Publications

A new technique, called tethered rocket, has been developed for testing in the penetration and/or impact modes. The technique involves tethering a rocket-motor assembly to an earth-fixed pivot so that the resulting semicircular arc delivers a payload to a precise impact point. Discussions are presented which describe the analytical and experimental activities of the tethered rocket technique. A series of analytical models has been integral to the success of the tethered rocket development. The analytic results were verified by testing. The tests demonstrated the viability of the technique for penetration and/or impact testing. Also included is a discussion of potential applications of the method. 18 refs., 53 figs., 17 tabs.

Cracking, craters, spotty damage (discoloration), and missing chunks of material have been observed on limiters and along the midplane of tokamak inner walls. This damage is assumed to be due to runaway electron discharges. These runaway electrons have been predicted to range in energy from a few MeV to several hundred MeV. The energy density from the runaway electron discharges ranges from 10 to 500 MJ/m{sup 2} over pulse lengths of 5 to 50 msec. The PTA code package is a unique application of PATRAN, the Integrated TIGER Series, and ABAQUS for modeling high energy electron impact on tokamak first wall and limiter materials. The PTA code package provides a three-dimensional, time dependent, computational code package which predicts energy deposition, temperature rise, and damage on relevant fusion materials from runaway electrons. In this benchmark study, three experiments were modeled to validate the PTA code package. The first and third experiment simulated runaway electrons scattering through a plasma facing surface (graphite) into an internal structure (copper), and the second experiment tested the thermal and structural response from high energy electron impact on different fusion relevant materials. The PTA calculations compared favorably with the experimental results. In particular, the PTA models identified gap conductance, thermal contact, x-ray generation in materials, and the placement of high stopping power materials as key factors in the design of plasma facing components that are resistant to runaway electron damage. 13 refs., 40 figs., 3 tabs.

We have determined experimentally the Shielding Effectiveness (SE) at microwave frequencies of various types of single- and double-braided cables and connectors typical of systems that have been hardened to electromagnetic fields. This report describes a laboratory-sized reverberation chamber and the techniques used to measure the SE of several interconnecting components. Graphical results are presented in the report, along with smoothed overlay plots for each category of measurements. The overlay plots indicate the general trends in the raw data and highlight the differences between tested components. 7 refs., 22 figs.

This report describes a statistical model for field amplitudes within a mode-stirred chamber. The parameters of the probability density function for field amplitudes are estimated by means of maximum likelihood. The accuracy of these parameters is specified as a function of the amount of data used. An experimental investigation of the possibility of using an existing electromagnetic shield room as a mode-stirred chamber is described. The physical alterations of the chamber and the instrumentation are summarized. Descriptions of the tests results are reported. The tests were conducted to determine: the unloaded and loaded Q of the chamber, descriptive statistics of the electromagnetic fields, correlation distances of the fields in frequency, tuner angle, and spatial position, and the possibility of using frequency stirring as an alternative to mechanical stirring. 10 refs., 20 figs., 10 tabs.

High-quality recording of an oscilloscope waveform is usually made on photographic film. Achieving high quality, especially in a possible radiation environment and with fast sweep speeds, requires a thorough understanding of all aspects of the imaging and recording processes. This paper represents a compilation of techniques and procedures to achieve optimum oscilloscope imagery under adverse conditions and in an environment where unwanted radiation is a possibility. 10 figs., 1 tab.

Structural system identification methods are analytical techniques for reconciling test data with analytical models. However, for system identification to become a practical tool for engineering analysis, the estimation techniques/codes must communicate with finite element software packages without intensive analyst intervention and supervision. This paper presents a technique used to integrate commercial software packages for finite element modeling (MSC/NASTRAN), mathematical programming techniques (ADS), and linear system analysis (PRO-MATLAB). The parameter estimation techniques and the software for controlling the overall system were programmed in PRO-MATLAB. Two examples of application of this software using measured data are presented. The examples consist of a truss structure in which the model form is well defined, and an electronics package whose model form is ill-defined since it is difficult to model with finite elements. A comparison of the resulting updated models with the experimental data showed significant improvement. 22 refs.

A Level II/III probabilistic risk assessment (PRA) has been performed for N Reactor, a Department of Energy (DOE) production reactor located on the Hanford reservation in Washington. The accident progression analysis documented in this report determines how core damage accidents identified in the Level I PRA progress from fuel damage to confinement response and potential releases the environment. The objectives of the study are to generate accident progression data for the Level II/III PRA source term model and to identify changes that could improve plant response under accident conditions. The scope of the analysis is comprehensive, excluding only sabotage and operator errors of commission. State-of-the-art methodology is employed based largely on the methods developed by Sandia for the US Nuclear Regulatory Commission in support of the NUREG-1150 study. The accident progression model allows complex interactions and dependencies between systems to be explicitly considered. Latin Hypecube sampling was used to assess the phenomenological and systemic uncertainties associated with the primary and confinement system responses to the core damage accident. The results of the analysis show that the N Reactor confinement concept provides significant radiological protection for most of the accident progression pathways studied.

This report documents the development and testing of the SA3263 high voltage rectifier diode manufactured by Microsemi. 15 refs., 4 tabs.

A new gridless electrostatic field solver which utilities Fourier decomposition in the azimuthal coordinate has been developed and tested. The scaling with the number of simulation particles is N log N. This algorithm has been implemented in the BUCKSHOT code, which originally used a direct summation algorithm with N{sup 2} scaling. The Fourier decomposition in the new algorithm is done about the center of mass of each species, thus nonlinear ion hose physics is included in the m = O mode. Higher order modes describe non-axisymmetric profile changes. The breakeven point between the new solver and the direct summation algorithm is about N = 64 particles per species when up to m = 2 Fourier modes are kept. For a typical ion hose simulation with 256 particles per species the new solver is faster by a factor of about 2.7. 8 refs., 11 figs.

In order to generate a lithium vapor on the anode surface within PBFA II, an electrically insulating, lithium-coated substrate is required. One approach for providing this lithium source is the ceramic-option anode. This anode consists of two halves, equatorially split, each containing an insulating ceramic insert onto which a lithium-bearing film is sputtered. A lithium vapor is generated by ohmically pulse heating this film to 1500 K. The half-anode structure required to produce this vapor consists of a ceramic insulator, steel housing, and disk conductors. This report describes the design and fabrication of these separate components and the procedures required to join them to form the half-anode assembly. In addition, appendices are included which contain detailed drawings and specifications for these operations. 5 refs., 10 figs.

This report describes standard design criteria for and intrabuilding and interbuilding telecommunications wiring system to provide voice and open data services to facilities at Sandia National Laboratories, Albuquerque.

The US Department of Energy's (DOE) Waste Isolation Pilot Plant (WIPP) must comply with EPA regulation 40 CFR Part 191, Subpart B, which sets environmental standards for radioactive waste disposal. The regulation, Environmental Radiation Protection Standards for Management and Disposal of Spent Nuclear Fuel, High-Level and Transuranic Radioactive Wastes (hereafter referred to as the Standard), was vacated in 1987 by a Federal Court of Appeals and is underground revision. By agreement with the Sate of New Mexico, the WIPP project is evaluating compliance with the Standard as promulgated, in 1985 until a new regulation is available. This report summarizes the early-1990 status of Sandia National Laboratories' (SNL) understanding of the Project's ability to achieve compliance. The report reviews the qualitative and quantitative requirements for compliance, and identifies unknowns complicating performance assessment. It discusses in relatively nontechnical terms the approaches to resolving those unknowns, and concludes that SNL has reasonable confidence that compliance is achievable with the Standard as first promulgated. 46 refs., 7 figs.

This report provides system designers with basic human factors information and guidelines to help in the selection of manual data input devices. The selection of such devices is important with respect to the environment in which the device with be used, speed of data entry required, error potential, and the user friendliness of the candidate devices. The report reviews several of the most commonly used data input devices and provides a description of each, experimental evaluations, and observations and recommendations based on review of the data. In addition, the appendix presents an input device matrix that gives general guidance concerning input devices and the physical and mission environment in which they might be used. Additional assistance should be requested from Sandia National Laboratories (SNL) Human Factors Personnel. 23 refs., 13 figs.

As a crosslinking polymer cures, dramatic changes in molecular architecture occur. These structural changes in turn affect the viscoelastic behavior of the material. At a critical extent of reaction (the gel point), the polymer undergoes a transition from a viscous liquid to an elastic solid. We have monitored the evolution of structure and viscoelasticity in the most common epoxy encapsulant used at Sandia, diethanolamine-cured Epon 828. The structure evolves according to percolation theory, and the viscoelasticity evolves according to our dynamic scaling theory for branched polymers. 9 refs., 12 figs.

Calculations are performed to predict the distribution of the (5p){sup 5}(5d)--(5p){sup 5}(6p)emission cross section in Xe in a strong magnetic field. For isotopes with no nuclear magnetic moment, the question is the calculation of Lande g factors. This is done with wavefunctions obtained by diagonalizing the electrostatic interaction in jj coupling, leading to reasonable accurate Lande g factors. For levels described by quantum numbers J and M, the Zeeman interaction is always diagonal in M, and with a 6 kG magnetic field the Zeeman interaction is effectively diagonal in J (the non-diagonal matrix elements are negligible), so the resulting cross section calculations are simple. For the isotopes with non-zero magnetic moments, one must determine the dipole and quadrupole hyperfine splitting coefficients. To do this and to improve the overall fit of the calculated and measured energy levels, it was necessary to include configuration interaction between terms of the (5p){sup 5}(5d) and (5p){sup 5}(6s) configurations. Comparisons are made between these calculated hyperfine parameters and experiment. Hyperfine splittings are tabulated as are the cross sections and energy shifts due to hyperfine interaction in each transition. When hyperfine interaction is included and levels are characterized by the quantum numbers F and M{sub F}, the Zeeman interaction is diagonal in M{sub F} but different F. All these effects were included in the calculations leading to a particularly rich spectrum for Xe(131) with I = 3/2. For example, the (5p){sup 5}(5d){sub J} = 4{minus}(5p){sup 5}(6p){sub J} = 3 transition is split into approximately 336 components. 21 refs., 3 figs., 12 tabs.

This annual report summarizes progress which has been made in Fiscal Year 1989 on this program of geotechnology for tight gas reservoirs. Most of the studies are an outgrowth of the results and experience from the Multiwell Experiment -- an unprecedented investigation of western gas reservoirs typical of the Mesaverde Formation. Results are presented in the following study areas: (1) tectonism, subsidence and fracturing of these reservoirs, (2) mechanism for the formation of regional fractures in flat-lying basins, (3) the case against natural hydraulic fracturing, (4) characterization and implications of dickite-mineralized fractures, (5) significance of coring-induced fractures, (6) determination of an effective stress law for permeability in tight sandstones, and (7) stress azimuths for two well sites in the Piceance Basin. In addition, technology transfer aspects and impact of the Multiwell Experiment are summarized. 27 refs., 28 figs., 1 tab.

This study was performed under FUTURE LOOK, a joint Defense Nuclear Agency/Department of Energy (DNA/DOE) sponsored study. The intent of FUTURE LOOK is to identify and develop means of providing requisite security and survivability to the Non-Strategic Nuclear Forces (NSNF) in the Twenty-First Century. Our current thinking about the future world in Europe is summarized. In this report we develop four scenarios/stockpile cases to cover the spectrum of potential happenings in Europe; we also develop general security and survivability implications and recommendations for each case. The four cases are: (1) a substantially reduced (factor of 2--10) European stockpile; (2) a near-zero stockpile, with no Army weapons remaining in Europe; (3) current stockpile in Europe remains; and (4) current stockpile numbers remain, but aggressive modernization is allowed. We plan to use the information in this report to assist in developing detailed security and survivability options as part of our follow-on to FUTURE LOOK studies. 8 refs., 6 tabs.

The purpose of this computer program is to serve as a tool in the daily operation of the R D storage function. This menu-driven, interactive program was written in DBase III+ for use on an IBM PC-XT computer to efficiently store items in a minimum space, inventory, locate, report, withdraw and record the activities in a history file. A drive path is utilized in numbering each storage location to minimize the distance and time required to store and retrieve an item. An empty-space listing is available for a limited inventory.

The United States Department of energy, after considering a number of alternative disposal methods for radioactive wastes in the United States, Proposed that these wastes should be disposed of in deep geologic repositories. This alternative is currently being developed at the Waste Isolation Pilot Plant (WIPP), for transuranic waste, and investigated at Yucca Mountain, for spent power-reactor fuel and vitrified high-level waste, the latter resulting principally from defense activities. In addition, a research program on subseabed disposal was active from 1973 until 1987 but is currently suspended. The two deep-geologic disposal projects are discussed in detail and the subseabed-disposal research project is briefly summarized. 28 refs., 39 figs., 4 tabs.

Thermal and mechanical models for intact and jointed rock mass behavior are being developed, verified, and validated at Sandia National Laboratories for the Yucca Mountain Project. Benchmarking is an essential part of this effort and is the primary tool for verifying engineering software used to solve thermomechanical problems. This report presents the results of the second phase of the first thermomechanical benchmark exercise. In the first phase of this exercise, three finite element codes for nonlinear heat conduction and one coupled thermoelastic boundary element code (HEFF) were used to solve the thermal portion of the benchmark problem. The boundary element code HEFF was used in this exercise because it calculates a solution to the coupled thermal/elastic problem using an approximate analytical method and, thus, provides a means of comparing the finite element solutions with a solution obtained by an independent method. The results from the thermal analysis were then used as input to the second phase of the analysis, which consisted of solving the structural portion of the benchmark problem using a linear elastic rock mass model. Five different structural codes, JAC, SPECTROM-31, VISCOT, and HEFF, were used by the participants in this portion of the study. The problem solved by each code was a two-dimensional idealization of a series of drifts with the approximate dimensions of the proposed design for vertical emplacement of nuclear waste at Yucca Mountain. 6 refs., 74 figs., 4 tabs.

This report documents the development and testing of the SA3262, a high voltage rectifier diode, manufactured by Microsemi. 13 figs., 4 tabs.

Dual focus laser velocimetry (L2F), photographic techniques, and pressure measurements were used to investigate particle and flame characteristics of a high velocity oxygen/fuel (HVOF) flame spray gun known as CDS''. Velocities of alumina, tungsten carbide, and Triballoy particles within the HVOF effluent stream have been measured using L2F techniques. Photographs of the exiting gases were used to determine the local Mach numbers within the gas stream. Measurements of Mach angles in the photographs were used to determine the actual gas velocity in the free jet of the device. Pressure measurements were made on the HVOF device which enabled calculations of the gas content, R, and the specific heat ratio, {kappa}. These calculations combined with estimates of gas temperature are used to calculate gas velocities at Mach 1 (nozzle exit). The HVOF device was used to produce dense WC/12 wt. % Co and Triballoy T-400 coatings. For the two gas flow conditions examined, higher hardness values and densities were observed for coatings deposited at the higher gas flow rates.

This report documents the characterization and development of the 381558 (2N6193JTXV), a medium power PNP silicon transistor designed for switching and wide band amplifier applications. The 2N6193JTXV is manufactured by Motorola. 50 figs., 6 tabs.

This report documents the characterization and development of the 381568 (2N5339JTXV), a medium power NPN silicon transistor designed for switching and wide band amplifier applications. The 2N5339JTXV is manufactured by Motorola. 50 figs., 6 tabs.

This report describes the major hardware and software components of the HERMES III Control and Monitor System at the Simulation Technology Laboratory (STL) at Sandia National Laboratories. The HERMES III Control and Monitor System is a computer controlled system that controls and monitors the charging, arming, and firing of the HERMES III accelerator. This documentation is intended to be a general introduction to the system for engineers and technicians involved in the maintenance and modification of the system. It may also be useful to persons interested in designing and constructing a similar control system. This report collects many of the documents produced throughout the project and directs the reader toward other documents written for this project.

This report describes the components and installation of the Oxygen Deficiency Monitor System (ODMS) at the Simulation Technology Laboratory (STL) at Sandia National Laboratories. The ODMS presently monitors the oxygen concentration of the ambient air in the lower levels of the laboratory where air circulation may be insufficient to disperse gases that may settle and accumulate creating an oxygen-deficient environment. The intent of this report is to provide a general introduction to the system for personnel involved in the maintenance and modifications of the system and may be useful to people interested in installing a similar system. This will report describe the hardware components, installation considerations, operation, and maintenance of the system. 6 refs., 5 figs.

The literature is reviewed on the amount and the characteristics of particulate material (crud), that is deposited on Light Water Reactor (LWR) fuel rods and assemblies. Currently available data on crud composition, specific activity, spallation mechanisms, potential environmental release, and particle size distributions is considered. In addition, literature that pertains to the possible impact of crud on repository operations is surveyed. This report consists of rather extensive excerpts from the published literature on crud that may have a bearing on repository risk assessment. Commentary on the possible effects of crud on repository operations and the applicability of available crud information to repository risk analyses is included. In addition, estimates are made of the quantity of crud that might be available for release during the different phases of repository operations. Using these estimates, the total effective dose equivalent is determined at several distances from a release point.

This 1989 report contains monitoring data from routine radiological and nonradiological environmental surveillance activities. Summaries of significant environmental compliance programs in progress such as National Environmental Policy Act documentation, environmental permits, environmental restoration, and various waste management programs for Sandia National Laboratories in Albuquerque (SNL, Albuquerque) are included. The maximum offsite dose impact was calculated to be 8.8 {times} 10{sup {minus}4} mrem. The total Albuquerque population received a collective dose of 0.097 person-rem during 1989 from SNL, Albuquerque, operations. As in the previous year, SNL, Albuquerque, operations in 1989 had no adverse impact on the general public or on the environment. 46 refs., 20 figs., 31 tabs.

This report summarizes the environmental surveillance activities conducted by Environmental Protection Agency (EPA) and Reynolds Electrical and Engineering Company (REECo) for the Tonopah Test Range (TTR) operated by Sandia National Laboratories (SNL). Other environmental compliance programs such as National Environmental Policy Act of 1969 (NEPA), environmental permits, environmental restoration, and waste management programs are also included. The maximum offsite dose impact from 1989 operations was 8.7 {times} 10{sup {minus}4} mrem as a result of an unusual occurrence. The population received a collective dose of 1.2 {times} 10{sup {minus}5} person-rem from this incidence, while the same populations received 4.94 person-rem from natural background radiation. The 1989 SNL, TTR operations had no adverse impact on the general public or the environment. 18 refs., 2 figs., 14 tabs.

Drillholes H-11b1, H-11b2, and H-11b3 were drilled from August to December 1983 for site characterization and hydrologic studies of the Culebra Dolomite Member of the Upper Permian Rustler Formation at the Waste Isolation Pilot Plant (WIPP) site in southeastern New Mexico. In October 1984, the three wells were subjected to a series of pumping tests designed to develop the wells, provide information on hydraulic communication between the wells, provide hydraulic properties information, and to obtain water samples for quality of water measurements. Based on these tests, it was determined that this location would provide an excellent pad to conduct a convergent-flow non-sorbing tracer test in the Culebra dolomite. In 1988, a fourth hole (H-11b4) was drilled at this complex to provide a tracer-injection hole for the H-11 convergent-flow tracer test and to provide an additional point at which the hydraulic response of the Culebra H-11 multipad pumping test could be monitored. A suite of geophysical logs was run on the drillholes and was used to identify different lithologies and aided in interpretation of the hydraulic tests. 4 refs., 6 figs., 6 tabs.

A computer model for simulating the explosive dispersal of a fuel agent in the far-field regime is described and is applied to a wide variety of initial conditions to judge their effect upon the resulting fuel/air cloud. This work was directed toward modeling the dispersal process associated with Fuel-Air-Explosives devices. The far-field dispersal regime is taken to be that time after the initial burster charge detonation in which the shock forces no longer dominate the flow field and initial canister and fuel mass breakup has occurred. The model was applied to a low vapor pressure fuel, a high vapor pressure fuel and a solid fuel. A strong dependence of the final cloud characteristics upon the initial droplet size distribution was demonstrated. The predicted fuel-air clouds were highly non-uniform in concentration. 18 refs., 86 figs., 4 tabs.

The Vindicator ETW-250 taut wire system combines a physical taut wire barrier with an intrusion detection sensor network. The sensor wires deter and/or slow physical entry into protected areas. The sensors themselves generate an alarm if the sensor wires are pulled, spread, cut, or climbed on. This physical motion is converted into an electrical waveform that is analyzed by the processor. The processor then determines if this motion is within the pre-programmed parameters. If it is not, an alarm is generated through a relay back to the monitoring station. Small changes, such as those caused by temperature, are rejected. Installation and testing are described.

Containment and Surveillance (C/S) equipment, which is used in international safeguards applications, is normally expected to operate unattended within a facility in a host country for extended periods of time. To ensure that this equipment consistently provides high-quality data, the equipment used to ensure the data's integrity must be highly reliable and tamper-resistant. Although designed specifically for use by the International Atomic Energy Agency to comply with the Non-Proliferation Treaty, the equipment has potential applications for both bilateral and multilateral verification schemes for other treaties. This report describes C/S equipment that has been developed by Sandia National Laboratories, and discusses its potential applications. This equipment includes surveillance equipment, seals, monitoring equipment, and authentication equipment. 16 refs., 20 figs.

Waste Isolation Pilot Plant (WIPP) sealing program results are embodied in the initial seal system strategy and reference design. The design provides a common basis for calculations and analyses so that results can be compared directly. The sealing strategy combines both long- and short-term seal components. Crushed salt is the principal long-term barrier to fluid flow. Short-term seal components are used until creep consolidation is sufficient. Concretes developed specifically for WIPP seals and a swelling clay material that exhibits low permeability to WIPP groundwater and brine have been chosen for the short-term components. A body of evidence exists showing the stability of these materials for the length of time they are required to function. Reference designs are described and drawings are shown for each of the principal multi-component seals. Confidence in the sealing strategy and the reference designs resulted from a combination of laboratory tests, numerical modeling, and in situ demonstrations. The sealing strategy, materials, and designs for the WIPP repository are consistent with the concepts and designs proposed previously for other national and international waste management programs. Past accomplishments and planned activities in the sealing program will produce a detailed conceptual design for the seal system and a seal system performance model. 48 refs., 11 figs., 6 tabs.

In the course of communication circuit design at Sandia National Laboratories, a set of communication symbols was created to aid, and hopefully standardize, the design process. These symbols, which allow the designer to build a circuit using black boxes, simplify circuit design and documentation. They also provide a standard set to help minimize interpretation problems among circuit designers. The symbols can be used to represent various devices in a circuit, such as modems, computers, terminals, encryption devices, converters, etc. When using these symbols to design communication circuits, the contours of each symbol show which devices interface together. Mismatch device contours indicate the need for another element (such as a null modem) between the two devices. In addition, the propagation of clock, data, and control signals through the circuit can be represented. Clocking modes on synchronous components (modems, multiplexers, etc.) and signal line crossovers can also be determined from the drawings during the design process. 30 figs.

A series of test has evaluated the current-carrying characteristics of several proposed detonator strong safety link (DSSL) drive cables to conduct current into an electrically simulated radiation case enclosure. The drive cables tested included a dielectric cable made up of either one or two braided Kevlar threads in a polysulfone sleeve, an existing DSSL conductive drive cable similar to a bicycle shift cable, with and without an external ground-strap diversion feature, and the flex circuit hook assembly used for DSSL instrumentation purposes. Each of the test samples was connected to a 200-kV, 30-kA Marx generator and terminated inside an electrically simulated radiation case enclosure. Two lengths of drive cables (4 and 13 in.) within the simulated radiation case were tested for each type. The results indicate that the conductive drive cables without an external short-circuit diversion feature conducted about 5 to 9 times as much current into the simulated radiation case as either the dielectric drive cables or the conductive drive cables with an external short-circuit feature. Surprisingly, the flex circuit hook assemblies, both the short and long cables, conducted nearly 100% of the available current into the simulated radiation case enclosure. The next series of experiments will repeat the tests at the SNL Lightning Facility in order to scale the results up to the maximum lightning threat levels of 200 kA. 18 figs., 1 tab.

The solderability of 60Sn40Pb solder on Kovar was examined as a function of surface-cleaning procedure, flux, and solder-bath temperature. Organic-acid fluxes were more effective at lowering the contact angle than was a mildly activated, rosin-based (RMA) flux on chemically etched Kovar. The contact angles were as low as 29{degree} {plus minus} 5{degree} as compared to 61{degree} {plus minus} 11{degree}, respectively. Varying the solder temperature through the range of 215{degree}C to 288{degree}C caused an insignificant change in the contact angle for the RMA flux and a decrease of the contact angle for a candidate water-based, organic-acid flux. The dilution strength of the flux and the elapsed cleaning time significantly influenced the solder-flux interfacial tension, {sub {gamma}LF}. T-peel strengths of Kovar-60Sn40Pb-OFHC copper joints had a low correlation with the contact angle derived from the solderability experiments. The results of the solderability tests and the T-peel mechanical tests, and subsequence microanalysis of the as-soldered and T-peel samples revealed that the best results for the RMA flux were achieved by using an electropolishing procedure and a solder temperature of 240{degree}C to 260{degree}C. A relatively low contact angle of 31{degree} {plus minus} 2{degree} was observed, with no evidence of cracking or thick-film intermetallic formation at the Kovar-solder interface. T-peel strengths were nominally 9.4{degree} {plus minus} 0.5 {times} 10{sup 6} dyn/cm. 21 refs., 36 figs., 11 tabs.

Parachute system performance issues such a turnover and wake recontact may be strongly influenced by velocities induced by the wake of the delivering aircraft, especially if the aircraft is maneuvering at the time of parachute deployment. The effect of the aircraft on the parachute system is a function of the aircraft size, weight, and flight path. In order to provide experimental data for validation of a computer code to predict aircraft wake velocities, a test was conducted in the NASA 14 {times} 22 ft wind tunnel using a 5.78% model of the B-1B strategic bomber. The model was strut mounted through the top of its fuselage by a mechanism which was capable of pitching the model at moderate rates. In this series of tests, the aircraft was pitched at 10{degree}/sec from a cruise angle of attack of 5.3{degree} to an angle of attack of 11{degree} in order to simulate a 2.2g pullup. Data were also taken for the subsequent pitch down sequence back to the cruise angle of attack. Instantaneous streamwise and vertical velocities were measured in the wake at a number of points using a hot wire anemometer. These data have been reduced to the form of downwash coefficients which are a function of the aircraft angle of attack time-history. Unsteady effects are accounted for by use of a wake convection lag-time correlation. 12 refs., 59 figs., 4 tabs.

This report presents the concept of formalizing the elicitation and use of expert judgment in the performance assessment of high-level radioactive waste (HLW) repositories in deep geologic formations. The report begins with a discussion of characteristics (advantages and disadvantages) of formalizing expert judgment examples of previous uses of expert judgment in radioactive waste programs, criteria that can assist in deciding when to formalize expert judgment, and the relationship of formal use of expert judgment to data collection and modeling. The current state of the art with respect to the elicitation, use, and communication of formal expert judgment is presented. The report concludes with a discussion on potential applications of formal expert judgment in performance assessment of HLW repositories. 93 refs.

As part of a Department of Energy/Commission of European Communities (DOE/CEC) cooperative program, Sandia National Laboratories was asked to develop a portable ultrasonic seal pattern reading system. The system consists of a data acquisition box (DAB), a mechanical reading head, and a portable IBM-compatible PC linked to the DAB by a serial RS-232C communication link. This manual focuses on the DAB subsystem. 8 refs., 13 figs., 8 tabs.

MCPRAM (Monte Carlo PReprocessor for AMEER), a computer program that uses Monte Carlo techniques to create an input file for the AMEER trajectory code, has been developed for the Sandia National Laboratories VAX and Cray computers. Users can select the number of trajectories to compute, which AMEER variables to investigate, and the type of probability distribution for each variable. Any legal AMEER input variable can be investigated anywhere in the input run stream with either a normal, uniform, or Rayleigh distribution. Users also have the option to use covariance matrices for the investigation of certain correlated variables such as booster pre-reentry errors and wind, axial force, and atmospheric models. In conjunction with MCPRAM, AMEER was modified to include the variables introduced by the covariance matrices and to include provisions for six types of fuze models. The new fuze models and the new AMEER variables are described in this report.

The purpose of this report is to summarize for the record the objectives, planning, progress, and documentation of excavating Brine Inflow Room Q and implementing an initial set of Room Q tests. The Room Q tests were designed primarily to test the scale-up accuracy of the current brine inflow model by providing data on brine flow from the host rock salt to a large-scale excavation in the Waste Isolation Pilot Plant (WIPP). Data from these tests will also be used to reduce uncertainties in flow parameters and evaluate proposed mechanistic models. Room Q was excavated with a tunnel boring machine. The initial tests were implemented to measure brine flow parameters and room closure. Pore pressure, permeability, and brine inflow were measured with 15 tools emplaced in boreholes above, below, and on the north side of the room at a station 75 feet into the host rock from the entrance to the room. These measurements were made before, during, and after Room Q was bored to obtain data on the responses in the host rock to the boring process. Closure measurements were started almost immediately after excavation progressed past each measurement station. The designs, timing, sequence, procedures, and as-built records for these tests were documented in Sandia National Laboratories WIPP Quality Assurance files and Westinghouse WIPP Engineering records. 21 refs., 5 figs., 5 tabs.

CTH is a software system under development at Sandia National Laboratories (SNL) to model multidimensional, multi-material, large deformation, strong shock wave physics. One-dimensional rectilinear, cylindrical, and spherical meshes; two-dimensional rectangular, and cylindrical meshes; and three-dimensional rectangular meshes are currently available. A two-step Eulerian solution scheme is used with these meshes. The first step is a Lagrangian step in which the cells distort to follow the material motion. The second step is a remesh step where the distorted cells are mapped back to the original Eulerian mesh. CTH has several thermodynamic models that are used for simulating strong shock, large deformation events. Both tabular and analytic equations of state are available. CTH can model material strength, high explosive detonation, fracture, and motion of fragments smaller than a computational cell. The material strength model is elastic perfectly plastic with thermal softening. A programmed burn model is available for computing the thermodynamic properties of explosive detonation. The Jones-Wilkins-Lee equation of state is available for modelling high explosive reaction products. Fracture can be initiated based on pressure or principle stress. A special model is available for moving fragments smaller than a computational cell with the correct statistical velocity. 7 refs.

A description is given of Sandia's CONCEPT-90 module, which represents a novel type of point-focus photovoltaic concentrator module designed for improved safety, reliability, and performance, and for ease of component fabrication and module assembly. These improvements will combine to decrease the cost of electricity produced by this type of concentrator module. Unique features of the CONCEPT-90 module include encapsulated cell assemblies, simple flat components, and integral use of plastics. The first prototype of this module has been made using back-contact silicon concentrator cells and refractive secondary optical elements. The first prototype module is described, and results from outdoor tests are presented.

The Software Utilities Package for the Engineering Sciences (SUPES) is a collection of subprograms which perform frequently used non- numerical services for the engineering applications programmer. The three functional categories of SUPES are: (1) input command parsing, (2) dynamic memory management, and (3) system dependent utilities. The subprograms in categories one and two are written in standard FORTRAN-77, while the subprograms in category three are written to provide a standardized FORTRAN interface to several system dependent features. 2 refs.

Magnet configurations are found that limit the 6-MeV electrons threatening satellite electronics to <1% of the incident flux. Successful configurations of permanent magnets and electromagnets require magnetic energies of {approximately}8 to 12 kJ to protect each liter of electronics volume. The fundamental strength of materials leads to a required minimum mass of {approximately}48 to 64 kg/liter to support the magnetic pressure. With the electronics requiring {approximately}5 liters, several hundred kilograms are needed for this support. Except for protecting small apertures, magnetic shielding provides little, if any, advantage over that obtained by coating with an equivalent mass using traditional methods. 7 refs., 9 figs., 1 tab.

Until recently, hydrologic characterization in closed sections of boreholes at the Waste Isolation Pilot Plant (WIPP) has relied on measurements of pressure and temperature to establish the permeability of the host geological formations. There were no provisions for monitoring tool compliance and salt creep resulting from borehole closure. The new permeability test tool used to characterize the WIPP underground facility has been equipped with a series of sensors to measure the movement of the tool with respect to the borehole and borehole wall movement. A FORTRAN program can interpret the output data from each test and calculate the change in borehole radius, test zone length, and test zone volume. These values provide a correlation of fluid compressibility and tool compliance with the permeability results derived from the test data. 4 figs., 3 tabs.

The capabilities of a versatile Nd:YAG pulsed-laser system developed at Sandia National Laboratories for solar cell processing applications is described. The results of statistically based, multifactor experiments used to characterize the influence of laser-system process variables on patterns produced in silicon wafers and silicon-oxide layers are presented, and an initial assessment of laser-grooved solar cell processing conditions is given.

AlGaAs/GaAs solar cells are typically characterized as having relatively high interface recombination velocities at the heteroface. Some of the factors influencing the design of solar cell window layers are examined, and the effect of substituting InAlAs/GaAs superlattice alloys and InAlAs bulk alloys in place of AlGaAs is considered. Potential advantages are reduced surface recombination at the heterojunction, reduced thermionic emission into the window layer, thinner window layers, and reduced absorption in the window layer. Theoretical models predict a lower effective surface recombination velocity and a smaller acceptor activation energy for superlattice alloys. Experimental absorption data show that superlattice alloys have a lower absorption coefficient at short wavelengths near the UV roll off.

An accepted technique for simulating pyrotechnic shock inputs has been the resonant plate test. The plate is designed so that its predominant modes generate the desired frequency content of a given shock test specification. The success of the test is dependent on the engineer's ability to effectively design and control the response of the resonant plate. In designing a test to simulated a pyrotechnic environment, the location and mass of the test item become very important considerations since they have a profound impact on the dynamic response of the resonant plate. A relatively massive test item can change the plates's resonant frequency. Differences in the relative frequencies of the test item's fixture and the resonant plate may also effect the input to the test items. In this study, a simple mock test assembly is used to study test item and resonant plate interactions during a test. The implications of this interaction regarding the deviations of the shock test specification are also discussed. Data from shock tests performed with the test assembly mounted to a rigid mounting surface and a flexible resonant plate are compared. Frequency response functions and shock response spectra are generated from the test data and compared to show the significance of: (1) the relative stiffness of the mounting surface; and (2) the location of the input control point during a resonant plate test. These factors are shown to be particularly important in using resonant plate testing to simulate pyrotechnic shock environments.

Spent pressurized-water reactor (PWR) and boiling-water reactor (BWR) fuel rods from three reactors were examined by hot cell periscope, energy dispersive x-ray analysis, and scanning electron micrography. In the case of fuel from the Quad Cities reactor, it was possible to develop a complete particle size distribution. It was found to be log-normal, with a median geometric diameter of 3 μm and a standard deviation of 1.87 μm.

The effects of pressure on the energetics and kinetics of electron emission and capture processes by several important deep levels in Si are discussed. The results yield the first quantitative measures of the breathing mode lattice relaxations accompanying these processes. © 1990, Taylor & Francis Group, LLC. All rights reserved.

Facilities are now coming under Agency safeguards which have large amounts of nuclear material and/or nuclear material which is very difficult to access for reverification. Containment and Surveillance (C/S) technologies may be used to assist in resolution of this problem. This study examines the concept of redundant and independent C/S Systems, and discusses how these systems could be used to lower the need for remeasurement of materials which are difficult to access, or materials included in very large inventories. This paper dose not address increasing levels of C/S measures to protect different types of materials. However, the paper does discuss how redundant and independent C/S Systems will improve the reliability of safeguards information. Equipment which may be used in such systems, and examples of potential systems, are presented. Decisions on how much C/S equipment is enough for a given facility, or type of material, must be made by the inspectorate. 6 refs., 4 figs.

A Level III probabilistic risk assessment (PRA) has been performed for N Reactor, a Department of Energy (DOE) production reactor located on the Hanford reservation in Washington. The objectives of the PRA are to assess the risks to the public and the Hanford site workers posed by the operation of N Reactor, to compare those risks to proposed DOE safety goals, and to identify changes to the plant that could reduce the risk. The scope of the PRA is comprehensive, excluding only sabotage and operation errors of commission. State-of-the-art methodology is employed based largely on the methods developed by Sandia for the US Nuclear Regulatory Commission in support of the NUREG-1150 study of five commercial nuclear power plants. The structure of the probabilistic models allowed complex interactions and dependencies between systems to be explicitly considered. Latin Hypercube sampling techniques were used to develop uncertainty distributions for the risks associated with postulated core damage events initiated by fire, seismic, and internal events as well as the overall combined risk. The combined risk results show that N Reactor meets the primary DOE safety goals and compared favorably to the plants considered in the NUREG-1150 analysis. 36 figs., 81 tabs.

This report discusses the performance of commercial amorphous silicon modules used in photovoltaic power systems from 1985 through 1989. Topics discussed include initial degradation, reliability, durability, and effects of temperature and solar irradiance on peak power and energy production. 6 refs., 18 figs.

This report is the outcome of a study of the technical and procedural requirements which would need to be met if the Agency and facility operators were to agree that under certain circumstances the operator could remove or apply on Agency seal in the absence of an inspector. In the FRG and USA Support Programmes respectively an electronic seal (VACOSS) and a CCTV system (MIVS) have been developed. Through a joint project, an interface has been demonstrated which enables the seal data to be superimposed upon the surveillance data. This interface is briefly described in the appendix. A proposed application for this integrated system is to allow facility operators to carry-out some of the seal procedures normally performed by an inspector, thereby reducing the need for inspector presence at certain crucial times.

Thermal battery functional test data are stored in an HP3000 minicomputer operated by the Power Sources Department. A program was written to read data from a battery data base, compute simple statistics (mean, minimum, maximum, standard deviation, and K-factor), print out the results, and store the data in a file for subsequent plotting. A separate program was written to plot the data. The programs were written in the Pascal programming language. 1 tab.

This document describes the Nuclear Weapons Complex (NWC) detached'' CIM file header. The file header concept is defined and its form and content are specified. Guidelines for the use of file headers by the CIM community in the NWC are also included. This document is the result of the combined efforts of the Lead Laboratory and the NWC File Header Subgroup. It has evolved through a process of cooperation and compromise and represents a consensus view of the NWC.

At Sandia National Laboratories data engineering is the application of both the art and science aspects of engineering principles to the acquisition and storage of product-related test and traceability data and to the transformation of this data into useful information through data retrieval and analysis processes. This report describes the application of data engineering to the data systems that have been developed in support of production agency built or procured product. The production agencies that are addresses in this report include Mason Hanger, Amarillo, TX; GEND, Largo, FL, Allied Signal, KCD, Kansas City, MO; and Mount, Miamisburg, OH. Also discussed is the Weapon Evaluation Test Laboratory (7264)/Amarillo. The scope of the data engineering program for each production agency (or test facility) is presented along with the interfaces and constraints. The present contractors' data system is described and system limitations and future plans are discussed. 7 refs., 38 figs.

BUCKL is an inexpensive x-ray deposition computer code which considers one-dimensional transport and accounts for two-dimensional effects in a buckling approximation. This manual contains input instructions and sample input.

A variety of geomechanical analyses are presented that support the WIPP project. The scale of the analyses ranged through laboratory experiments, small-scale in-situ tests, large-scale in-situ tests, underground rooms, shafts and shaft keys, and multi-room panels. The structural behavior of underground rooms, shafts, and experiments was investigated using the finite element method. Both two and three dimensional analyses simulated the time-dependent behavior of the salt host rock. Two different constitutive models were used to represent the creeping motion of the salt. The investigations aided in experimental planning, code validation, and assessing excavation responses for safety and performance assessment. This report compiles ten different structural analyses which assess the performance of excavations and experiments located at the Waste Isolation Pilot Plant (WIPP) in Carlsbad, NM. Chapter 2 discusses the constitutive models used to represent the salt behavior. Each of Chapters 3 through 12 presents an analysis. Chapter 13 concludes the report. 36 refs., 48 figs., 17 tabs.

An interactive computerized and automated system to provide environmental control for atmospheric corrosion experiments has been added to the FACT, as well as computerized data acquisition for sample weighing. The FACT allows control of corrosive gas concentrations to simulate industrial atmospheric conditions and requires constant manual adjustment to provide a stable test environment. Because constant manual adjustment is impractical, we have automated this facility to achieve the desired stability. This system incorporates an IBM PC AT using Keithley's Series 500 hardware and Quick500 software development environment to calibrate gas analyzers, and to monitor exposure time, test chamber temperature, and gas concentrations. A second PC has been connected to a Mettler M3 microbalance through an IEEE-488 interface communicating under Lotus Measure. Weighings with a sensitivity of 1 {times} 10{sup {minus}6} gram are transferred directly into a Lotus 123 spreadsheet where the data can then be easily manipulated and plotted. Under computer control, the FACT can now run unattended for more than a week and maintain much better control over gas concentrations (200 {plus minus} 5 ppb and 10 {plus minus} 0.5 ppb for NO{sub 2} and H{sub 2}O and H{sub 2}S, respectively) than was possible with manual control (100 {plus minus} 25 ppb for either gas), after initial stabilization. 9 figs.

The Linear Explosive Shaped Charge Analysis (LESCA) code is used to analytically model and optimize the design of a linear shaped charge (LSC). A variety of LSCs are initially modeled with the LESCA code, and the predicted jet penetration versus standoff data are compared to experimental data. The LSCs varied in explosive loading size form 600 to 10,500 grains per foot. The LSC liner material for this study was cooper. The variables optimized in this study included the LSC apex angle, liner thickness, explosive width, and explosive width, and explosive height. 8 ref., 24 figs.

The PCP PHEMTO-CHEM 100 ion mobility spectrometer (IMS) exhibits a number of characteristics that affect its performance for the quanititative and qualitative analysis of explosives in solution and in the gas phase. These characteristics, as well as modifications to the system that will either eliminate, or reduce, the extent of some problems associated with these characteristics, are described. Also described are other aspects of the operation and performance of this system. 9 refs., 10 figs., 1 tab.

This report discusses the purpose and requirements that were established for the data logger at the 34-m diameter, research- oriented vertical axis wind turbine, the Test Bed, which Sandia National Laboratories built at Bushland, Texas. The data logger is a minicomputer-based system that collects data from 35 channels, displays the collected data, and records them on a hard disc. Both the hardware and software that make up the data logger are also described, and the operator's instructions and the operating system commands and procedure files are appended. The data logger is used to obtain long-term data to characterize the wind at the site of the turbine, record the performance data of the control system, obtain a continuous record of events at the test sire, consolidate displays for the test engineer, and provide a display of current information for visitors to the site. 7 refs., 3 figs., 4 tabs.

Analytical equations for barrel-tamped explosively accelerated flyer plates are used to generate graphical solutions to flyer problems. Given the problem geometrical dimensions, explosive weight, detonation velocity, explosive exponent, barrel-tamping weight, and flyer weight, the graphical representation of the calculated data allows for a fast approximation of the final or maximum flyer plate velocity. Graphically obtained flyer velocities are compared to experimentally published data. The graphical solution for flyer velocity is particularly useful when a computer is not available. The graphical representation of the various barrel-tamped flyer parameters results in a parametric study which illustrates the effect on final flyer velocity in varying parameters. The graphical analysis scheme can be used with any explosive, tamper and flyer materials. 15 refs., 12 figs., 4 tabs.

This report presents the results of numerical modeling of the electron beam generation, transport, and conditioning in the Sandia accelerators RADLAC, IBEX, and RLA for the year 1989. The codes used were the particle code MAGIC, the trajectory code TRAJ, and some preliminary work with the 3-D code Quicksilver. The results are mostly in the areas of injector design, beam propagation in IFR channels and B{sub {Theta}} cells, and emittance measurements. The energy range of these electron beams is from 1 MeV to 20 MeV. 16 refs., 42 figs.

Finite-difference time-domain (FDTD) codes can, in principle, be used to determine the electromagnetic response of complex scatterers. However, the extent to which structural details can be accommodated is limited by computer resources and one's ability to specify necessary parameters. By embedding into the FDTD code alternative numerical methods that solve the aspects of the problem which are not practical, or possible, for the FDTD code to handle, power and flexibility can be added. This report investigates three such hybrid schemes. Topics include: (1) embedding a transient multiconductor/circuit-analysis code so that coupling down to the component level can be directly computed; (2) the effectiveness of using a multiconductor transmission-line code to analyze shielded multiwire cables in FDTD calculations; and (3) the effectiveness of using two-- and three-- dimensional aperture transfer functions to model narrow apertures in FDTD formulations. These topics were selected because of their immediate need in system assessments. Experimental measurements and/or alternative solution methods are used to verify the hybrid approaches. 56 figs.

In past five years, Department 1510 has developed a state-of-the-art Aerosol Dynamics Laboratory (ADL). This report documents the current instrumentation and capabilities that exist in this laboratory. The ADL was developed from a variety of sources, with a primary contribution from Department 1510's Independent Research and Development program in aerosol dynamics. Current capabilities of the ADL include: (1) generation of calibration-quality monodisperse particles with diameters between 0.005 to 100 {mu}m, (2) real-time measurement of particle size distributions for particle diameters between 0.01 and 100 {mu}m, (3) in situ, real-time measurement of particle size distributions for particle diameters between 0.3 and 100 {mu}m, and (4) real-time measurement of particle charge distributions for particle diameters between 0.01 and 1.0 {mu}m. 14 refs., 5 figs.

Analyses related to the Supplemental Environmental Impact Statement and preliminary performance assessment studies have suggested that alteration of the method of waste emplacement in the Waste Isolation Pilot Plant (WIPP) may be necessary in order to satisfy waste storage regulations. Good engineering practice also dictates consideration of changes which are useful for better containment of waste. This report presents a preliminary evaluation of various engineered modifications that might be considered. The report is based on work that has been ongoing at Sandia National Laboratories since FY88, before formation of the present Engineering Alternative Task Force by the Department of Energy WIPP Project Office. The engineered modifications under consideration are described and characterized in the first part of the report according to: the objective that would be addressed by their application; their level of complexity; and some of the presently understood limitations and uncertainties of their use. Results of studies conducted to date to examine the feasibility of some of the modification concepts are presented, with emphasis on the effects of waste supercompaction.'' 21 refs., 14 figs., 5 tabs.

When the Morton Salt Mine in Weeks Island, Louisiana was converted into a strategic Petroleum Reserve oil reservoir, massive concrete bulkheads were installed to seal the access shafts against oil or water leakage. Recent inspection of these bulkheads has raised questions about their ability to perform satisfactorily in the event of a catastrophic water leak into the mine. Calculations are reported here which examine the response of the five bulkheads to a worst-case scenario of flooding by brine from the surface into the oil reservoir below the bulkheads. These calculations show that, under conservative analysis assumptions, factors of safety under such a load for the bulkheads sealing the service shaft and the two raisebores are close to 1. The Markel incline and production shaft bulkheads exhibit safety factors in excess of 2 and 3, respectively. 10 refs., 24 figs., 3 tabs.

A seismic signal processing procedure is designed so that its performance is optimized for a specific seismic array looking for explosions at a specific teleseismic location. In this report we first describe the processing procedure, which essentially estimates beamformer signal power as a function of time in a specified frequency band. Then we calibrate the procedure for the Norwegian Regional Seismic array (NRSA) in terms of equivalent body magnitude'' (emb) level versus signal power using US Department of Interior/Geological Survey (USGS) epicenter data from documented explosions at the USSR Semipalatinsk test area in Eastern Kazakh. Finally, we test the performance of the procedure on actual NRSA data and estimate that explosions above approximately mb 4.0 at Semipalatinsk correspond with an event rate in the emb signal on the order of one to ten events per hour. We conclude that, to detect and analyze events around the clock at levels below mb 4.0, an automatic event locator must be used to process the output of the procedure described here. 8 refs., 19 figs., 1 tab.

This interim report provides results of the molten salt pump and valve loop testing, lessons learned, and recommendations based on the test results to date. The molten salt pump and valve test loop is intended to demonstrate the effectiveness of full-scale hot and cold salt pumps and valves. The pump and valve testing consists of two pumped loops, one to simulate the hot side of the receiver (565{degree}C, referred to as the hot loop) and one for the cold side (285{degree}C, referred to as the cold loop). Each loop contains a pump and six representative valves scaled for a 60-MW{sub e} commercial solar power plant using molten salt heat transport fluid. The test loop is part of the Molten Salt Subsystem/Component Test Experiment (MSS/CTE), which is being conducted to reduce the technical risk of building and operating commercial solar central receiver plants. The project, managed by Sandia National Laboratories (SNL) with Babcock and Wilcox (B W) as the prime contractor, is cost shared by DOE and six contractors. The hot loop has operated over 2400 hours in the fully automatic sequence mode. The last 500 hours have been through continuous 24-hour, 7-day operation. The hot pump operation hours simulate over 2 years of pump cycles. The cold loop has operated 12 hours in the manual mode; this is because of problems caused in the manufacturing of the pump and motor. 9 refs., 6 figs., 1 tab.

Sandia National Laboratories operates the Primary Standards Laboratory (PSL) for the Department of Energy, Albuquerque Operations Office (DOE/AL). This report summarizes metrology activities that received emphasis in the second half of 1989 and provides information pertinent to the operation of the DOE/AL system-wide Standards and Calibration Program. 7 refs.

The technology that led to very large-scale integrated circuits on silicon chips also provides a basis for new microsensors that are small, inexpensive, low power, rugged, and reliable. Two examples of microsensors Sandia is developing that take advantage of this technology are the microelectronic chemical-sensor array and the radiation-sensing field-effect transistor (RADFET). Increasingly, the technology of chemical sensing needs new microsensor concepts. Applications in this area include environmental monitoring, criminal investigations, and state-of-health monitoring, both for equipment and living things. Chemical microsensors can satisfy sensing needs in the industrial, consumer, aerospace, and defense sectors. The microelectronic chemical-sensor array (Figure 1) may address some of these applications. We have fabricated six separate chemical gas-sensing areas on the microelectronic chemical-sensor array. By using different catalytic metals on the gate areas of the diodes, we can selectively sense several gases. 14 refs., 12 figs.

The characteristics of transportation cask surface contamination and the weeping'' phenomenon are reviewed. In addition, literature that pertains to the possible impact of surface contamination on repository operations is reviewed. This report consists of commentary on and rather extensive excerpts from the published literature on cask surface contamination that may have a bearing on repository risk assessment. In addition, estimates are made of the quantity of contamination that might be present on a cask. These estimates are used to calculate the direct exposure rates to personnel located at several distances from the cask. 15 refs., 15 tabs.

Sandia National Laboratories has conducted research and development in the area of enhanced or unconventional natural gas recovery since the mid-1970's. This report is a compilation, in chronological order, of the formal documentation that has resulted from that work. Since its inception, this R D has covered five general areas, which evolved in roughly the following order: instrumentation, mineback experimentation, propellant fracturing, multiwell experiment, and geoscience. The Department of Energy's U:nconvetnional Gas Program has been the predominant sponsor ofthe work represented in this bibliography. All entries of this bibliography are reports, papers, and abstracts which are available publicly -- either in published journals or as reports available through the National Technical Information Service, US Department of Commerce, 5285 Port Royal Road, Springfield, VA 22161. The Journal of Petroleum Technology and other Society of Petroleum Engineers publications contain many of the journal papers. Sandia National Laboratories reports are the majority of the published reports. Abstracts are included only if they were published.

Preliminary results for the parametric dependences of the 2.63 and 2.65 {mu}m lines of a high-pressure xenon laser are given. The power deposition is varied from 200 to 800 W/cm{sup 3} for gas mixtures of Ar(830 Torr)/Xe(4 Torr), Ar(750 Torr)/Xe(83 Torr) and Ar(621 Torr)/He(210 Torr)/Xe(4 Torr). The 2.65 {mu}m line dominates the 2.63 {mu}m line for all gas mixtures and the ratio of the 2.63 {mu}m line intensity to that for the 2.65 {mu}m line is suppressed by the higher concentration of xenon. 13 refs., 4 figs.

This manual describes the procedures for implementing IMPACT-BRC Version 2.0. IMPACTS-BRC is a generic, radiological assessment code intended to be used by the US Nuclear Regulatory Commission (NRC) to evaluate petitions to classify specific waste streams as below regulatory concern (BRC). The code is designed to demonstrate compliance to BRC standards by modeling and calculating annual radiological impacts to the maximal individual, critical groups, and the general population as the result of transportation treatment, disposal, and post-disposal activities involving low-level radioactive waste. Impacts are calculated for multiple nuclides and pathways depending on data input and treatment and disposal options specified by the code user. The treatment and disposal options include onsite incineration, offsite incineration at municipal and hazardous waste landfills. Included within the disposal options is the ability to calculate impacts from the sorting and/or recycling of metal containers and metal and glass materials. Nuclide-specific accounting is provided to facilitate identification of the critical nuclides and pathways contributing to the impacts. Default environmental and facility parameters are developed from reference treatment/disposal sites. The user has the option to replace default parameters with site-specific parameters to provide more realistic estimation of impacts. 8 refs., 10 figs., 44 tabs.

The split cavity oscillator is a resonant cavity device which can be used to highly modulate the current of a relativistic electron beam for the purpose of generating high power microwaves. It consists of a cylindrical cavity resonator which has been divided into two identical cavities by a conducting foil whose radius is less than the inner radius of the cylinder. The gap between the foil endpoint and cylinder walls forms an annular slot which couples the cavities electromagnetically. Using a particle-in-cell code, we have performed a numerical investigation of SCO structures driven by high current, magnetized, annular, relativistic electron beams. Results are presented which illustrate the dependence of current modulation efficiency and oscillation frequency on injected beam current density. In addition, simulation results are presented for a new, double-foil SCO which indicate significantly enhanced performance in comparison to the single-foil device. 10 refs., 10 figs., 2 tabs.

The purposes of this one day meeting were to identify and to consolidate the issues associated with the performance of dimensional measurement systems as indicated by the results of the DOD Quality Assurance Council, the National Science Foundation, the Rich Walker GIDEP Alert, the B89 Standards Committee's work, IMOG Measurement Technology Subgroup discussions, NIST, and the CAM-I DITS (Dimensional Inspection Technologies Standards) Project. The expected results were a clearer definition and understanding of the problems, establishment of objectives for problem resolution, an approach to resolve the problems, and the identification of potential funding requirements and sources. 10 figs.

The Hypersonic Arbitrary-Body Aerodynamics (HABA) computer program predicts static and dynamic aerodynamic derivatives at hypersonic speeds for any vehicle geometry. It is intended to be used during conceptual design studies where fast computational speed is required. It uses the same geometry and hypersonic aerodynamic methods as the Mark IV Supersonic/Hypersonic Arbitrary-Body Program (SHABP) developed under sponsorship of the Air Force Flight Dynamics Laboratory; however, the input and output formats have been improved to make it easier to use. This program is available as part of the Department 9140 CAE software.

Part 1 of this review deals with the effects of ionizing radiation on glass in the absence of hydrogen and should be consulted for background information not repeated in Part 2. This part includes information on the behavior of hydrogen in glass and how it is affected by experimental variables such as temperature, pressure, and glass composition. The reaction of hydrogen with irradiated glass is treated next, and finally the effects of ionizing radiation on hydrogen-impregnated glass are summarized. 51 refs., 1 tab.

This report documents the software developed to characterize tuning fork resonators used in the Quartz Digital Accelerometer. The results, after characterizing numerous resonators, indicate a resonant frequency sensitivity to input drive level. Also, the resonant frequency increased for some of the tuning fork resonators but decreased for others. The characterization process used to obtain these results is summarized. 4 refs., 14 figs.

A two-part polyurethane foam supplied by Poly Plug, Inc., has been tested in the laboratory and in the field to assess its utility in controlling lost circulation encountered when drilling geothermal wells. A field in The Geysers was conducted, based on earlier laboratory work that showed the foam chemical formulation to be capable of expanding under elevated temperatures and pressures to form a rigid, impermeable polymer that should be effective in plugging fluid-loss zones. Although the downhole tool used to deploy the foam chemicals apparently functioned properly in the field test, the chemicals failed to expand significantly downhole, instead forming a dense polymer that may be ineffective in flowing into and sealing loss zones. Subsequent laboratory tests were conducted under simulated downhole conditions to determine the cause of the polymer's failure to sufficiently expand. The results indicate that the foam chemicals undergo vigorous mixing with water in the wellbore, which disturbs the kinetics of the chemical reaction more than was previously contemplated. The results indicate that without significant changes in the foam chemical formulation or delivery technique, the existing foam system will be ineffective in lost circulation control except under very favorable conditions. 6 refs., 46 figs., 7 tabs.

To assist in the repair of the Modular Integrated Video System (MIVS) printed circuit boards, a maintenance or service manual is essential. This manual provides a simplified overview of each PC board and explains the functions of each component. Setup procedures and parts lists for each board are included to minimize the task of aligning the boards and identifying replacement parts.

The Plasma Opening Switch (POS) designed for use on PBFA-2 was operated on the Blackjack 5 generator at Maxwell Laboratories in early 1988. Various switch configurations were tested, with the overall goal of understanding the point at which the switch begins to open, and improving uniformity of opening. Improved load current rate-or-rise and current transfer into high impedance loads were also goals. A baseline-design POS appears to have produced results similar to those seen in an earlier test series of this hardware on Blackjack 5 in 1986. Addition of a second-stage opening switch yielded improvements in the areas mentioned above. Analysis of current signals indicates that switch opening in all geometries was characterized by significant power flow asymmetry downstream of the POS. This report is an analysis of data from this test series.

This MIVS instruction manual provides a detailed description of all the capabilities that this system can perform. It provides step by step instruction for setting up the system parameters and the procedure for initiating surveillance. This information complements the training received prior to field operation of this system. 6 figs., 13 tabs.

The effects of ionizing radiation (e.g., beams of electrons of {gamma}-radiation) on silica and borosilicate glasses are summarized in this review article. In Part 1, irradiation in the absence of hydrogen is considered. The combined effects of hydrogen and irradiation are treated in Part 2. Descriptions and, if available, mechanisms of changes in the glass properties are discussed. Several experimental variables which may affect the outcome of an irradiation procedure are also outlined. 47 refs.

An elastic/plastic material model has been developed for use with the suite of Sandia Engineering Analysis Department finite element codes. This model describes post-yield strain hardening by a power law equation involving the equivalent plastic strain and includes a yield plateau or Lueders strain region. This combination of power law hardening and Lueders strain accurately represents the mechanical behavior of a large number of commonly used engineering materials. The material model is vectorized to take advantage of current super-computer architecture. The model shows only a modest increase in CPU time over the linear hardening material model currently in the codes. Several example problems are presented to show the accuracy and flexibility of the elastic/plastic power law hardening model. 12 refs., 10 figs., 3 tabs.

In this document, masses of the STAR-C power system and an optimized out-of-core thermionic reactor (OTR) power system versus power level are investigated. The impacts of key system parameters on system performance are also addressed. The STAR-C is mass competitive below about 15 kWe, but at higher power levels the scalability is relatively poor. An optimized OR is the least massive space nuclear power system below 25 kWe, and scales well to 50 kWe. The system parameters that have a significant impact on the scalability of the STAR-C are core thermal flux, thermionic converter efficiency, and core length to diameter ratio. The emissivity of the core surface is shown to be a relatively unimportant parameter. For an optimized OR power system, the most significant system parameter is the maximum allowable fuel temperature. It is also shown that if advanced radiation-hardened electronics are used in the satellite payload, a very large mass savings is realized. 10 refs., 23 figs., 7 tabs.

ANEOS is an in-line software package which provides thermodynamic information for shock physics codes. Solids, liquids, vapors, plasmas and phase mixtures are considered in a thermodynamically consistent and complete manner. The package is flexible and easy to use. This users manual contains input instructions, examples, and descriptions of user output. 14 refs.

Techniques for propagating data and parameter uncertainties in high-level waste (HLW) repository performance assessment models are discussed. Uncertainty analysis techniques techniques ascribe quantitative measures of reliability to model predictions. Both 10 CFR 60 and 40 CFR 191 require consideration of uncertainties, including uncertainties in data and parameters, in the performance assessment of an HLW repository system. Four categories of uncertainty analysis methods are discussed: Monte Carlo simulation, replacement models (response surface techniques), differential techniques (direct, adjoint, and Green's function technique), and geostatistical techniques (stochastic modeling using Monte Carlo simulation and spectral analysis). Advantages, disadvantages and applications of each technique are presented. Propagation of uncertainties through multiple, linked models is also discussed. Application of these techniques to sensitivity analysis is also presented. Sensitivity analyses can be useful to uncertainty studies because the number of parameters included in the uncertainty analysis can be reduced by eliminating those parameters for which the uncertainty has a minimal effect on the performance variable(s).

For improved reliability and safety, nuclear power plants are designed with redundant safety systems, many of which also have redundant trains of equipment within the system. However, the very high reliability theoretically achievable through the use of redundancy is often compromised by single events that can individually render redundant components unavailable (common cause failure (CCF) events). As evidenced by the results of probabilistic risk assessments (PRAs) and by historical experience with nuclear power plant operations, CCF events are usually major contributors to the risk posed by nuclear power plant operation. Thus, it is important that PRAs recognize the potential for CCF events and realistically account for CCF contributions to system unavailability and plant risk. Much progress has been made over the years in the area of CCF analysis, including the development of both qualitative analysis methods. Until now, however, CCF methodologies have not explicitly and systematically accounted for the impact of plant-specific defenses, such as design features and operational and maintenance policies, in place to reduce the likelihood of failure occurrences at nuclear power plants. Recognizing the importance of this issue, the NRC has funded a research effort that has focused on developing the cause-defense methodology for CCF analysis and prevention. This report presents the results of this research. Specifically, this report discusses the development of (1) procedures for identifying the potential for CCF events at individual nuclear power plants and (2) cause-defense matrices for analysis of CCF events. Also, new concepts and more precise definitions are introduced to enhance CCF terminology and interpretation of historical event data. Contains 35 refs., 8 figs., 32 tabs.

The performance and availability of the five basic identity verifiers can now meet the requirements of most physical and information security needs. However, with the lack of any evaluation standards, the independent testing of verifiers requires care with due consideration for both parts of the verifier systems; the verifier hardware and software and the user with his biometric features which is the least consistent part of the system. The method of testing and data processing must be done with care and should be reported along with reduced results.

Integrated access control portals (booths) are fast becoming a familiar part of medium-to-high security systems. Facilities wishing to expand their operations or to tighten their security, while at the same time limit or reduce their security operating expenses, find the application of portals to be a cost-effective alternative to manned entry points. With the advent of microprocessors and commuter control, portals may now be designed to operate in an automated (and in some cases, stand-alone) mode, requiring human intervention only in the event of an alarm condition. Because human intervention is minimized, a single guard can monitor the operation of several portals and thereby control multiple entry points. This report presents a description of a typical portal and its functioning and provides the information necessary to formulate a set of portal requirements. 8 figs.

The PCP, Inc. Large Reaction Volume ion Mobility Spectrometer (LRVIMS) was characterized and evaluated for use as a contraband explosives vapor detector in personnel and package portal screening applications. The limit-of-detection was found to be a constant {approximately}0.3 PPT experimentally and in calibrations using a Thermedics RDX generator. The minimum LOD in terms of RDX vapor molecular flow rate was {approximately}1.8 {times} 10{sup 9} molecules/sec at 16.6 L/min airflow through the 100 cm{sup 2} square tube area of this ion mobility spectrometer. Samples of 0.5 gm of TNT in plastic bags in the center of the personnel screening portal were easily detected. Bomb quantity (8 oz) samples of TNT and Comp B (40% TNT, 60% RDX) were also detectable in the personnel portal configuration. No detections of RDX were possible in any position of either C-4 or Comp B or of PETN in Detasheet or Det Cord. Operation in the presence of observed background interferants, operation at very low airflow rates, and proposed operation in conjunction with preconcentrators, also are described. 14 figs.

This status report presents preliminary analyses of flow through the rooms, drifts, seals, and shafts of the Waste Isolation Pilot Plant (WIPP). The purpose of these analyses is to evaluate the importance of various components and parameters of the transuranic waste repository. These analyses are presented to show the current status of repository/shaft system modeling, and to provide input for evaluating proposed engineered modifications to the waste and rooms to ensure compliance with the Environmental Protection Agency's Environmental Standards for the Management and Disposal of Spent Nuclear Fuel, High-Level and Transuranic Waste. Detailed descriptions are given for nine computational models of the WIPP repository for either undisturbed or human intrusion conditions. Some models are refined versions of earlier models; others include rudimentary studies of an additional phenomenon, flow of generated gas. The models of an undisturbed repository substantiated the results of earlier models by showing that no waste leaves the vicinity of the disposal area in 10,000 yr. The models that studies gas flow agreed with this position; however, the models are too rudimentary to permit conclusive statements. The five models of the human intrusion event explored the importance of parameters that influence the flow of brine through the waste, establishing a base for understanding the behavior of the waste disposal rooms, drifts,and interbeds in the host rock. 63 refs., 92 figs., 29 tabs.

In 1981 the Waste Isolation Pilot Plant (WIPP) Project, under the direction of the US Department of Energy (DOE), began construction of a facility in southeastern New Mexico to develop the technology for disposing of radioactive waste from the defense programs. This facility may eventually become a repository for defense Transuranic (TRU) wastes, provided that the facility is demonstrated to be acceptable. Although the complete facility includes both surface and underground construction, the Repository Isolation Systems Division of the Nuclear Waste Technology Department at Sandia National Laboratories (SNL) is primarily concerned with development of the underground portion of the facility; we focus on that portion of the facility in this report. This report is specific to the Thermal Structural Interactions (TSI) in situ tests of the Experimental Area and is one of a series intended to document the data obtained from the TSI in situ tests and to make these data available to potential users. 32 refs., 60 figs., 29 tabs.

The equilibrium swelling of silicones, fluorosilicones, VITON and ethylene-propylene-diene (EPDM) elastomers in an environment of the jet fuel JP4 was investigated. The volume of silicone and DPDM elastomers increased by approximately 100% when they were placed in a saturated environment of JP4. Conversely, the volume of the fluorosilicone elastomer increased by approximately 15% and that of VITON less than 1%. In acetone, a commonly used solvent, the equilibrium swelling of VITON and the fluorosilicone elastomer was excessive, on the order of 100%, wheras the silicone and EPDM elastomers exhibited small changes in dimensions. Reasons for these observations are discussed in detail. We also present a simple scheme by which one may, qualitatively, determine the dimensional stability of these elastomers in different solvents if the cohesive energy density of the solvent, which is readily available in a number of handbooks, is known. We also evaluated the vulnerability of some commonly used engineering thermoplastics to JP4. The results are tabulated. 13 refs., 6 figs., 3 tab.

An understanding of dispersal of nuclear materials from an explosive event is needed to support design studies of weapon storage and transportation. Assessing the consequences and requirements for cleanup of a fire or nonnuclear detonation of a system containing nuclear material requires knowledge of the aerosol formation process. Information about the aerosol chemical composition, the physical size and shape of the particulates, as well as the efficiency of aerosol formation ate needed to conduct meaningful assessments. This report describes laboratory tests to study aerosol from materials of interest. An electromagnetic launcher is used to heat and propel molten metallic samples under energetic high-velocity conditions. We describe the apparatus and first results from tests using uranium-molybdenum alloy samples. Contained laboratory-scale measurements are described that determine aerosol morphology, chemical composition, and aerosol formation efficiency under high-velocity conditions. Data from the launcher tests describe (1) the aerodynamic breakup process of high-velocity molten liquid into droplets, and (2) the formation of still finer aerosols by combustion of these droplets at high velocity. The measurements show efficient aerosol production in air that is dominated by the formation of fine chain-agglomerate combustion aerosol. Particle morphology information for both the chain agglomerate and the less common liquid breakup products is described. The aerodynamic breakup of the liquid sample material is described. Lognormal distributions are shown to accurately represent the data. The geometric mean diameter is related to the mass mean diameter and maximum stable droplet diameter for the distributions. 28 refs., 27 figs., 3 tabs.

Several potential incident scenarios involving the accidental release of radioactive material at five reference, nonreactor nuclear material licensees are analyzed in this report. The economic risk ($/licensee/yr) of decontamination is evaluated for each reference licensee. Although most releases and cleanup costs are minor, some less frequent incidents may result in very high cleanup costs that dominate the economic risk of decontamination of a particular licensee. The economic risk for the 5 plants ranged from a low of $14,000 per licensee per year to a high of $104,000 per licensee per year. This report is the second of two reports by Sandia National Laboratories on the economic risk of nonreactor nuclear material licensee operations. 40 refs., 21 figs., 31 tabs.

Both the US Environmental Protection Agency (EPA) and the US Nuclear Regulatory Commission (NRC) have promulgated regulations regarding the performance of geologic repositories for the disposal of high-level nuclear waste. One of the responsibilities of the US Department of Energy (DOE) is to demonstrate compliance with the appropriate regulations. The DOE will most likely use extensive numerical modeling to show compliance with the various quantitative requirements. These analyses will then be evaluated by the NRC. There are different levels of evaluation: peer review, conservative estimates,used of existing models/codes, and development of models/codes by the NRC. The intensity of the review will vary from analysis to analysis, depending on the importance of the analysis, the acceptability of the conceptual model behind the analysis and the solution technique used, and the potential for increasing confidence in the system description, should the NRC decide to develop its own models/codes. An appropriate level of review can be determined by applying these four criteria in a specific manner. 24 refs.

This report examines the computational implementation of a continuum model for jointed rock media. The jointed rock model uses strain partitioning between the elastic rock matrix and joint sets with nonlinear normal and shear responses. A specific model using a rational polynomial to describe normal joint response was first used as the basis for a computational implementation of a jointed rock model for two-dimensional problems. This particular implementation can be extended to three dimensions, but it would be a very expensive material model from a computational standpoint. The problem of trying to implement a joint model in three dimensions so that it would not be an extremely expensive computational tool has led to a study of various computational implementations of joint models for two-dimensional geometries. These studies have produced implementations of joint models that are very computationally efficient and that can handle joint models with normal joint behavior described by general relations. The implementations studied in this report make the use of jointed rock models in three dimensions much more feasible in terms of computational expense. 6 refs., 8 figs., 2 tabs.

Thermal imagers are effective tools for detecting aggressive actions and enhancing physical security in both tactical and peacetime environments. However, from an operator's perspective, these devices are rarely used on a continuous basis because of inconvenience and a requirement to have the operator be the detector'' while using the imager as a sensor. This paper describes an area sensor and assessment system designed to reduce operator fatigue and improve the effectiveness of costly thermal imagers. Several prototypes have been installed and operated at sites worldwide. The device uses a thermal imager as the primary sensor but also incorporates a laser rangefinder, automatic area precision scanning, robust scan-to-scan scene change detection, a deliberate-motion detection features. The system setup, control, and alarm assessment functions of the operator console are described. The digital processing is discussed and performance measures are given. 2 refs., 7 figs.

This report describes the development of the following new catalytic materials based on hydrous metal oxide (HMO) ion exchange materials: Na-Ti, Nb, Zr, and mixtures of hydrated silica with hydrous Ti-oxide. HMO's provide a versatile system for the preparation of heterogeneous catalysts. The preparation chemistry allows synthesis of catalysts that can be tailored to particular processes with respect to both chemical and physical properties. Bulk catalysts with surface areas over 300 m{sup 2}/g and pore volumes up to 0.4 cc/g as well as thin films of the HMO materials can be prepared on supports having a wide range of catalytically important physical properties. This report, the first of two parts, presents research performed to date regarding the preparation chemistry, and physical and chemical properties of HMO materials which may be used to develop heterogeneous catalysts for direct coal liquefaction processes. During the course of this work, new ideas for research areas relative to direct coal liquefaction were briefly explored. Two of them that merit further work, catalyst-anchored hydrogen donors and alkoxide-derived crystalline titanate compounds, are briefly described. 25 refs., 34 figs., 8 tabs.

Drillholes H-17 and H-18 were drilled at the WIPP site to assess uncertainties in site hydrologic parameters and to serve as monitoring points for planned hydrologic tests. H-17 was drilled south of H-11 and east of P-17 to evaluate the existence of a high-permeability region in the Culebra Dolomite Member that had been indicated by groundwater-flow modeling and surface geophysical surveys. H-18 was drilled north of H-2 to help reduce the uncertainties of boundaries between high and low transmissivities and fluid density that had been identified by drilling and by modeling. 1 ref., 4 figs., 6 tabs.

An extensive literature review has been conducted as part of an effort to quantify the fidelity of Sandia's lightning burn-through simulation technique. The dominant parameters affecting damage have been identified and are discussed. Two alternative techniques for qualitatively improving the Sandia simulation have been identified, but quantification of the correlation of the results of each with those of natural lightning awaits completion of further experimental work. A systematic set of laboratory experiments is proposed to assess the sensitivity of each technique to key simulation parameters. An available calibration linkage to natural lightning is the reproduction of damage spots that were created by lightning on a set of copper disks mounted on TV towers, and an attempt to do this is included in the proposed experiments. In order to reduce the uncertainties of this approach, more lightning-spot data are required, along with records of the flash currents that produced them. It is recommended that such data be acquired in conjunction with the Rocket-Triggered Lightning Program being conducted each summer at the Kennedy Space Center. 25 refs., 5 figs., 1 tab.

The inverse triax diode is a high power, low impedance electron diode which offers significant advantages over conventional electron diodes on short-pulse (<30 ns FWHM) high power x-ray simulators. Parametric calculations show that the radiation efficiency of the inverse triax is competitive with standard diodes fro mean photon energies below about 120 keV, and sometimes up to 150 keV. Particle-in-cell code simulations show the impedance behavior and flow pattern in the inverse triax with and without the presence of an anode plasma. The simulation results are used to suggest design rules for inverse triax diodes. Experimental results show good agreement with calculations of the impedance behavior and electron beam dynamics. Using inverse triax diodes, we have produced peak doses of 1.4 {times} 10{sup 11} rad(TLD)/s over 840 cm{sup 2} with a mean photon energy of 120 keV on SPEED and 3.1 {times} 10{sup 11} rad(TLD)/s over 3700 cm{sup 2} with a mean photon energy of 140 keV on Saturn. 20 refs., 16 figs.

The BES Materials Science program at Sandia Albuquerque has the central theme of Scientifically Tailored Materials. The major objective of this program is to combine Sandia's expertise and capabilities in the areas of solid state sciences, advanced atomic-level diagnostics and materials-processing science to produce new classes of tailorable materials for the US energy industry, the electronics industry and for defense needs. Current research in this program includes the physics and chemistry of ceramics, the use of energetic particles for the synthesis and study of materials, high-temperature and organic superconductors, tailored surfaces for materials applications, chemical vapor deposition sciences, strained-layer semiconductors, advanced growth techniques for improved semiconductor structures and boron-rich very high temperature semiconductors. A new start just getting underway deals with the atomic level science of interfacial adhesion. Our interdisciplinary program utilizes a broad array of sophisticated, state-of-the-art experimental capabilities provided by other programs. The major capabilities include several molecular-beam epitaxy and chemical-vapor-deposition facilities, electron- and ion-beam accelerators, laser-based diagnostics, advanced surface spectroscopies, unique combined high-pressure/low-temperature/high-magnetic-field facilities, and the soon to be added scanning tunneling and atomic force microscopies.

Calorimetry was performed on Sandia National Laboratories' Test Bed Concentrator {number sign}1 (TBC-1) during late July and early August 1989. The purpose of the tests was to determine the total power available from the concentrator and the amount of the total power that can be focused through a 22-cm aperture plate located at the nominal focal point of the dish. The 22-cm aperture corresponds to the diameter of several reflux receivers that are currently under development, fabrication and testing at Sandia. The calorimeter test will allow the efficiency of the sodium reflux receivers to be calculated. The total power (normalized to 1000 W/m{sup 2}) available from TBC-1 is 66.4 kW into the 22-cm aperture plate. Within error limits, this power level is the same with or without the aperture plate. The power levels stated are for this time (July 1989) and will probably change as the mirrors further degrade. Since the last calorimetry tests were performed, the mirror facets have degraded significantly, and the results presented here support this effect. Finally, three of the 220 facets were missing. 3 refs., 5 figs., 2 tabs.

This report describes research leading to the development of new catalytic materials based on hydrous metal oxide (HMO) ion exchangers. Present in this part, the second of two parts, are results of catalyst-related research and application of the materials to catalytic reactions for direct coal liquefaction processes. HMO materials are inorganic ion exchangers, derived from the alkoxides of Ti, Zr, Nb, or Ta, that exhibit a number of properties applicable to the preparation of catalysts. Research on the catalytic properties of HMO's has focused on the hydrous titanium oxide (HTO) system. However, exploratory coal liquefaction experiments with hydrous niobium oxides (HNO's) and hydrous zirconium oxides (HZO's) have demonstrated that these HMO's also exhibit potential as coal liquefaction catalysts. Studies performed during the course of this research include (1) preliminary coal liquefaction and hydrotreating tests, (2) tests of hydrogenation, hydrodesulfurization, hydrodeoxygenation and hydrodenitrogenation activity using model compounds, (3) development of catalyst pretreatment and activation procedures, (4) modification of HTO supports with silicon, (5) preparation and testing of thin film HTO catalysts, (6) synthesis, characterization and evaluation of base and noble metal catalyst deactivation tests, and (9) exploratory tests of applications other than direct liquefaction. The versatility of the HTO system for synthesis of catalysts allows great potential for further improvements in activity and selectivity as well as tailoring of catalysts for specific processes. Research is continuing in these areas. 54 refs., 63 figs., 25 tabs.

Drillholes H-14 and H-15 were drilled to investigate data gaps in the hydrologic hole distribution at the WIPP site. In addition to the information gained on the Culebra Dolomite Member, the holes yielded hydraulic and/or stratigraphic information on the Forty-niner, Magenta Dolomite, and Tamarisk Members of the Rustler Formation in an era where no such information was available. Hydraulic tests were also conducted on the lower part of the Dewey Lake Redbeds in H-14. A suite of geophysical logs was run on the drillholes and was used to identify different lithologies and aided in the interpretation of the hydraulic tests. 3 refs., 4 figs., 6 tabs.

This report presents a method of running batch jobs from menu-driven interactive EQUEL programs. EQUEL is the embedded query language of INGRES, a popular database management system used widely at Sandia. The method is framed in the VAX/VMS operating system environment.

For more than 10 years, the US Department of Energy's Solar Thermal Program has pioneered the development of heliostats, mirrors that track the sun, for solar central-receiver power plants. The field of heliostats is the single most expensive part of such plants, so their cost must be as low as possible for the technology to be commercially successful. Recent efforts have focused on the development of heliostats that use stretched-membrane reflectors in place of the more familiar glass mirrors. In such heliostats, metal foils are stretched over both sides of a large-diameter metal ring. The reflective surface is a silvered-polymer film glued to the front membrane. A slight vacuum in the space between the two membranes is actively controlled to provide a concave, focused contour to the mirror, and in an emergency this space can be rapidly pressurized to defocus it. Because of their simplicity and lighter weight, stretched- membrane heliostats have the potential to cost significantly less than current glass-mirror designs. The first 50-m{sup 2} mirror modules, built under contract to Sandia in 1986, demonstrated that membrane heliostats could perform at least as well as heliostats using glass mirrors. Insights gained from Sandia's testing and evaluation of the first-generation units were incorporated into the designs of two improved 50-m{sup 2} mirror modules. The results of Sandia's evaluation show significant improvement in optical performance over the first-generation designs, especially in windy conditions. 22 refs., 29 figs.

This report describes the application of word processing, graphics and data base software to the task necessary for the exclusion of Building 823 from the secure technical area at Sandia National Laboratories. In particular, this report focuses on the development of the building floor plans layouts and the space/personnel data base which were used by management to plan and coordinate the project. Once the project is complete, these information systems will continue to be maintained by other personnel for administrative purposes. The software developed has potential applicability to other facilities where administrative monitoring or space assessment is required. 6 figs.

Personnel from Stockpile Evaluation Program Division I, 7261, have been testing Joint Test Assemblies (JTAs) at Meppen Range, Federal Republic of Germany (FRG) since 1984. JTA trajectories were obtained from cinetheodolite film. The MPS-36 radar at Meppen Range is required to track the aircraft before bomb release to verify the release parameters for range safety and for the bomb trajectory after release. This is a difficult task because of the low-level approach of the aircraft. Division 7261 personnel asked Tonopah Test Range Department 7170 to assist in solving radar tracking problems. We recommended a new closed-circuit television system with a zoom lens and a force-operated, two-axis joystick. This system provides the operator a means of overriding the automode of the radar and manually positioning the radar antenna in azimuth (AZ) and elevation (EL). The joystick operator keeps the target (aircraft or bomb) centered in the TV picture by applying the correct pressure to the joystick. At the same time, the radar console operator maintains automatic range tracking by assisting the range gate through ground clutter using the control level of the range gate, as a rate-aid control in automatic mode. During the period May 8-17, 1989, the visual tracking equipment was installed in the Meppen radar. On May 16, 1989 a bomb dummy unit, loft maneuver was tracked successfully. The video, with time of day, was recorded for posttest, quick-look data. In the ten years of planned testing, a twenty-fold cost savings would be achieved with incorporation of the visual tracking capability to the MPS-36 radar, rather than providing radar beacons on each JTA. 8 figs.

Sandia National Laboratories, as part of the Containment Integrity Programs under the sponsorship of the Nuclear Regulatory Commission (NRC), has developed analytical techniques for predicting the performance of light water reactor steel containment buildings subject to loads beyond the design basis. The analytical techniques are based on experience with large-scale steel containment model tests that provided important insights and experimental validation of the analytical methods. As a means of demonstrating these analytical techniques, the NRC asked Sandia to conduct a structural evaluation of an actual steel containment building. The objective of the analysis was to determine the actual pressure capacity and the mode, location, and size of failure, where a functional definition of failure is used. The purpose of this report is to document the calculations performed to determine the pressure limits for the shell- rupture mode of failure. General failure of the containment shell is predicted by application of a failure criterion to the results from finite element structural analyses. The failure criterion relates the calculated values of strain in the containment plates, due to internal-pressurization loading, to the ultimate strain limit of the steel. Included in the failure criterion are adjustments for factors inherent in finite element analysis, such as level of detail and element size of the finite element model and variations in material property data. Separate finite element models were used to evaluate the overall free-field behavior of the structure and the localized behavior at a specific penetration location. 18 refs., 68 figs., 10 tabs.

In an experiment conducted at Sandia National Laboratories, 1:6-scale model of a reinforced concrete light water reactor containment building was pressurized with nitrogen gas to more than three times its design pressure. The pressurization produced one large tear and several smaller tears in the steel liner plate that functioned as the primary pneumatic seal for the structure. The data collected from the overpressurization test have been used to evaluate and further refine methods of structural analysis that can be used to predict the performance of containment buildings under conditions produced by a severe accident. This report describes posttest finite element analyses of the 1:6-scale model tests and compares pretest predictions of the structural response to the experimental results. Strain and displacements calculated in axisymmetric finite element analyses of the 1:6-scale model are compared to strains and displacement measured in the experiment. Detailed analyses of the liner plate are also described in the report. The region of the liner surrounding the large tear was analyzed using two different two-dimensional finite elements model. The results from these analyzed indicate that the primary mechanisms that initiated the tear can be captured in a two- dimensional finite element model. Furthermore, the analyses show that studs used to anchor the liner to the concrete wall, played an important role in initiating the liner tear. Three-dimensional finite element analyses of liner plates loaded by studs are also presented. Results from the three-dimensional analyses are compared to results from two-dimensional analyses of the same problems. 12 refs., 56 figs., 1 tab.

The Yucca Mountain Project (YMP) is examining the feasibility of siting a repository for high-level nuclear waste at Yucca Mountain, on and adjacent to the Nevada Test Site (NTS). The proposed repository will be excavated in the Topopah Spring Member, which is a moderately fractured, unsaturated, welded tuff. Excavation stability will be required during construction, waste emplacement, retrieval (if required), and closure to ensure worker safety. The subsurface excavations will be subject to stress changes resulting from thermal expansion of the rock mass and seismic events associated with regional tectonic activity and underground nuclear explosions (UNEs). Analyses of drift stability are required to assess the acceptable waste emplacement density, to design the drift shapes and ground support systems, and to establish schedules and cost of construction. This paper outlines the proposed methodology to assess drift stability and then focuses on an example of its application to the YMP repository drifts based on preliminary site data. Because site characterization activities have not begun, the database currently lacks the extensive site-specific field and laboratory data needed to form conclusions as to the final ground support requirements. This drift design methodology will be applied and refined as more site-specific data are generated and as analytical techniques and methodologies are verified during the site characterization process.

This Test Plan describes laboratory and modeling studies of: the chemistry of brines that could enter Waste Isolation Pilot Plant (WIPP) disposal rooms; the effects of anoxic corrosion of metals in steel containers and the waste on the gas and H{sub 2}O budgets of the repository; the effects of microbial activity, especially microbial degradation of cellulosics in the waste, on the gas and H{sub 2}O budgets of the repository, the Eh and pH of any brine present, and the chemical behavior of radionuclides; the effects of radiolysis on the gas and H{sub 2}O budgets of the repository; the efficacy of backfill additives proposed to remove microbially produced CO{sub 2} or prevent the formation of H{sub 2} from anoxic corrosion, and their effects on repository chemistry; the chemical behavior of Pu, Am, Th, and U in WIPP brines; additional development of the EQ3/6 geochemical software package for use in predicting the behavior of silicates and radionuclides in brines. This Test Plan describes studies of the chemical behavior of the repository as currently designed, and the chemical behavior of radionuclides under these conditions. Addenda will discuss additional studies relevant to design modifications, especially reprocessed waste, and chemically hazardous waste constituents. 165 refs., 7 tabs.

Generally multicomponent mixtures can exhibit a rich collection of phenomena. Thus it is to be expected that they will be described by complicated theories. In this paper we describe a relatively simple theory that is still theoretically correct, and discuss some of the phenomena that it exhibits. 12 refs.

Guest-host poled polymer films have become an active area of research as potential candidates for second-order nonlinear optical and electro-optic devices. This interest derives mainly from their large nonlinear optical coefficients, ease of fabrication, and high optical quality. Progress has been rapid in producing stable, efficient materials, and in building demonstration devices. The second-order nonlinear optical properties arise from the orientational order induced in a collection of highly nonlinear molecules incorporated in a glassy polymer matrix. After reviewing the alignment physics, we present results of nonlinear optical measurements on a methacrylate polymer functionalized with a dicyanovinyl terminated azo dye. Device issues concerning nonlinear optical devices are described with particular attention to phase-matching. We present data on the demonstration of anomalous-dispersion phase matched second harmonic generation in dye solutions. We also present results on electro-optic modulators. © 1989 SPIE.

The author describes a waveform-recorder evaluation system which is controlled by a Microvax II with instrumentation control through the IEEE-488 bus. Evaluation procedures are described with attention to the 'pathological cases' that can lead to significant misestimates of a digitizer's performance. The aim of these evaluation procedures is consistency with the new Trial Waveform Digitizer Standard generated by the Waveform Measurements and Analysis Committee appointed by the Instrumentation and Measurement Society of the IEEE. Methods are discussed for measuring the effective-bits performance of a waveform digitizer and determining differential nonlinearity.

The Primary Standards Laboratory at Sandia National Laboratories (SNL) and the Precision Engineering Division at the National Institute of Standards and Technology (NIST) are in the process of implementing software error correction on two nearly identical high-accuracy coordinate measuring machines (CMMs). Both machines are Moore Special Tool Company M-48 CMMs which are fitted with laser positioning transducers. Although both machines were manufactured to high tolerance levels, the overall volumetric accuracy was insufficient for calibrating standards to the levels both laboratories require. The error mapping procedure was developed at NIST in the mid 1970's on an earlier but similar model. The error mapping procedure was originally very complicated and did not make any assumptions about the rigidness of the machine as it moved, each of the possible error motions was measured at each point of the error map independently. A simpler mapping procedure was developed during the early 1980's which assumed rigid body motion of the machine. This method has been used to calibrate lower accuracy machines with a high degree of success and similar software correction schemes have been implemented by many CMM manufacturers. The rigid body model has not yet been used on highly repeatable CMMs such as the M48. In this report we present early mapping data for the two M48 CMMs. The SNL CMM was manufactured in 1985 and has been in service for approximately four years, whereas the NIST CMM was delivered in early 1989. 4 refs., 5 figs.

Merlin is a memory based, interconnection system designed to provide very high-performance capability in a disturbed multicomputer environment. By using dynamically mapped reflective memory operations, the system creates a virtual memory environment which permits users to utilize both local and shared memory techniques. This mapped virtual memory approach permits selected information to be shared at high speeds and with relatively low latency. There is no software involvement in the actual sharing of information and the system automatically overlaps computation and communication, to the extent possible, on a word-by-word basis. Memory-to-Memory mapping allows Merlin to provide a uniform programming environment which is independent of interconnection topology, processing elements, and languages. 14 refs., 4 figs.

In the most transmissive parts of the Culebra Dolomite, fluid flow is controlled by fractures. Gypsum (CaSO{sub 4} 2H{sub 2}O) and corrensite (a mixed chlorite/smectite) are the most abundant fracture-fill minerals. Radionuclide/clay interactions may be the dominant mechanism for radionuclide retardation. For this reason, the focus of this study is to examine the extent of the sorption of uranium and plutonium onto clays within the Culebra matrix and fractures. This paper describes several coordinated activities which will evaluate the potential retardation of radionuclide migration by sorption onto clays within the Culebras. These include characterization of the compositions of clays and groundwaters along the flow path; studies of the surface properties of simple reference clays and Culebra clays in dilute solutions and saline mixed electrolytes; development of a database of intrinsic equilibrium constants and specific-interaction parameters for calculations of the aqueous speciation of uranium and plutonium in Na-Cl-Ca-SO{sub 4}-CO{sub 3}-EDTA solutions which range in ionic strength from 0.1--4.0 molal; and measurement of surface complexation constants for uranium and plutonium in simple and mixed electrolyte solutions containing clays. 2 refs., 2 figs.

The nickel/hydrogen battery was developed in the early nineteen-seventies as an energy storage subsystem for commercial communication satellites. The advantages offered by nickel/hydrogen batteries, including long life, low maintenance and high reliability, make it very attractive for terrestrial applications such as stand-alone photovoltaic systems. The major drawback to the wider use of the nickel/hydrogen battery is its high initial cost. Sandia National Laboratories has placed cost-shared contracts with Comsat Laboratories and Johnson Controls, Inc., to reduce the cost, and a battery consisting of prismatic cells in a common pressure vessel has evolved. A 7-kWh battery has been on test at Sandia since January 1988 using a flat-plate photovoltaic array for charging. © 1990 IEEE

In component reliability assessment programs, three major sources of data are available for reliability assessment: a development program, production data, and field test data. In practice, reliability assessments are required at the end of each stages, and a common method of assessment is to simply combine the test data and provide a pooled estimate. The method suggested in this paper is Bayesian in that the uncertainty about the unreliability is expressed by means of a prior distribution with a specified upper limit. The method is hierarchical Bayes in that the uncertainty about the limit of that prior distribution is also expressed by means of a prior distribution. The data from the development program are incorporated with the prior on the unreliability and with the prior on the upper limit of the prior to obtain a new prior on unreliability. The production data are then used to obtain a revised estimate of the unreliability as well as a modified value for the limit of the prior distribution. This same concept will be carried through when the field data are obtained. The result is a final Bayesian reliability assessment that is iterative in nature and incorporates in a sequential fashion data from each of the three stages common to a component development, production, and surveillance program. 4 refs., 2 tabs.

Power loadings experienced by tokamak plasma-facing components during normal operation and during off-normal events are discussed. A model for power and particle flow in the tokamak boundary layer is presented and model predictions are compared to infrared measurements of component heating. The inclusion of the full three-dimensional geometry of the component and of the magnetic flux surface is very important in the modeling. Experimental measurements show that misalignment of component armour tile surfaces by only a millimeter can lead to significant localized heating. An application to the design of plasma-facing components for future machines is presented. Finally, thermal loads expected during tokamak disruptions are discussed. The primary problems are surface melting and vaporization due to localized intense heating during the disruption thermal quench and volumetric heating of the component armour and structure due to localized impact of runaway electrons. © 1990.

The tungsten subfluoride mechanism as well as other proposed mechanisms of selectivity loss are reviewed. To further demonstrate the viability of the tungsten subfluoride mechanism, we have extended the measurement of the tungsten subfluoride production rate down to 450{degree}C. We also report results from some preliminary experiments designed to identify the selectivity loss mechanism when elemental silicon is available for reaction. Comments regarding the origins of the insulator effect and selectivity loss for silane reduction are offered. 23 refs., 2 figs.

The use of NUREG-1150 and similar Probabilistic Risk Assessments in NRC and industry risk management programs is discussed. Risk management'' is more comprehensive than the commonly used term accident management.'' Accident management includes strategies to prevent vessel breach, mitigate radionuclide releases from the reactor coolant system, and mitigate radionuclide releases to the environment. Risk management also addresses prevention of accident initiators, prevention of core damage, and implementation of effective emergency response procedures. The methods and results produced in NUREG-1150 provide a framework within which current risk management strategies can be evaluated, and future risk management programs can be developed and assessed. Examples of the use of the NUREG-1150 framework for identifying and evaluating risk management options are presented. All phases of risk management are discussed, with particular attention given to the early phases of accidents. Plans and methods for evaluating accident management strategies that have been identified in the NRC accident management program are discussed. 2 refs., 3 figs.

A new interfacial force microscope capable of measuring the forces between two surfaces over the entire range of surface separations, up to contact, has been developed. The design is centered around a differential capacitance displacement sensor where the common capacitor plate is supported by torsion bars. A force-feedback control system balances the interfacial forces at the sensor, maintaining the common capacitor plate at its rest position. This control eliminates the instability which occurs with the conventional cantilever-based force sensors when the attractive force gradient exceeds the mechanical stiffness of the cantilever. The ability to measure interfacial forces at surface separations smaller than this instability point using the feedback control is demonstrated. 11 refs., 3 figs.

The lowest excited electronic state of molecular oxygen, singlet oxygen ({sup 1}{Delta}{sub g}0{sub 2}), can be produced in solid organic polymers by a variety of different methods. Once produced, singlet oxygen will return to the ground triplet state by two pathways, radiative (phosphorescence) and non-radiative decay. Although the quantum efficiency of phosphorescence is small ({minus}10{sup {minus}5}), singlet oxygen can be detected by its emission at 1270 mn in both steady-state and time-resolved experiments. The phosphorescence of singlet oxygen can be used to characterize many properties of a solid organic polymer. 2 refs., 5 figs.

We review our work on multi component polymeric nonlinear optical materials. These materials consist of nonlinear optical molecules incorporated in a polymeric host. A cross-linked triazine polymer incorporating a dicyanovinyl terminated azo dye was found to be relatively stable at 85{degree} and posses an electro-optic coefficient of 11pm/V. We have also observed the zero dispersion condition in a new anomalous dispersion dye for phase matched second harmonic generation, and expect efficient conversion to the blue. A squarylium dye, ISQ, has been found to posses a large third order nonlinearity, and may display two-level behavior. 24 refs., 11 figs.

ULSI manufacturing technologies have resulted in the development of Ultra-Pure Processing (UPP) capabilities for the world-wide semiconductor industry. The primary goal of Ultra Pure Processing is the elimination of extraneous contaminants, both gaseous and particulate, from the wafer process environment. This calls for a comprehensive approach to the design, operation, and maintenance of semiconductor process equipment. Through UPP one may reduce the number of uncontrolled variables within a system enhancing implementation of Statistical Process Control on the process environment within the tool (in situ). Greater control over the process environment translates into increased product quality, manufacturability, throughput and yield. Instituting UPP requires the capability of monitoring contaminants in the process environment a well as a systematic approach to isolating and eliminating contamination sources. Ultra Pure Processing can result from a Contamination Reduction Program. Presented here are the results from a Contamination Reduction Program performed on a state-of-the-art vertical thermal process reactor (VTR). 8 figs., 5 tabs.

Most previous Probabilistic Risk Assessments have excluded consideration of accidents initiated in low power and shutdown modes of operation. A study of the risk associated with operation in low power and shutdown is being performed at Sandia National Laboratories for a US Boiling Water Reactor (BWR). This paper describes the proposed methodology for the analysis of the risk associated with the operation of a BWR during low power and shutdown modes and presents preliminary information resulting from the application of the methodology. 2 refs., 2 tabs.

In this paper we formulate a speech coding system that incorporates trellis coded vector quantization (TCVQ) and adaptive predictive coding (APC). A method for optimizing'' the TCVQ codebooks is presented and experimental results concerning survivor path mergings are reported. Simulation results are given for encoding rates of 16 and 9.6 kbps for a variety of coder parameters. The quality of the encoded speech is deemed excellent at an encoding rate of 16 kbps and very good at 9.6 kbps. 13 refs., 2 figs., 4 tabs.

The Institute of Certified Records Managers (ICRM) is a non-profit, certifying organization of professional records managers and administrators. ICRM members are experienced in information requirements, records and information systems, and the related office systems and technologies. All members have met certification requirements and have received the Certified Records Manager (CRM) designation. As the field of information and records management moves toward standardization, and as the application of new technologies and technicalities complicate the measurement and demonstration of professional competence, the need for a means of identifying persons who have basic competency increases. The ICRM is providing such a means by testing and certifying basic knowledge. More and more job announcements are requiring this evidence of competency. Unfortunately, as an organization, NIRMA has a relatively small number of CRMs. The goal of the ICRM Development Group is two-fold; (1) to encourage NIRMA members to obtain their certification by providing basic information and support and; (2) to develop the Nuclear Specialist test module which will demonstrate that bearers have demonstrated expertise in nuclear records management as well as basic competencies. This report covers the examination process.

The Nuclear Information and Records Management Association (NIRMA) Task Force on Requirements Identification is currently involved in a four part project. During the course of the next year the Task Force will: (1) identify the generic requirements documents which have common applicability to nuclear utilities and DOE organizations; (2) research the requirements documents to identify individual requirements; (3) develop and implement a PC based tracking system to present and maintain the research data; and (4) implement a process for ongoing review of requirements. This report discusses these issues.

Multiplexer and amplifier systems must be designed with transistors that can perform satisfactorily over ten years to a total gamma dose of 120E6 rads and a total neutron fluence of 1.6E15 nvt for the SP-100 reactor system. Series of gamma and neutron tests have been completed to measure transistor degradation as a function of total dose, fluence, and temperature. Test results indicate that modest increases in temperature result in substantial improvement of transistor performance at a neutron flux of 8E8 n/cm{sup 2}/s. 2 refs., 3 figs.

Critical Heat Flux (CHF), also called burnout, is one of the major design limits for water-cooled divertors in tokamaks. Another important design issue is the correct thermal modeling of the divertor plate geometry where heat is applied to only one side of the plate and highly subcooled flow boiling in internal passages is used for heat removal. This paper discusses analytical techniques developed to address these design issues, and the experimental evidence gathered in support of the approach. Typical water-cooled divertor designs for the International Thermonuclear Experimental Reactor (ITER) are analyzed, and design margins estimated. Peaking of the heat flux at the tube-water boundary is shown to be an important issue, and design concerns which could lead to imposing large design safety margins are identified. The use of flow enhancement techniques such as internal twisted tapes and fins are discussed, and some estimates of the gains in the design margin are presented. Finally, unresolved issues and concerns regarding hydraulic design of divertors are summarized, and some experiments which could help the ITER final design process identified. 23 refs., 10 figs.

Our previous calorimetric studies of weld melting efficiency and arc efficiency in the GTAW and PAW processes have naturally led us to speculate as to the magnitude of the efficiencies in the LBW process which to data have also not been adequately investigated. Most welding engineers that have had experience with the LBW process are acutely aware that the metals' absorptivity, the surface finish, and the laser wavelength, all play an important role in affecting the energy transfer efficiency, but the extent of their influence and our understanding of the influence of other process variables is not well understood. In addition, it is widely thought that only the LBW or EBW processes can be selected for applications where thermal damage and distortion from the welding process must be kept to a minimum. For these reasons, we have looked forward to performing these calorimetric experiments since they potentially can answer such important questions as: whether or not the melting efficiency of the LBW process is superior to that obtainable with conventional GTAW and PAW welding processes This study was prompted by poor production yields on switching device due to cracking of the ceramic header after final closure welding with the CO{sub 2} LBW process. This calorimetric study was begun in hopes of determining if allowed variations in production process control variables were responsible for increases in heat input and the resulting thermal stresses. By measuring the net heat input to the workpiece with the calorimeter and by measuring the laser output energy and the weld fusion zone size it was possible to determine the magnitudes of both the energy transfer efficiency and the melting efficiency as well as observe their dependence on the process variables. 3 refs.

Component test plans are often designed by allocating a system's reliability goal among the system's components, then designing individual component test plans suitable for demonstrating achievement of each component's reliability goal. One use of the resulting component test data is the calculation of estimated system reliability, based on a model linking the component reliabilities to system reliability. The statistical precision of this system estimate depends on the component test plans (numbers of each component tested and the type of tests, e.g., variables or attributes) and, hence, is determined by the component test planners. Because system reliability may be of considerable interest, we feel an integrated view of component testing is required to assure that the ensemble of component tests will provide an adequate system reliability estimate. This paper considers the case of a series system of different components and binomial component data. For the case of equal numbers of units tested of each component (which can be shown to minimize total cost, subject to the risk constraints) the O.C. envelope is readily derived and from this envelope component test plans that satisfy the specified risks can be derived from equations that involve the cumulative binomial distribution function. Existing tables pertaining to acceptance sampling plans based on the binomial distribution can be used to determine the required number of component tests. 10 refs., 2 figs.

Weak formulations in Analytical Dynamics are developed, paralleling the variational methods in elastostatics, and including a fundamental yet novel approach for treating constraints (both holonomic and nonholonomic). A general three field approach is presented, in which the momentum balance conditions, the compatibility conditions between displacement and velocity, the constitutive relations and the displacement and momentum boundary conditions are all enforced in weak form. A primal, or kinematic formulation is developed from the general form by enforcing the compatibility conditions and displacement boundary conditions a priori. The conditional stability of the kinematic formulation is the counterpart of the locking phenomenon in elastostatics and may be avoided, either by reduced order integration, or by utilizing a mixed formulation. Toward this end, a two field mixed formulation is presented, which follows from the general form, when the constitutive relations are satisfied a priori. A general set of the constraint equations are introduced into the kinematic and mixed formulations, using a specific choice of multipliers, which results in modified variational principles. Several simple examples concerning rigid body dynamics are presented. 15 refs., 18 figs.

This paper describes arc discharge tests conducted in a prepressurized, constant-volume pressure vessel to study arc behavior over a wide range of current densities, discharge durations and initial vessel pressures. This method allows controlled access to a wider range of conditions than those previously studied in capillary tests. We have investigated aspects of the radiative heat transfer by calculating the material opacity and mean free paths of photons for conditions typical of arc diagnostics. We also performed one-dimensional Eulerian hydrodynamic calculations of the boundary layer behavior in the radiative diffusion approximation. These calculations, which describe the radial mass flow and heat transfer in the absence of turbulent flow effects, show the characteristic times for equilibrium of the high-pressure arc. Finally, we describe progress on a promising means for increasing the mass flux from the capillary discharge through the use of chemically reactive media on the capillary walls. 20 refs., 7 figs.

Integrated circuit logic states are maintained by virtue of specific transistor combinations being either on'' (conducting) or off'' (nonconducting). High energy ion strikes on the microcircuit generate photocurrents whose primary detrimental effect is to make off'' transistors appear on,'' confusing the logic state and leading to single event upset (SEU). Protection against these soft errors is accomplished using either technology or circuit techniques, actions that generally impact yield and performance relative to unhardened circuits. We describe, and using circuit simulations analyze, a technique for hardening latches which requires combinations of technology and circuit modifications, but which provides SEU immunity without loss of speed. Specifically, a single logic state is hardened against SEU using technology methods and the information concerning valid states is then used to simplify hardened circuit design. The technique emphasizes some basic hardening concepts, ideas for which will be reviewed. 3 refs., 2 figs.

Fabrication of high-efficiency silicon solar cells requires processing technology capable of maintaining long bulk carrier lifetime and low surface recombination. Development of long-lifetime processing techniques using experimental designs based on statistical methods is described. The first three experiments investigated pre-oxidation cleans, phosphorus gettering, and a comparison of different phosphorus diffusion sources. Optimal processing parameters were found to depend on type of silicon material. 2 refs., 2 figs., 2 tabs.

Thin film ferroelectric materials are the basis for a new, promising IC nonvolatile memory technology. The primary material being studied for ferroelectric memories is PZT. One of the key factors in determining the feasibility of PZT ferroelectric memories for weapon or space applications is whether PZT ferroelectric technology can be integrated into a radiation-hardened CMOS or bipolar process. Sandia National Laboratories has a program to study ferroelectric/CMOS process integration issues. The primary goal of this program is to determine if radiation-hardened reliable ferroelectric/CMOS IC memories can be fabricated. This program includes both the fabrication and characterization of ferroelectric test capacitors. In this paper we will give a brief overview of the program, discuss techniques developed to characterize ferroelectric devices for retention and endurance, and give results on studies of fatigue and retention of capacitors.

A travelling wave Faraday effect fiber current sensor, consisting of a helical optical fiber coil immersed in a dielectric medium, has been demonstrated. Improved phase matching conditions have led to measured bandwidth enhancements of greater than a factor of four. Sensitive devices with multi-gigahertz bandwidths are possible using this technique. 7 refs., 3 figs.

The authors present sufficient conditions for the design of strictly positive real (SPR), fixed-order dynamic compensators. The primary motivation for designing SPR compensators is for application to positive real (PR) plants. When an SPR compensator is connected to a PR plant in a negative feedback configuration, the closed loop is guaranteed stable for arbitrary plant variations as long as the plant remains PR. Equations that are a modified form of the optimal projection equations, with the separation principle not holding in either the full- or reduced-order case, are given. A solution to the design equations in shown to exist when the plant is PR (or just stable). Finally, the closed-loop system consisting of a PR plant and an SPR compensator is shown to be S-structured Lyapunov stable.

A Nuisance Alarm Data System (NADS) was developed to gather long-term background alarm data on exterior intrusion detectors as part of their evaluation. Since nuisance alarms play an important part in the selection of intrusion detectors for use at Department of Energy (DOE) facilities, an economical and reliable way to monitor and record these alarms was needed. NADS consists of an IBM Personal Computer and printer along with other commercial units to communicate with the detectors, to gather weather data and to record video for assessment. Each alarm, its assessment and the weather conditions occurring at alarm time are placed into a database that is used in the evaluation of the detector. The operating software is written in Turbo Pascal for easy maintenance and modification. A portable system, based on the NADS design, has been built and shipped to other DOE locations to do on-site alarm monitoring. This has been valuable for the comparison of different detectors in the on-site environment and for testing new detectors when the appropriate conditions do not exist or cannot be simulated at the Exterior Intrusion Detection Testbed.

Statistical process control (SPC) of technology parameters relevant to radiation hardness, test structure to IC correlation, and extrapolation from laboratory to threat scenarios are keys to implementing QML for radiation hardness assurance in a cost-effective manner. Data from approximately 300 wafer lots fabricated in Sandia's 4/3-µm and CMOS IIIA (2-µm) technologies are used to demonstrate approaches to, and highlight issues associated with, implementing QML for radiation-hardened CMOS in space applications. An approach is demonstrated to implement QML for single-event upset (SEU) immunity on 16k SRAMs that involves relating values of feedback resistance to system error rates. It is seen that the process capability indices, Cp and Cpk, for the manufacture of 400 kΩ feedback resistors required to provide SEU tolerance do not conform to “6σ” quality standards. For total-dose, ΔVit shifts measured on transistors are correlated with circuit response in the space environment. SPC is illustrated for ΔVit, and violations of SPC rules are interpreted in terms of continuous improvement. Finally, design validation for SEU, and quality conformance inspections for total-dose, are identified as major obstacles to cost-effective QML implementation. Techniques and tools that will help QML provide real cost savings are identified as physical models, 3D device-plus-circuit codes, and improved design simulators. © 1990 IEEE

We have measured 1/f noise in MOS transistors as a function of gate and drain bias, total ionizing dose, and postirradiation biased annealing time. The transistors tested varied in size, radiation hardness, and process technology. The radiation-induced 1/f noise correlates strikingly with the oxide trap charge through irradiation and anneal, but not with interface-trap charge, for frequencies up to 10 kHz. This implies that oxide trapped charge is the pre-dominant factor which leads to the increased 1/f noise in irradiated MOS devices. © 1990 IEEE

A 2D-Laser Radar Imaging System consisting of a prototype 2D-Laser Radar Sensor and an Image Processing System is currently being developed as an intrusion detection system capable of immediate detection and quick assessment for perimeter security and surveillance. The objective of this system is to produce a thin laser wall as an invisible intrusion barrier. Since only a small space is needed to create a narrow laser radar wall, this system will work well where there is only limited or narrow zones available to create the secure perimeter. Images are created of objects which penetrate the laser radar wall for assessment and to determine the appropriate alarm response. Such a system can be used to protect against airborne threats from rooftop areas or to guard against ground threats across perimeter zones of critical facilities. This paper will discuss the operational concepts, the technology, and an initial performance of this prototype system. 2 refs., 6 figs.

The SEU vulnerability of the SA3300 16-bit microprocessor has been characterized, and the effects of two different design revisions on error rate have been explored. We found that the threshold for upset depends on the data pattern written into the general purpose registers. With all bits in the general purpose registers set to logic one, a design with 2-µm n- and p-channel transistor lengths had a threshold LET of 35 MeV-cm2/mg at 25°C and 4.5 volt operation. With all zero's stored in the registers the upset threshold increased by more than a factor of two to 83 MeV-cm2/mg. A second design revision, with 1.25-µm and 1.75-µm n- and p-channel transistor lengths, respectively, was more vulnerable to upset, but exhibited a smaller dependence on logic state. Measured threshold LET was 23 and 35 MeV-cm2/mg with all one's and all zero's, respectively. Microprobe measurements using a pulsed Nd:YAG laser suggest that the observed pattern dependence for both design revisions is due to bipolar photocurrent in a vertical n+pn transistor. A slight temperature dependence was observed in both design revisions. This is consistent with the use of oversized restoring transistors to minimize SEU vulnerability rather than polysilicon feedback resistors. More recent data show thresholds above 120 MeV-cm2/mg with 80 kΩ feedback resistors. © 1990 IEEE

The paper reviews the interaction of plasmas with materials and presents a status summary based on experience in large fusion experiments, laboratory investigations and design studies. The phenomena that are discussed limit the power densities and confinement properties attainable in plasmas; their control is an essential element of the design of future fusion devices. © 1990 IOP Publishing Ltd.

The use of porous oxide coatings, formed using sol-gel chemistry routes, as the discriminating elements of acoustic wave (AW) chemical sensors, is investigated. These coatings provide several unique advantages: durability, high adsorption capacity based on large surface areas, and chemical selectivity based on both molecular size and chemical interactions. The porosity of these coatings is determined by performing nitrogen adsorption isotherms using the AW device response to monitor the uptake of nitrogen at 77 K. The chemical sensitivity and selectivity obtained with this class of coatings is demonstrated using several examples: hydrous titanate ion exchange coatings, zeolite/silicate microcomposite coatings, and surface modified silicate films.

In light sources such as tungsten filament bulbs, fluorescent tubes and gas tube type radioluminescent (RL) lamps, visible light is emitted from a thin surface layer of excited material. In contrast, neon bulbs, xenon flash tubes and lasers emit light generated throughout their volumes. The first group can be characterized as surface emitters and the latter as volumetric emitters. Theoretically, an ideal volumetric light source has definite advantages over a surface source. In reality, practical volumetric sources will have limitations as well. These advantages and limitations will be discussed with particular emphasis on comparisons between current gas tube type RL lamps and the more advanced volumetric RL lamps.

A new generation of digital multimeters was used to compare the ratios of the resistances of wire-wound reference resistors and quantized Hall resistances. The accuracies are better than 0.1 ppM for ratios as large as 4:1 if the multimeters are calibrated with a Josephson array. 9 refs.

A class of borazene polymers was developed which consists of a two‐dimensional array of six‐membered borazene rings with the borons of adjacent borazene rings separated by ‐NH‐ groups. Pyrolysis of these polymers above ∼1000°C leads to crystalline graphite‐like boron nitride (h‐BN). The thermal chemistry of thin films of one polymer deposited on KOH‐eched aluminum was examined by thermal decomposition mass spectroscopy (TDMS) and thermal gravimetric analysis (TGA), and the gas evolution chemistry was found to be essentially complete at temperatures less than 400°C. All products desorb with the same temperature profile and the major desorbing species are NH3 and N2, consistent with a loss of excess nitrogen and hydrogen in the polymer, and HCl from decomposition of byproducts of the synthesis step. Since the formation of ordered crystalline h‐BN films requires heating to temperatures of the order of 1000°C, whereas the gas evolution chemistry is complete by roughly 400°C, it is concluded that gas evolution chemical processes are not rate limiting in BN ceramic production. Copyright © 1990, Wiley Blackwell. All rights reserved

Constitutive modeling and bifurcation analyses are combined with axisymmetric (triaxial), triaxial/torsion, and plane-strain experiments to interpret and anticipate the development of shear localization in rocks. This paper discusses preliminary results. 22 refs., 3 figs.

The US Department of Energy (DOE) has supported the development of the sodium-sulfur technology since 1973. The programs have focused on progressing core aspects of the technology and completing initial battery engineering for both mobile and stationary applications. An overview of the Office of Energy Management (OEM) activities is contained in this paper. Two major development programs have been active: the first with Ford Aerospace and Communications Corporation (1975 to 1985), and the second with Chloride Silent Power Limited (1985 to 1990). With the completion this year of the qualification of a cell suitable for initial Solar Energy Systems (SES) applications, the emphasis of future DOE/OEM sodium/sulfur programs will shift to SES-battery engineering and development. The initial effort will resolve a number of issues related to the feasibility of utilizing the sodium/sulfur technology in these large-scale applications. This multi-year activity will represent the initial phase of an integrated long-term DOE-supported program to produce a commercially viable battery system.

The integrity of many mechanical assemblies and electrical components depends on small threaded fasteners. The design standards for small (less than {1/4} inch in diameter) screws made of stainless steel are not as well developed as those for larger sizes of high strength steels. The typical design approach is based on the application of static design principals. Steady state accelerations are applied to the component or assembly and sufficient screws are installed in mounting hardware for attachment to the next assembly. These design principals have been used successfully for years in a wide variety of applications. As the parts requiring small screws have continued to decrease in size, some design requirements include greater thread depths and adherence to strict interpretation of the governing thread standards. These design requirements have their origins in the lack of adequate definitions and standards for designs using small threaded fasteners. These design practices have led to significant problems in manufacturing parts with small threaded fasteners by requiring thread depths to four and more diameters of engagement while maintaining thread heights (radial engagement) of 75 percent throughout the thread interfaces. A test program was developed to address questions regarding design and manufacturing issues involving small threaded fasteners which included tensile strength, length of engagement needed to achieve the full strengths of the screws, and verification of the static design principals in dynamic conditions. This paper summarizes the initial results obtained to date from this test program and describes the work-in-progress on the dynamic tests with their related static tests. 2 refs., 4 figs., 4 tabs.

An isotropic continuum damage theory which accounts for the degradation of material strength under quasi-static loading conditions has been developed in the present investigation. The damage mechanism in this theory has been selected to be the interaction and growth of subscale cracks. The development of the theory follows closely the strain-rate dependent dynamic model advanced by the first author and his coworkers. Briefly, the cracks are activated by the maximum principal tensile strain and the density of activated cracks is described by a Weibull statistical distribution. The moduli of a cracked solid derived by Budiansky and O'Connell are then used to represent the global material degradation due to subscale cracking. Two additional material constants have been introduced in this model. These constants are determined from uniaxial tensile test data. The model has been implemented into a finite element code. Sample calculations involving the uniaxial and biaxial responses of plain concrete panels are presented to demonstrate the utility of the model. 7 refs., 2 figs.

The first in a series of multi-factor experiments designed to optimize the chemical cleaning procedure for four types of silicon material used in solar cell fabrication has been completed. The goal of this first experiment (a twenty-two factor main-effects experiment) was to determine the factors associated with chemical cleaning procedures that are most important in obtaining high excess charge-carrier recombination lifetime following a high-temperature furnace oxidation. It was determined that the factors having the strongest influence on charge-carrier lifetime were different for the four different silicon materials considered. In general, the lower the lifetime of the material, the less sensitive the material was to different chemical cleaning steps. The stability of the lifetime was also evaluated with several factors exhibiting a significant effect for high-quality silicon. Chemical cleaning procedures were identified that resulted in stable post-oxidation lifetimes greater than 2 ms for high-resistivity float-zone silicon. 3 refs., 8 figs.

The closure measurements from a large scale, heated, in situ experimental room in salt are compared to numerical calculations using the most recent predictive technology, with very good agreement, limited potentially only by the unmodeled roof fracture and separation.

Insulations are used in metallic glass ribbon cores in pulse power applications to prevent interlaminar eddy currents due to voltages induced between adjacent laminations. These interlaminar eddy currents can greatly increase the losses in cores, and, thereby, decrease the pulse permeability at high magnetization rates. This paper reports results of experiments with various insulation materials and both low and high induced anisotropy energy iron-base metallic glass ribbons. Co-wound insulation films as well as conformal insulations were investigated. Magnetic properties and voltage hold-off strengths are reported. 11 refs., 11 figs., 5 tabs.

When quartz controlled oscillators are required for use in applications demanding precision many factors will ultimately place limitations on the ability of the oscillator to remain at the desired frequency. These factors include temperature, resonator Q, pullability, radiation, output load variability, and the electronic components. This paper addresses the subject of frequency instability of oscillator circuits due to power supply voltage variations. In particular, the primary sources of this instability are described for a Pierce oscillator employing a bipolar transistor and design techniques are presented which minimize these frequency pulling effects. 4 refs., 17 figs.

The three-dimensional structural analysis of reentry vehicles presents a considerable challenge to the analyst. This is due to the mechanics of the problem as well as the incorporation of results from several disciplines into the environmental description of the problem. Separate results from aero-analyses, frequently computed in one-dimensional format must be combined into a three-dimensional format suitable for a structural finite element analysis. Features required for the analysis include the ablated thickness of the heatshield structure, as well as pressure on the vehicle and the temperature distribution through the heatshield. By combining these environments, a complete description of all factors which affect the structural performance of reentry vehicles are included into one analysis. This paper presents a method of analyzing the structural response of reentry vehicles using the complete three-dimensional environmental load description.

Reflection Mass Spectrometry (REMS) consists of a cryo-shrouded mass spectrometer which measures mass-analyzed, line-of-sight chemical fluxes from a growing wafer. It is especially useful during III/V molecular beam epitaxy (MBE) for which there are always substantial group V fluxes and often some group III fluxes leaving the wafer during growth. These fluxes depend sensitively on the instantaneous chemical reactivity of the surface. That chemical reactivity in turn depends on instantaneous alloy composition (III/III ratio), surface stoichiometry (As coverage) and temperature. In this brief summary of our work, we describe two examples of the engineering'' usefulness of REMS, involving MBE of InAlAs and InGaAs and one example of measurements of basic scientific interest. 3 figs.

A program is under way to develop liquid metal heat pipes that can transfer energy from the focal point of a parabolic solar concentrator to the heater tubes of one or more Stirling engines. To design high performance wicks for heat pipe solar receivers, it is necessary to have an accurate assessment of the wick's properties. Procedures for measuring the flow properties of wicks before and after fabrication processes take place are presented. The testing procedures provide a useful method of determining the validity of a wick design before full-scale testing is attempted.

Significant progress is continuing in the development of photovoltaic (PV) concentrator technology. New record cell and module efficiencies have been achieved, and improvements in cells, cell assemblies, and modules are increasing reliability and decreasing cost. The number of firms actively pursuing PV concentrator module technology has increased substantially in the last three years. Two new concentrator systems were installed last year, and we are likely to see more in the near future. This paper describes the most significant developments of the last two years, including descriptions of PV concentrator module development and reliability activities, advances in concentrator cell technology, the new PV concentrator array installations, a new Concentrator Initiative Program, and results of the latest costing study. 26 refs., 9 figs., 1 tab.

Chacahoula salt dome, eight miles southwest of Thibodaux, LA, could be solution mined to create caverns for storing as much as 500 million barrels (MMB) of crude oil, should the Strategic Petroleum Reserve (SPR) require additional storage volume. The salt mass geometry is confirmed by more than 50 oil wells, and also from previous exploratory drilling for sulphur. Top of salt occurs at {minus}1100 ft, and some 1300 acres exist within the {minus}2000 ft salt contour. Frasch mining of 1.35 million long tons of sulphur caused the surface to subside about one foot on the northeastern part of the dome. Creep-induced subsidence averaging {approximately}2.7 ft over 30 yrs is estimated for a 200 MMB cavern array, which would require perimeter diking to control localized perennial flooding. Earthquakes approaching intensity MM 6 have occurred nearby and are expected to recur on the order of {approximately}100 yrs but would not affect cavern stability. Additional study of brine disposal methods and hurricane surge probabilities are needed to establish design parameters and cost estimates for storage. 11 refs., 8 figs., 2 tabs.

A Nuisance Alarm Data System (NADS) was developed to gather long- term background alarm data on exterior intrusion detectors as part of their evaluation. Since nuisance alarms play an important part in the selection of intrusion detectors for use at Department of Energy (DOE) facilities, an economical and reliable way to monitor and record there alarms was needed. NADS consists of an IBM Personal Computer and printer along with other commercial units to communicate with detectors, to gather weather data and to record video for assessment. Each alarm, its assessment and the weather conditions occurring at alarm time are placed into a database that is used in the evaluation of the detector. The operating software is written in Turbo Pascal for easy maintenance and modification. A portable system, based on the NADS design, has been built and shipped to other DOE locations to do on-site alarm monitoring. This has been valuable for the comparison of different detectors in the on-site environment and for testing new detectors when the appropriate conditions do not exist or cannot be simulated at the Exterior Intrusion Detection Testbed.

A molten salt cavity receiver was solar tested at Sandia National Laboratories during a year-long test program. Upon completion of testing, an analysis was performed to determine the effect of thermal cycling on the receiver. The results indicate substantial fatigue damage accumulation for the receiver when the relatively short test time is considered. This paper describes the methodology used to analyze the cycling, the results, and how they affect future receiver design. The test receiver was configured as a C-shaped cavity with eight multipass heat absorption panels. The tubes were Alloy 800. The heat exchange medium was a molten nitrate salt mixture (60% sodium nitrate, 40% potassium nitrate by weight). The operating temperature range was from 288°C to 566°C.

Under compressive stresses, brittle polycrystalline materials fail as the result of the growth, interaction and coalesence of microcracks. To predict the deformation of damaging material, constitutive laws developed for such materials must incorporate the effects of crack size, density, orientation, and interaction.A method of incorporating the accumulation and growth of microcracks into a continuum model is to use a measure of microcrack growth and interaction defined as damage. Although a number of damage theories have been proposed, there is no generally accepted experimental technique for detecting and measuring damage. Acoustic emissions (AE) have been correlated with microcrack nucleation and growth. We propose that AE locations and density are useful measures of damage that can be correlated with calculated damage. Our approach is to use acoustic emissions (AE) and computer modeling to study the development of damage in geomaterials.

Consideration is given to the problem of stabilizing a plant using a suboptimal stable compensator of fixed order. The resulting equations are a modified form of the optimal projection equations, with the separation principle not holding in either the full- or reduced-order case. An overbounding technique on the state covariance guarantees that the compensator is stable if nonnegative definite solutions exist to the design equations.

The Function Point (FP) concept was introduced to define'' a measure for applications development and maintenance functions avoiding the problems inherent in productivity measures in the late 1970s. At that time, Albrecht outlines three essentials elements for software size measurement: the measure must be technology independent; the technique must measure all the application functions delivered to the end customer; and the technique must measure only the application functions as delivered. Using these three attributes of a measurement, further concentrated analysis could be performed for languages, technologies, methodologies, and tools. The characterization of systems and the quality of the product are motives for subscribing to FPs. Since the inception of FPs, attempts have been made to improve the process of quantifying FPs. Some of these attempts have strayed from the intended use of FPs and have diverted valuable energy away from consistent application. The purpose of this article is to describe the process and the quantification of complexity factors for each of the five Unadjusted FPs. 4 refs.

Light ion fusion research has developed ion diodes that have unique properties when compared to other ion diodes. These diodes involve relativistic electrons, ion beam stagnation pressures that compress the magnetic field to the order of 10 Tesla, and large space-charge and particle current effects throughout the accelerating region. These diodes have required new theories and models to account for effects that previously were unimportant. One of the most important effects of the magnetic field compression and large space-charge has been impedance collapse. The impedance collapse can lead to poor energy transfer efficiency, beam debunching, and rapid change of the beam focus. This paper discusses our current understanding of these effects, some of the methods we are using to ameliorate them, and the future directions our theory and modeling will take. 40 refs., 6 figs.

A new scanning electron microscopy imaging technique has been developed to examine the logic state of conductors on passivated CMOS integrated circuits. This technique employs a modified Resistive Contrast Imaging system to acquire image data on powered devices. The image is generated by monitoring subtle shifts in the power supply current of an integrated circuit as an electron beam is scanned over the device surface. The images produced with this new technique resemble voltage contrast data from devices with the passivation removed and the surface topography subtracted. Non-destructive applications of this imaging method to functional and failed integrated circuits are described. Possible irradiation effects and methods to minimize them are also discussed. 2 refs., 1 fig.

Transit time, the time from bridgewire burst until breakout of detonation from the output pellet of an exploding bridgewire detonator, was measured as a function of burst current. From this data, in conjunction with known equations for run distance versus pressure, unreacted explosive Hugoniots, and detonation properties of the initial pressing pellet, the run distance in the initial pressing explosive pellet and shock pressure from the exploding bridgewire were determined, both as a function of burst current.

Fifteen years of solar thermal technology development have produced a considerable amount of knowledge relating to the production of electricity from central receiver power plants. This body of knowledge is under examination by researchers from the United States and the Federal Republic of Germany for the purpose of defining the next generation central receiver electricity producers. This second generation power plant is expected to represent a significant step towards commercialization of these systems. During the course of the study, specific activities needed to realize this next-step technology are being defined. The study is an international team effort. Under the International Energy Agency Small Solar Power Systems project, researchers from DLR, Interatom, Sandia National Laboratories, and Bechtel have designed a study in which technologies relating to existing systems are quantified, logical next-step systems are characterized, and future potential advances are identified. The receiver concepts under investigation are: salt-in- tube, volumetric, and direct absorption. Two plant performance levels are examined, 30 and 100 MW{sub e}. Each concept is applied with common capacity factors, solar multiples, and types and sizes of heliostats at each performance level. Availability and uncertainty analyses are also performed. Annual energy production figures are calculated using the SOLERGY computer code. Capital and Operation and Maintenance cost methodologies are mutually agreed upon in order that levelized energy cost calculations will be consistent for each power plant. During the course of this effort, further potential advances in central receiver technology have continued to become apparent. These possible areas for improvement will be described. An additional comparison is being made between central receivers and trough-based systems. 8 refs., 2 figs.

A hierarchical control architecture for telerobotic vehicles intended to yield a modular, flexible, and easily expanded control system is presented. This architecture is proposed for applications where simple teleoperation is required but where additional capabilities might be quickly added without major changes to the control system. Similarities to the NASREM architecture are noted. Results are given from hardware implementation of the control system on a telerobotic vehicle, Raybot, at Sandia National Laboratories.

A systematic study is described which addresses the technical issues associated with launching flier-plates intact to hypervelocitites. First, very high pressures are needed to launch the flier plates to hypervelocitites, and second this high pressure loading must be uniform and nearly shockless. To achieve both these criteria, a graded-density material referred to as a pillow'' is used to impact a flier plate. When this graded-density material is used to impact a flier plate at high velocities on a two-stage light-gas gun, nearly shockless megabar pressure pulses are introduced into the flier plate. Since the loading on the flier plate is shockless, melting of the flier plate is prevented. This technique has been used to launch a 2-mm thick titanium alloy (Ti-6Al-4V) plate to a velocity of 8.1 km/s, and a 1-mm thick aluminum alloy (6061-T6) plate to a velocity of 10.4 km/s. A method is described by which the flier plate velocities could be further augmented to velocities approaching 14 km/s. 18 refs., 16 figs.

A new technique is reported for the rapid determination of interstitial oxygen (O{sub i}) in heavily doped n{sup +} and p{sup +} silicon. This technique includes application of a selective electrochemical thinning (SET) process and FTIR transmittance measurement on a limited area of a silicon wafer. The O{sub i} is calculated using ASTM F1188--88 with the IOC 88 calibration factor. An advantage of SET over mechanical thinning is that the original wafer thickness and diameter are maintained for additional processing. 1 tab.

The Shippable Storage Cask Demonstration Project is intended to demonstrate casks which can be used for both shipping and storing spent nuclear fuel assemblies. The demonstration included the requirement that the casks be certified for shipping by the US Nuclear Regulatory Commission (NRC). After a lengthy review process which resulted in the resolution of several important technical issues, designs for two similar casks have been certified. This paper describes the certification phase of the demonstration. Based on experience gained during certification phase of the demonstration. Based on experience gained during certification, observations and recommendations have been developed which can benefit others seeking NRC approval of transportation cask designs.

Reviews of normal breakdown and current induced avalanche breakdown mechanisms in silicon power transistors are presented. We show the applicability of the current induced avalanche model to heavy ion induced burnouts. Finally, we present solutions to current induced avalanche in silicon power semiconductors. 7 refs., 5 figs.

The electronic properties of heavily and orderly Si-doped nipi structures in GaAs are studied theoretically using the ab-initio self-consistent pseudopotential method within the local density approximation. Two nipi configurations are considered. Besides investigating the nature of the impurity-related band edge states, the xy-planar-averaged local ionic and self-consistent potentials are also analyzed. The screening effect of the host crystal on the doping induced potential is found to be small. The effects of the doping induced electric field and the strain due to dopings are also examined. 13 refs., 9 figs., 2 tabs.

The near field surrounding buried waste in the proposed high level nuclear waste repository in Yucca Mountain, Nye County, Nevada, is a region where strongly heat driven processes can exist. These strongly heat driven processes further complicate an already very difficult problem, i.e,. predicting groundwater flow and chemical transport through unsaturated fractured, heterogeneous porous media. The coupling between fluid flow and heat emanation is central to understanding these strongly heat driven processes. Although it is important that all of couplings be investigated, the intent of this paper is to discuss the mathematical models and associated computer codes that can be used in investigating the coupled heat emanation and fluid flow in unsaturated porous media. The information in this paper should be useful to those studying these phenomena, validating these models, or investigating the coupling of fluid flow and heat emanation with the other phenomena. The codes implementing these models are commonly referred to as nonisothermal two-phase flow codes. 5 refs., 4 tabs.

The United States Department of Energy (DOE) is developing the Waste Isolation Pilot Plant (WIPP), located in southeastern New Mexico, for disposal of transuranic wastes generated by defense programs. The DOE must first demonstrate compliance with the Environmental Protection Agency's (EPA) Environmental Standards for the Management and Disposal of Spent Nuclear Fuel, High-Level and Transuranic Radioactive Wastes hereafter called the Standard. The Containment Requirements in Subpart B of the Standard set limits on the probability that cumulative radionuclide releases to the accessible environment during the 10,000 years following decommissioning of the repository will exceed certain limits. To comply with these requirements, performance assessments must construct a modeling system that can adequately simulate all realistic future states of the repository that might result in radionuclide releases. Because the regulatory limits are probabilistic, performance assessments must accurately reflect variability and uncertainty within all factors that contribute to the simulation, including variability and uncertainty within all factors that contribute to the simulation, including variability in material properties, probabilities of future human actions, and uncertainties inherent in the conceptual and numerical models that simulate reality. This paper describes conceptual and numerical improvements in the performance assessment methodology made during 1990, and summarizes the present status of WIPP performance assessment. All results to date are preliminary, and cannot be used to determine compliance or non-compliance. The DOE anticipates determining compliance after evaluating a final performance assessment in 1994. 11 refs., 3 figs.

Low pressure (200 Torr) metalorganic chemical vapor deposition (MOCVD) of InSb has been examined through variation of the Column III (TMIn) and Column V (TMSb or TESb) precursor partial pressures. The use of lower growth pressure significantly enhanced the range of allowable Column III Column V partial pressures in which specular morphology InSb could be obtained without the formation of In droplets or Sb crystals. In addition, a 70% improvement in the average hole mobility was obtained, compared to InSb grown in the same reactor at atmospheric pressure. SIMS analysis revealed that Si at the substrate/epitaxial layer interface is an important impurity that may contribute to degradation of the mobility. Substitution of TESb for TMSb did not result in any improvement in the purity of the InSb. 6 refs.

The long length and relatively small cross sectional area of the robotic arms envisioned for use inside of the underground nuclear waste storage tanks will require the control of flexible structures. This will become an important problem in the characterization and remediation of these tanks. We are developing control strategies to actively damp residual vibrations in flexible robotic arms caused by high speed motion and abrupt external forces. A planar, two-link flexible arm is currently being used to test these control strategies. In this paper, two methods of control are discussed. The first is a minimum-time control approach which utilizes a finite element model and and optimization program. These tools plan the motor torque profiles necessary for the tip of the arm to move along a straight line, in minimum time, within the motors' torque constraints, and end in a quiescent state. To account for modeling errors in the finite element model, errors in joint angles, velocities, and link curvatures are added to the optimal torque trajectory. Linear quadratic Gaussian (LQG) regulatory design theory is used to determine the feedback gains. The second method of control is a teleoperated joystick controller which uses an input shaping technique to alter the commands of the joystick so as to reduce the residual vibration of the fundamental modes. Approximating the system as linear, the natural frequency and damping ratio are estimated on-line for the complete system, which includes the structure plus a lower level proportional derivative controller. An input shaping filter is determined from the estimated natural frequency, estimated damping ratio, and the desired transfer function of the system. 11 reps., 9 figs.

The concept of solar driven chemical reactions in a commercial-scale volumetric receiver/reactor on a parabolic concentrator was successfully demonstrated in the CAtalytically Enhanced Solar Absorption Receiver (CAESAR) test. Solar reforming of methane (CH{sub 4}) with carbon dioxide (CO{sub 2}) was achieved in a 64-cm diameter direct absorption reactor on a parabolic dish capable of 150 kW solar power. The reactor was a catalytic volumetric absorber consisting of a multi-layered, porous alumina foam disk coated with rhodium (Rh) catalyst. The system was operated during both steady-state and solar transient (cloud passage) conditions. The total solar power absorbed reached values up to 97 kW and the maximum methane conversion was 70%. Receiver thermal efficiencies ranged up to 85% and chemical efficiencies peaked at 54%. The absorber performed satisfactorily in promoting the reforming reaction during the tests without carbon formation. However, problems of cracking and degradation of the porous matrix, nonuniform dispersion of the Rh through the absorber, and catalyst deactivation due to sintering and possible encapsulation, must be resolved to achieve long-term operation and eventual commercialization. 17 refs., 11 figs., 1 tab.

We have performed MD simulations of adhesive phenomena, on an atomic scale, between metals possessing both smooth and stepped-surfaces. Studies of adhesion between identical metals, consisting of either Au, Cu, or Ni, with (001) or (111) orientations, reveal the existence of adhesive avalanches as the bodies are brought to within a critical separation ({approximately}2 {angstrom}). That is, as the surfaces approach one another, one or both surface layers becomes unstable, and abruptly moves toward the other. This signals a transition from an initial system with two distinct surfaces to one possessing no identifiable surfaces. The presence of adhesive avalanches will pose difficulties in determining adhesive forces and energies by means of atomic force microscopy at sub-nanometer separations of probe tip and sample surface. 7 refs., 3 figs.

An improved standard total-dose test method is described to qualify electronics for a low-dose radiation environment typical of space systems. The method consists of {sup 60}Co irradiation at a dose rate of 1--3 Gy(Si)/s (100--300 rad(Si)/s) and a subsequent 373 K (100{degree}C) bake. New initiatives in radiation hardness assurance are also briefly discussed, including the Qualified Manufacturers List (QML) test methodology and the possible use of 1/f noise measurements as a nondestructive screen for oxide-trap charge related failure. 8 refs.

A two-stage data compression technique that provides for exact, bit-for-bit recovery is described. The first stage is a modified form of conventional linear prediction which generates an error or residue sequence in such a way that exact reconstruction of the original data sequence can be accomplished with a simple recovery algorithm. The second stage is bi-level sequence coding. Even though the residue sequence from the first stage is essential white and Gaussian with seismic or other similar waveform data, bi-level sequence coding will generally provide further compression. The complete technique is described briefly in this summary, and examples of its performance are presented. A full paper on the algorithm is available from the author. 12 refs., 2 figs., 2 tabs.

We have synthesized a new tool, a lasing phase diagram, for designing high efficiency surface-emitting laser resonators and have demonstrated its usefulness by fabricating and operating many different laser resonators. 4 refs., 4 figs.

This paper is concerned with controlling the morphology of microporous polymers prepared via thermal demixing of solutions. 2 wt % solutions of poly(acrylonitrile) in maleic anhydride, a poor solvent, are first cooled to produce separated polymer-rich and solvent-rich phases. Removing the solvent by freeze drying then produces a microporous material having a density of 33 mg/cm{sup 3}, a void fraction of 97%, and a pore size of about 10 {mu}m. We find that the morphology cannot be explained by existing models, which focus on phase diagrams and kinetics of phase transformations during cooling of the solution. In conflict with those models, we find that two radically different morphologies can be produced even when the polymer concentration and cooling path are held strictly constant. A hypothesis that polymer degradation causes the different morphologies is not supported by GPC, {sup 13}C NMR, and FTIR experiments. Instead, we offer evidence that the different microporous morphologies are caused by different polymer conformations in solutions having the same concentration and temperature. 11 refs., 3 figs.

The nuclear industry uses sensitive or classified parts and material that must be protected and accounted for. We believe there is a need for an automated system that can help protect and inventory these parts and material. In response to this need Sandia National Laboratories Division 5245 is developing a personnel and material tracking system named PAMTRAK to safeguard sensitive parts and material at selected Department of Energy facilities. This paper describes the project's background, design goals and features.