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Implications of Fatigue-Crack Healing in Nanocrystalline Metals [Slides]

Boyce, Brad B.; Barr, Christopher M.; Duong, Ta; Bufford, Daniel C.; Molkeri, A.; Heckman, Nathan H.; Adams, David L.; Hattar, Khalid M.; Demkowicz, Michael J.

Under high-cycle fatigue conditions, a fatigue crack in nanocrystalline Pt was observed to undergo healing. The healing appears to occur by cold welding, facilitated by grain boundary migration, and also by local closure stresses. The healing may help explain several observations: role of air (or vacuum) on fatigue life, impeded subsurface fatigue cracking, apparent flaw healing in sub-critical cycling of ceramics, the existence of a fatigue threshold, and the role of vacuum on the fatigue threshold.

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Long-Term Stability of PVD/Sputtered Au Electrical Contacts to Thermoelectric Bi2Te2 (Re-evaluation of SAND2015-7203)

Sugar, Joshua D.; Bartelt, Norman C.; Sharma, Peter A.; Adams, David L.; Michael, Joseph R.

The fabrication of long-lived electrical contacts to thermoelectric Bi2Te3-based modules is a challenging problem due to chemical incompatibilities and rapid diffusion rates. Previously, technical guidance from SAND report 2015-7203 selected electroplated Au as the preferred method for fabrication of long-lived contacts because of concerns that the grain structure of sputtered/physical vapor deposited (PVD) Au contacts can evolve during aging. We have re-evaluated PVD Au contacts and show that they are appropriate for long-life service. We measure grain size and morphology at different aging times under accelerated temperature gradient conditions, and we show that the PVD Au contacts are stable and remain relatively unchanged. The PVD Au fabricated here is not subject to the deterioration observed in the previous report.

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5 Results
5 Results