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Acquisition of Real-Time Operation Analytics for an Automated Serial Sectioning System

Integrating Materials and Manufacturing Innovation

Madison, Jonathan D.; Poulter, Gregory A.; Huffman, Elizabeth M.

Mechanical serial sectioning is a highly repetitive technique employed in metallography for the rendering of 3D reconstructions of microstructure. While alternate techniques such as ultrasonic detection, micro-computed tomography, and focused ion beam milling have progressed much in recent years, few alternatives provide equivalent opportunities for comparatively high resolutions over significantly sized cross-sectional areas and volumes. To that end, the introduction of automated serial sectioning systems has greatly heightened repeatability and increased data collection rates while diminishing opportunity for mishandling and other user-introduced errors. Unfortunately, even among current, state-of-the-art automated serial sectioning systems, challenges in data collection have not been fully eradicated. Therefore, this paper highlights two specific advances to assist in this area; a non-contact laser triangulation method for assessment of material removal rates and a newly developed graphical user interface providing real-time monitoring of experimental progress. Furthermore, both are shown to be helpful in the rapid identification of anomalies and interruptions, while also providing comparable and less error-prone measures of removal rate over the course of these long-term, challenging, and innately destructive characterization experiments.

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The automation of the Facility for Atmospheric Corrosion Testing (FACT)

Poulter, Gregory A.

An interactive computerized and automated system to provide environmental control for atmospheric corrosion experiments has been added to the FACT, as well as computerized data acquisition for sample weighing. The FACT allows control of corrosive gas concentrations to simulate industrial atmospheric conditions and requires constant manual adjustment to provide a stable test environment. Because constant manual adjustment is impractical, we have automated this facility to achieve the desired stability. This system incorporates an IBM PC AT using Keithley's Series 500 hardware and Quick500 software development environment to calibrate gas analyzers, and to monitor exposure time, test chamber temperature, and gas concentrations. A second PC has been connected to a Mettler M3 microbalance through an IEEE-488 interface communicating under Lotus Measure. Weighings with a sensitivity of 1 {times} 10{sup {minus}6} gram are transferred directly into a Lotus 123 spreadsheet where the data can then be easily manipulated and plotted. Under computer control, the FACT can now run unattended for more than a week and maintain much better control over gas concentrations (200 {plus minus} 5 ppb and 10 {plus minus} 0.5 ppb for NO{sub 2} and H{sub 2}O and H{sub 2}S, respectively) than was possible with manual control (100 {plus minus} 25 ppb for either gas), after initial stabilization. 9 figs.

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6 Results
6 Results