integrated in two LPBF machines and linked to the Peregrine ML software. The software was successfully calibrated on both machines and used to image hundreds of layers of multiple builds to train the ML software in identifying printed part vs powder. The software's validation accuracy to identify this aspect increased from 56% to 98.8% over three builds. Lighting conditions inside the chamber were found to significantly impact ML algorithm predictions from in-situ sensors, so these were tailored to each machine's internal framework. Finally, 3D part reconstructions were successfully generated for a build from the compressed stack of layer-wise images. Resolution differences nearest and furthest from the optical camera were discussed. Future work aims to improve optical resolution, increase process anomalies identified, and integrate more sensor modalities.

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Effects of spatial energy distribution-induced porosity on mechanical properties of laser powder bed fusion 316L stainless steel

Additive Manufacturing

Moore, David G.; Robbins, Aron; Saldana, Christopher; Miers, John C.

Laser powder bed fusion (LPBF) additive manufacturing (AM) offers a variety of advantages over traditional manufacturing, however its usefulness for manufacturing of high-performance components is currently hampered by internal defects (porosity) created during the LPBF process that have an unknown impact on global mechanical performance. By inducing porosity distributions through variations in print energy density and inspecting the resulting tensile samples using computed tomography, nearly 50,000 pores across 75 samples were identified. Porosity characteristics were quantitatively extracted from inspection data and compared with mechanical properties to understand the strength of relationships between porosity and global tensile performance. Useful porosity characteristics were identified for prediction of part performance. Results indicate that ductility and strain at ultimate tensile strength are the global tensile properties most significantly impacted by porosity and can be predicted with reasonable accuracy using simple porosity shape descriptors such as volume, diameter, and surface area. Moreover, it was found that the largest pores influenced behavior most significantly. Specifically, pores in excess of 125 µm in diameter were found to be a sufficient threshold for property estimation. These results establish an initial understanding of the complex defect-performance relationship in AM 316L stainless steel and can be leveraged to develop certification standards and improve confidence in part quality and reliability for the broader set of engineering alloys.

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Understanding Microstructural Effects on Dynamic Performance Towards the Development of Shock Metamaterials

Branch, Brittany A.; Specht, Paul E.; Ruggles, Timothy; Moore, David G.; Jared, Bradley H.

With the recent advances in additive manufacturing (AM), long-range periodic lattice assemblies are being developed for vibration and shock mitigation components in aerospace and military applications with unique geometric and topological structures. There has been extensive work in understanding the static properties associated with varying topology of these lattice architectures, but there is almost no understanding of microstructural affects in such structures under high-strain rate dynamic loading conditions. Here we report the shock behavior of lattices with varying intrinsic grain structures achieved by post process annealing. High resolution 316L stainless steel lattices were 3D printed by a laser-powder bed fusion machine and characterized by computed tomography. Subsequent annealing resulted in stress-relieved and recrystallized lattices. Overall the lattices had strong cubic texture aligning with the x-, y- and z-directions of the build with a preference outside the build direction (z). The recrystallized sample had more equiaxed polygonal grains and a layer of BCC ferrite at the surface of the structure approximately 1 grain thick. Upon dynamic compression the as-deposited lattice showed steady compaction behavior while the heat-treated lattices exhibit negative velocity behavior indicative of failure. We attribute this to the stiffer BCC ferrite in the annealed lattices becoming damaged and fragmenting during compression.

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Cookoff experiments of a melt cast explosive (Comp-B3)

Combustion and Flame

Hobbs, Michael L.; Kaneshige, Michael; Erikson, William W.; Brown, Judith A.; Anderson, Mark U.; Todd, Steven N.; Moore, David G.

Validated models of melt cast explosives exposed to accidental fires are essential for safety analysis. In the current work, we provide several experiments that can be used to develop and validate cookoff models of melt cast explosives such as Comp-B3 composed of 60:40 wt% RDX:TNT. We present several vented and sealed experiments from 2.5 mg to 4.2 kg of Comp-B3 in several configurations. We measured pressure, spatial temperature, and ignition time. Some experiments included borescope images obtained during both vented and sealed decomposition. We observed the TNT melt, the suspension of RDX particles in the melt, bubble formation caused by RDX decomposition, and bubble-induced mixing of the suspension. The RDX suspension did not completely dissolve, even as temperatures approached ignition. Our results contrast with published measurements of RDX solubility in hot TNT that suggest RDX would be completely dissolved at these high temperatures. These different observations are attributed to sample purity. We did not observe significant movement of the two-phase mixture until decomposition gases formed bubbles. Bubble generation was inhibited in our sealed experiments and suppressed mixing.

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Heterogeneities dominate mechanical performance of additively manufactured metal lattice struts

Additive Manufacturing

Dressler, Amber D.; Boyce, Brad L.; Moore, David G.; Miers, John C.; Jost, Elliott W.; Seepersad, Carolyn C.

Architected structural metamaterials, also known as lattice, truss, or acoustic materials, provide opportunities to produce tailored effective properties that are not achievable in bulk monolithic materials. These topologies are typically designed under the assumption of uniform, isotropic base material properties taken from reference databases and without consideration for sub-optimal as-printed properties or off-nominal dimensional heterogeneities. However, manufacturing imperfections such as surface roughness are present throughout the lattices and their constituent struts create significant variability in mechanical properties and part performance. This study utilized a customized tensile bar with a gauge section consisting of five parallel struts loaded in a stretch (tensile) orientation to examine the impact of manufacturing heterogeneities on quasi-static deformation of the struts, with a focus on ultimate tensile strength and ductility. The customized tensile specimen was designed to prevent damage during handling, despite the sub-millimeter thickness of each strut, and to enable efficient, high-throughput mechanical testing. The strut tensile specimens and reference monolithic tensile bars were manufactured using a direct metal laser sintering (also known as laser powder bed fusion or selective laser melting) process in a precipitation hardened stainless steel alloy, 17-4PH, with minimum feature sizes ranging from 0.5-0.82 mm, comparable to minimum allowable dimensions for the process. Over 70 tensile stress-strain tests were performed revealing that the effective mechanical properties of the struts were highly stochastic, considerably inferior to the properties of larger as-printed reference tensile bars, and well below the minimum allowable values for the alloy. Pre- and post-test non-destructive analyses revealed that the primary source of the reduced properties and increased variability was attributable to heterogeneous surface topography with stress-concentrating contours and commensurate reduction in effective load-bearing area.

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Listening to temperature: Ultrasonic non-destructive identification of material phase and temperature

AIP Conference Proceedings

Moore, David G.; Jack, David; Jeffrey, Taylor

In the chemical transport field, such as petro-chemicals or food processing, there is a need to quantify the spatially varying temperature and phase state of the material within a cylindrical vessel, such as a pipeline, using non-invasive techniques. Using ultrasonic signals, which vary in time-of-flight, intensity, and wave characteristics based on the temperature and phase of a material, an automated technique is presented which can provide a non-axisymmetric map of the phase and temperature inside a cylindrical vessel within a single plane using exclusively information from the through-transmission wave and the external temperature profile. This research demonstrates the approach using an amorphous wax, due to its stable nature and ability to be reheated many times without changing the properties of the wax. Due to its amorphous nature, the wax transitions from a solid to a low-viscosity fluid over a range of temperatures. This behavior is similar to that of a thermoplastic and a slurry experiencing curing. As the spatial temperature within a container of wax increases the time of flight for an ultrasonic signal will change. Results presented indicate the ability of the investigated technique to map the temperature and phase change of the wax based solely on the ultrasonic signals and knowledge of the external temperature on the outer edge of the vessel.

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Characterization and nondestructive inspection of additively manufactured materials

AIP Conference Proceedings

Stair, Sarah L.; Moore, David G.

Additively manufactured (AM) components often exhibit significant discontinuities and indications without a clear understanding of how they might affect the mechanical properties of a part during qualification and service. This uncertainty is unacceptable for the design and manufacturing of most aerospace components. Current research in both mechanical testing and nondestructive evaluation involves developing methods for characterizing and inspecting AM components as the use of such materials continues to rise. Although several AM manufacturing methods have been developed in recent decades, this paper focuses on AM production-ready processes for a direct metal laser sintering (DMLS) powder bed fusion machine and will provide background on Sandia National Laboratories' research efforts in this area. Tensile bar samples manufactured using the DMLS powder bed fusion method were inspected in this study, and the results of ultrasonic spectroscopy for assessing internal flaws will be presented. A combination of material property evaluation, microstructural characterization, and nondestructive inspection techniques will also be described. The results obtained from these material evaluation methods assist in determining inspection limits and methods for qualifying AM materials.

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Effects of spatial energy distribution on defects and fracture of LPBF 316L stainless steel

Solid Freeform Fabrication 2019: Proceedings of the 30th Annual International Solid Freeform Fabrication Symposium - An Additive Manufacturing Conference, SFF 2019

Jost, Elliott W.; Moore, David G.; Robbins, Aron; Miers, John C.; Saldana, Christopher

Measures of energy input and spatial energy distribution during laser powder bed fusion additive manufacturing have significant implications for the build quality of parts, specifically relating to formation of internal defects during processing. In this study, scanning electron microscopy was leveraged to investigate the effects of these distributions on the mechanical performance of parts manufactured using laser powder bed fusion as seen through the fracture surfaces resulting from uniaxial tensile testing. Variation in spatial energy density is shown to manifest in differences in defect morphology and mechanical properties. Computed tomography and scanning electron microscopy inspections revealed significant evidence of porosity acting as failure mechanisms in printed parts. These results establish an improved understanding of the effects of spatial energy distributions in laser powder bed fusion on mechanical performance.

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Non-destructive inspection approach using ultrasound to identify the material state for amorphous and semi-crystalline materials

AIP Conference Proceedings

Moore, David G.; Jack, David

At present, there are many methods to identify the temperature and phase of a material using invasive techniques. However, most current methods require physical contact or implicit methods utilizing light reflectance of the specimen. This work presents a nondestructive inspection method using ultrasonic wave technology that circumvents these disadvantages to identify phase change regions and infer the temperature state of a material. In the present study an experiment is performed to monitor the time of flight within a wax as it undergoes melting and the subsequent cooling. Results presented in this work show a clear relationship between a material's speed of sound and its temperature. The phase change transition of the material is clear from the time of flight results, and in the case of the investigated material, this change in the material state occurs over a range of temperatures. The range of temperatures over which the wax material melts is readily identified by speed of sound represented as a function of material temperature. The melt temperature, obtained acoustically, is validated using Differential Scanning Calorimetry (DSC), which uses shifts in heat flow rates to identify phase transition temperature ranges. The investigated ultrasonic NDE method has direct applications in many industries, including oil and gas, food and beverage, and polymer composites, in addition to many implications for future capabilities of nondestructive inspection of multi-phase materials.

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The relationship between experimental geometry, heat rate, and ultrasound wave speed measurement while observing phase changes in highly attenuative materials

AIP Conference Proceedings

Moore, David G.; Stair, Sarah L.; Jack, David A.

Ultrasound techniques are capable of monitoring changes in the time-of-flight as a material is exposed to different thermal environments. The focus of the present study is to identify the phase of a material via ultrasound compression wave measurements in a through transmission experimental setup as the material is heated from a solid to a liquid and then allowed to re-solidify. The present work seeks to expand upon the authors' previous research, which proved this through transmission phase monitoring technique was possible, by considering different experimental geometries. The relationship between geometry, the measured speed of sound, and the temperature profile is presented. The use of different volumes helps in establishing a baseline understanding of which aspects of the experiment are geometry dependent and which are independent. The present study also investigates the relationship between the heating rate observed in the experiment and the measured speed of sound. The trends identified between the experimental geometry, heat rate and ultrasound wave speed measurement assist in providing a baseline understanding of the applicability of this technique to various industries, including the polymer industry and the oil industry.

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Non-Destructive Evaluation of the Bondline Interface between Carbon Fiber Reinforced Laminated Composites and Metal Materials via Ultrasonic Inspection Methods

Proposed Journal Article, unpublished

Moore, David G.; Stair, Sarah L.; Jack, David A.; Nelson, Ciji

Woven fiber, laminated composites allow the design engineer to create high strength parts, but the effectiveness of the final processed part is greatly diminished through weak or nonexistent bonds between the composite and the substrate to which it is bonded. Additionally, these layered laminates are commonly made by curing the resin infused carbon fiber fabrics in predefined layers and then bonding them to another composite or a metallic structure using either a pre-cure or a co-cure method. The focus of this study is the identification of the defect caused by a disbond or a delamination located at the interface between a composite laminate stack and the substrate to which it is bonded. We present a nondestructive approach using various ultrasonic methods to identify the existence of the bond between composite and composite-to-metal interface. This paper explores contact and immersion ultrasound methods using pulse-echo for evaluating the composite material and adhesive bondline and the signal attenuation undergone by the wave as it propagates through the composite. Finally, a summary of the detection and analysis techniques developed to identify disbonds, including Fast Fourier Transform analysis of the immersion data, is presented. Lastly, each of the methods evaluated in this study is able to detect the transition from bonded to unbonded sections at the bondline from either side of the bonded part, with the immersion technique providing a significantly higher resolution of the edge of the bondline.

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Application of temporal moments and other signal processing algorithms to analysis of ultrasonic signals through melting wax

AIP Conference Proceedings

Moore, David G.; Lau, Sarah J.; Nelson, Ciji; Stair, Sarah L.

Ultrasonic analysis is being explored as a way to capture events during melting of highly dispersive wax. Typical events include temperature changes in the material, phase transition of the material, surface flows and reformations, and void filling as the material melts. Melt tests are performed with wax to evaluate the usefulness of different signal processing algorithms in capturing event data. Several algorithm paths are being pursued. The first looks at changes in the velocity of the signal through the material. This is only appropriate when the changes from one ultrasonic signal to the next can be represented by a linear relationship, which is not always the case. The second tracks changes in the frequency content of the signal. The third algorithm tracks changes in the temporal moments of a signal over a full test. This method does not require that the changes in the signal be represented by a linear relationship, but attaching changes in the temporal moments to physical events can be difficult. This paper describes the algorithm paths applied to experimental data from ultrasonic signals as wax melts and explores different ways to display the results.

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Wave speed propagation measurements on highly attenuative heated materials

Physics Procedia

Moore, David G.; Ober, Curtis C.; Rodacy, Philip J.; Nelson, Ciji

Ultrasonic wave propagation decreases as a material is heated. Two factors that can characterize material properties are changes in wave speed and energy loss from interactions within the media. Relatively small variations in velocity and attenuation can detect significant differences in microstructures. This paper discusses an overview of experimental techniques that document the changes within a highly attenuative material as it is either being heated or cooled from 25°C to 90°C. The experimental set-up utilizes ultrasonic probes in a through-transmission configuration. The waveforms are recorded and analyzed during thermal experiments. To complement the ultrasonic data, a Discontinuous-Galerkin Model (DGM) was also created which uses unstructured meshes and documents how waves travel in these anisotropic media. This numerical method solves particle motion travel using partial differential equations and outputs a wave trace per unit time. Both experimental and analytical data are compared and presented.

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FAA Fluorescent Penetrant Laboratory Inspections

Windes, Connor L.; Moore, David G.

The Federal Aviation Administration Airworthiness Assurance NDI Validation Center currently assesses the capability of various non-destructive inspection (NDI) methods used for analyzing aircraft components. The focus of one such exercise is to evaluate the sensitivity of fluorescent liquid penetrant inspection. A baseline procedure using the water-washable fluorescent penetrant method defines a foundation for comparing the brightness of low cycle fatigue cracks in titanium test panels. The analysis of deviations in the baseline procedure will determine an acceptable range of operation for the steps in the inspection process. The data also gives insight into the depth of each crack and which step(s) of the inspection process most affect penetrant sensitivities. A set of six low cycle fatigue cracks produced in 6.35-mm thick Ti-6Al-4V specimens was used to conduct the experiments to produce sensitivity data. The results will document the consistency of the crack readings and compare previous experiments to find the best parameters for water-washable penetrant.

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Sensitivity Variation on Low Cycle Fatigue Cracks Using Level 4/Method B Penetrant

Moore, David G.

The Federal Aviation Administration's Airworthiness Assurance NDI Validation Center (AANC) is currently conducting experiments with Level 4, Method B penetrant on low cycle fatigue specimens. The main focus of these experiments is to document the affect on penetrant brightness readings by varying inspection parameters. This paper discusses the results of changing drying temperature, drying time, and dwell time of both penetrant and emulsifier on low cycle fatigue specimens.

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Stress Corrosion Crack Detection on HU-25 Guardian Aircraft

Moore, David G.

Several ultrasonic inspection methods were developed at the Federal Aviation Administration's Airworthiness Assurance NDI Validation Center (AANC) to easily and rapidly detect hidden stress corrosion cracks in all vertical windshield posts on the US Coast Guard (USCG) HU-25 Guardian aircraft. The inspection procedure locates cracks as small as 2.0 millimeters emanating from internal fastener holes and determines their length. A test procedure was developed and a baseline assessment of the USCG fleet was conducted. Inspection results on twenty-five aircraft revealed a good correlation with results made during subsequent structural disassembly and visual inspection.

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High-Density Plasma Etching of Group-III Nitride Films for Device Application

Moore, David G.

As III-V nitride device structures become more complicated and design rules shrink, well-controlled etch processes are necessary. Due to limited wet chemical etch results for the group-III nitrides, a significant amount of effort has been devoted to the development of dry etch processing. Dry etch development was initially focused on mesa structures where high etch rates, anisotropic profiles, smooth sidewalls, and equi-rate etching of dissimilar materials were required. For example, commercially available LEDs and laser facets for GaN-based laser diodes have been patterned using reactive ion etching (RIE). With the recent interest in high power, high temperature electronic devices, etch characteristics may also require smooth surface morphology, low plasma-induced damage, and selective etching of one layer over another. The principal criteria for any plasma etch process is its utility in the fabrication of a device. In this study, we will report plasma etch results for the group-III nitrides and their application to device structures.

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FAA Fluorescent Penetrant Activities - An Update

Moore, David G.

The Federal Aviation Administration's Airworthiness Assurance NDI Validation Center (AANC) is currently characterizing low cycle fatigue specimens that will support the needs of penetrant manufacturers, commercial airline industry and the Federal Aviation Administration. The main focus of this characterization is to maintain and enhance the evaluation of penetrant inspection materials and apply resources to support the aircraft community needs. This paper discusses efforts to-date to document the Wright Laboratory penetrant evaluation process and characterize penetrant brightness readings in the initial set of sample calibration panels using Type 1 penetrant.

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Emerging NDE Technology for aging aircraft

Moore, David G.

This paper presents an overview of several emerging nondestructive evaluation technologies that are being employed or considered for use to inspect commercial transport, commuter aircraft and military aircraft. An overview of the Federal Aviation Administration (FAA) Airworthiness Assurance NDI Validation Center (AANC) is described and how AANC teams with industry, universities, and other federal entities to assess these technologies.

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Nondestructive inspection assessment of eddy current and electrochemical analysis to separate inconel and stainless steel alloys

Moore, David G.

This report presents a nondestructive inspection assessment of eddy current and electrochemical analysis to separate inconel alloys from stainless steel alloys as well as an evaluation of cleaning techniques to remove a thermal oxide layer on aircraft exhaust components. The results of this assessment are presented in terms of how effective each technique classifies a known exhaust material. Results indicate that either inspection technique can separate inconel and stainless steel alloys. Based on the experiments conducted, the electrochemical spot test is the optimum for use by airframe and powerplant mechanics. A spot test procedure is proposed for incorporation into the Federal Aviation Administration Advisory Circular 65-9A Airframe & Powerplant Mechanic - General Handbook. 3 refs., 70 figs., 7 tabs.

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Crack detection on HC-130H aircraft using low frequency eddy current

Moore, David G.

An eddy current inspection method was developed at the Federal Aviation Administration`s Airworthiness Assurance NDI Validation Center (AANC) to easily and rapidly detect subsurface fatigue cracks in the wheel well fairing on the US Coast Guard (USCG) HC-130H aircraft caused by fatigue. The inspection procedure locates cracks as small as 10.2 millimeters in length at 2.54 mm below the skin surface at raised fastener sites. The test procedure developed baseline three USCG aircraft. Inspection results on the three aircraft reveals good correlation with results made during subsequent structural disassembly.

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FAA fluorescent penetrant activities

Moore, David G.

The Federal Aviation Administration`s Airworthiness Assurance NDI Validation Center (AANC) and the Center for Aviation Systems Reliability (CASR) are currently working to develop a liquid penetrant inspection (LPI) system evaluation capability that will support the needs of the penetrant manufacturers, commercial airline industry and the FAA. The main focus of this facility is to support the evaluation of penetrant inspection materials, penetrant systems and to apply resources to support industry needs. This paper discusses efforts to create such a facility and an initial project to produce fatigue crack specimens for evaluation of Type 1 penetrant sensitivities.

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Low-voltage radiography on aircraft composite doublers

Moore, David G.

Composite doublers are gaining popularity for their ability to repair and reinforce commercial aircraft structures and it is anticipated that the potential cost savings may spur wider use of this technology. But before composite doublers can be accepted by the civil aviation industry, inspection techniques must be developed to verify the integrity of the doubler and the parent material under the doubler. The Federal Aviation Administration Airworthiness Assurance NDI Validation Center (AANC) is currently developing test methods to inspect aircraft structures under composite doublers using low kilovoltage radiography. This paper documents the radiographic techniques developed by the AANC which have been found to give the best contrast of the radiographic image with reduced image distortion.

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Effect of conductivity between fasteners and aluminum skin on eddy current specimens

Moore, David G.

The Federal Aviation Administration Airworthiness Assurance Nondestructive Inspection Validation Center (FAA-AANC) and Boeing Commercial Airplane Group are currently developing a study pertaining to the detection of cracks in multi-layered aluminum sheets. The specimen panels model pertinent aspects of the lap splice joints for Boeing 737 aircraft, Line Numbers 292 - 2565. Upon initial characterization of the specimen panels, it became clear that signals produced from a sliding probe at fastener sites were not representative of an in-service lap splice, and therefore, could not be used in a probability of detection experiment. This paper discusses specimen characterization and steps taken to make the specimens useful for nondestructive technology assessment.

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Crack detection on HU-25 Guardian aircraft

Moore, David G.

An ultrasonic inspection method was developed at FAA`s Airworthiness Assurance NDI Validation Center (AANC) to easily and rapidly detect hidden fatigue cracks in the copilot vertical windshield post on USCG (Coast Guard) HU-25 `Guardian` aircraft. The inspection procedure locates hidden cracks as small as 3.2 mm emanating from internal fastener holes and determines their length. A test procedure was developed and a baseline assessment of the USCG fleet conducted. Inspection results on 41 aircraft revealed good correlation with results made during subsequent structural disassembly and visual inspection of selected aircraft.

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Characterization of a resonant plate shock system using finite element analysis

Moore, David G.

The dynamic performance of a 250 Hz resonant plate shock system which simulates pyrotechnic shock environments on micro-electrical components is evaluated. A series of experiments recording strain rate histories and acceleration time histories at several plate locations were conducted. This empirical data is used to compare the analytical results obtained from a finite element based numerical simulation. The comparison revealed a good correlation between experimental and analytical results.

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135 Results
135 Results