Publications

The irradiation embrittlement of neutron shield tank (NST) material (A212 Grade B steel) from the Shippingport reactor has been characterized. Irradiation increases the Charpy transition temperature (CTT) by 23--28{degrees}C (41--50{degrees}F) and decreases the upper-shelf energy. The shift in CTT is not as severe as that observed in high-flux isotope reactor (HFIR) surveillance specimens. However, the actual value of the CTT is higher than that for the HFIR data. The increase in yield stress is 51 MPa (7.4 ksi), which is comparable to HFIR data. The NST material is weaker in the transverse orientation than in the longitudinal orientation. Some effects of position across the thickness of the wall are also observed; the CTT shift is slightly greater for specimens from the inner region of the wall. Annealing studies indicate complete recovery from embrittlement after 1 h at 400{degrees}C (752{degrees}F). Although the weld metal is significantly tougher than the base metal, the shifts in CTT are comparable. The shifts in CTT for the Shippingport NST are consistent with the test and Army reactor data for irradiations at <232{degrees}C (<450{degrees}F) and show very good agreement with the results for HFIR A212-B steel irradiated in the Oak Ridge Research Reactor (ORR). The effects of irradiation temperature, fluence rate, and neutron flux spectrum are discussed. The results indicate that fluence rate has no effect on radiation embrittlement at rates as low as 2 {times} 10{sup 8} n/cm{sup 2}{center dot}s and at the low operating temperatures of the Shippingport NST, i.e., 55{degrees}C (130{degrees}F). This suggests that the accelerated embrittlement of HFIR surveillance samples is most likely due to the relatively higher proportion of thermal neutrons in the HFIR spectrum compared to that for the test reactors. 28 refs., 25 figs.

An analysis of thermosyphoning in a stream generator model is presented. The model considers the transient development of buoyancy-driven steam flow in the steam generator tubing, secondary side heat transfer and an inlet plenum mixing model. Numerical solutions are obtained for conditions intended to simulate the natural circulation phenomena in a 3-Loop pressurized water reactor in a loss-of-coolant accident scenario. The relation between the circulation rate and the heating rate is determined. The sensitivity of the model to various key parameters is examined. 16 refs.

The drive designed and built by the Solar Power Engineering Company (SPECO) for its large area heliostat failed under high wind loads during a winter storm. This report details the testing and analysis done to verify the load capabilities of the rebuilt heliostat drive. Changes in design and improvements in fabrication resulted in a usable drive. 12 figs., 7 tabs.

Data are presented from the 18 W/m{sup 2} Mockup for Defense High-Level Waste, a very large scale in situ test fielded underground at the Waste Isolation Pilot Plant (WIPP). These data include selected fielding information, test configuration, instrumentation activities, and comprehensive results from a large number of gages. The results in this report give measured data from the mechanical response gages, i.e., room closure gages, extensometers, and stress meters emplaced in the test. Construction of the test began in June 1984; gage data in this report cover the complete test duration, that is, to June 1990.

Coaxial transmission cells have been developed for testing optical fiber current sensors. Three of these cells are airlines that provide transverse electromagnetic mode operation to 1.0, 2.3, and 13.7 GHz. Standing wave ratios are <1.5 for the unloaded airlines over their given frequency ranges. Solid and liquid dielectric coaxial cells use materials with high relative permittivities, >9.1. A ceramic test cell has a useful frequency range to 2.5 GHz; the liquid cells, filled with propanol, methanol, or water, are good to {approximately}500 MHz. The properties of the liquid cells are described using a model of a multilayer coaxial dielectric system with complex relative permittivities. 15 refs.

Structural calculations were performed to evaluate the source-term nuclear fuels transport cask (ST Cask) under various hypothetical accident scenarios. (1) Three-dimensional transient dynamic analyses were performed to evaluate the strength of the cask`s end-closure clamp mechanism. The calculations were performed for two impact orientations: a side impact and a 20{degrees} corner impact. The calculations identified three weaknesses in the clamp design: a gap designed between the clamp and the cask provides a deformation mode which loosens the clamp, two unconstrained swing bolts used to fasten the clamp can lose preload and come free; and insufficient stiffness of the clamp in torsion. (2) An axisymmetric finite element model was used to evaluate the dynamics of end-drops from 5 and 10 ft. The calculations show that loads generated in the end-drops could break the payload support cable and damage the payload winch. Lead slump resulted in both end-drop calculations. The stresses generated in the cask wall during the end-drops was insufficient to cause buckling. (3) To determine the factor of safety to yield, calculations in which the cask was treated as a beam loaded under its own weight were performed for two support configurations: simply supported at both ends and simply supported at the center (trunnion loading). (4) The survival of the cask from a 1-m drop onto a mild steel punch was evaluated based on equations derived from empirical data. The calculations showed that the ST Cask could survive such an event. (5) Finally, the bolt configuration for the upper-closure was analyzed and determined to be inadequate because it does not prevent the closure from sliding relative to the cask body. Specific recommendations for design changes are made in the report to eliminate identified problems.

A major thrust of the Atmospheric Radiation Measurements (ARM) Program is the establishment of 5 primary and 4 supplementary Cloud and Radiation Testbed (CART) sites. The CART sites will provide the means to acquire the necessary data to test and further develop the components of GCMs (General Circulation Models) which describe the relationships between the characteristics of the atmosphere and the solar and thermal radiation which passes through it. The CART Locale Recommendation Team has presented a priority-ordered set of recommended locales for the primary and supplementary sites, along with alternatives for each. The selection was based primarily on the following criteria: geographical and climatological homogeneity; occurrence of climatologically important cloud types; seasonal change of surface properties; variability of radiatively-active atmospheric components; synergism with other programs; and manageable logistics. An additional criterion was that, taken together, the set of recommended locales must span a broad range of climate regimes. The recommended primary locales include two land and three ocean locales. The first CART Site will be established in the Southern Great Plains (SGP) of the US. The next CART site to be established on land is to be in the polar regions, on the North Slope of Alaska (NSA).

Thermal and mechanical models for intact and jointed rock mass behavior are being developed, verified, and validated at Sandia National Laboratories for the Yucca Mountain Site Characterization Project. Benchmarking is an essential part of this effort and is one of the tools used to demonstrate verification of engineering software used to solve thermomechanical problems. This report presents the results of the third (and final) phase of the first thermomechanical benchmark exercise. In the first phase of this exercise, nonlinear heat conduction code were used to solve the thermal portion of the benchmark problem. The results from the thermal analysis were then used as input to the second and third phases of the exercise, which consisted of solving the structural portion of the benchmark problem. In the second phase of the exercise, a linear elastic rock mass model was used. In the third phase of the exercise, two different nonlinear jointed rock mass models were used to solve the thermostructural problem. Both models, the Sandia compliant joint model and the RE/SPEC joint empirical model, explicitly incorporate the effect of the joints on the response of the continuum. Three different structural codes, JAC, SANCHO, and SPECTROM-31, were used with the above models in the third phase of the study. Each model was implemented in two different codes so that direct comparisons of results from each model could be made. The results submitted by the participants showed that the finite element solutions using each model were in reasonable agreement. Some consistent differences between the solutions using the two different models were noted but are not considered important to verification of the codes. 9 refs., 18 figs., 8 tabs.

Licensing of the potential nuclear-waste repository at Yucca Mountain by the Nuclear Regulatory Commission would require, among other things, demonstrations of the long term usability of the underground facilities. Such a demonstration involves analysis of the mechanical response of the rock to the presence of underground openings and heat-producing waste, which in turn requires data on the mechanical properties of the rock. This document describes the experimental results from a scoping study which led to the development of procedures for performing quality-affecting rock-mechanics experiments on intact rock. The future experiments performed with these procedures will produce information on the time-dependent deformation of welded tuff and represent one aspect of the overall effort to characterize the rheology of the rock mass. 3 refs., 42 figs., 6 tabs.

This report describes a joint shear model used in conjunction with a computational model for jointed media with orthogonal joint sets. The joint shear model allows nonlinear behavior for both joint sets. Because nonlinear behavior is allowed for both joint sets, a great many cases must be considered to fully describe the joint shear behavior of the jointed medium. An extensive set of equations is required to describe the joint shear stress and slip displacements that can occur for all the various cases. This report examines possible methods for simplifying this set of equations so that the model can be implemented efficiently form a computational standpoint. The shear model must be examined carefully to obtain a computationally efficient implementation that does not lead to numerical problems. The application to fractures in rock is discussed. 5 refs., 4 figs.

Sandia National Laboratories has completed a requirements study for a networked mass storage system. The areas of user functionality, network connectivity, and performance were analyzed to determine specifications for a Network Storage Service to operate in supercomputer environment. 4 refs.

The Network File System (NFS) is used in UNIX-based networks to provide transparent file sharing between heterogeneous systems. Although NFS is well-known for being weak in security, it is widely used and has become a de facto standard. This paper examines the user authentication shortcomings of NFS and the approach Sandia National Laboratories has taken to strengthen it with Kerberos. The implementation on a Cray Y-MP8/864 running UNICOS is described and resource/performance issues are discussed. 4 refs., 4 figs.

Ground water flow in unsaturated, fractured rock is often assumed to be dominated by the porous matrix component. This is frequently based on the argument that water flowing in the fractures is rapidly imbibed into the rock matrix by capillary suction forces with negligible resistance to uptake at the matrix-fracture interface. However, the existence of a low-permeability mineralized layer or coating at this interface may substantially reduce matrix imbibition and consequently result in fracture-dominated flow. To test this concept, four tuff samples containing natural fractures were obtained from tuff formations in southern Nevada. By performing imbibition experiments into the matrix rock, across a mineralized fracture face and then across a fresh uncoated fracture face, water uptake as a function of time and coating was measured. A relatively simple model has been developed to describe the imbibition behavior. 6 refs.

An important aspect of environmentally-conscious operations is adoption of an aggressive waste minimization program. This paper describes the waste minimization and pollution prevention program at Sandia National Laboratories. Although Sandia's approach is patterned after the generic waste minimization models proposed by the Environmental Protection Agency and the Department of Energy, the specifics of implementation, and the potential for payoff, are influenced by the R&D nature of Sandia's work. Key aspects of the program are discussed, including why Sandia is developing and conducting the program; objectives; elements of the program; our approach to implementation; the magnitude of the undertaking; and the expected payoff.

The distribution of copper in aluminum thin films is examined with respect to how the copper can influence electromigration behavior. Al-Cu thin films annealed in the single-phase region, to just below the solvus temperature, have θ-phase Al₂Cu precipitates at the aluminum grain boundaries. The grain boundaries between precipitates are depleted in copper. Al-Cu thin films heat treated at lower temperatures, within the two-phase region, also have θ-phase precipitates at the grain boundaries but the aluminum grain boundaries continuously become enriched in copper, perhaps due to the formation of a thin coating of θ-phase at the grain boundary. Here, it is proposed that electromigration behavior of aluminum is improved by adding copper because the θ-phase precipitates may hinder aluminum diffusion along the grain boundaries. It was also found that resistivity of Al-Cu thin films decrease during accelerated electromigration testing prior to failure. Pure Al films did not exhibit this behavior. The decrease in resistivity is attributed to there distribution of copper from the aluminum grain matrix to the θ-phase precipitates growing at the grain boundaries thereby reducing the number of defects in the microstructure.

We have designed and manufactured a test chip devoted to the study of interconnect voiding. The test chip is suitable for evaluating theoretical models, acceleration recipes, and the effects of process variations. We describe the chip and a simple, stress-free packaging technique that eliminates any stress to the chip from die bonding or packaging thermal cycles. With this test chip, we can perform many necessary and desirable experiments: determining stress, observing or stimulating void growth, profiling hydrogen concentrations, and measuring excess current noise. We report here preliminary measurements of residual stress, observations of voids, and determinations of hydrogen concentrations of hydrogen concentration under variations in aluminum annealing and passivation. In agreement with observations elsewhere, we find that passivations which differ greatly in intrinsic stress do not differ much in the stress they impart to patterned metal; some workers have suggested instead that excess hydrogen in the aluminum contributes to voiding. Following this lead, we have used nuclear reaction analysis to profile the hydrogen concentration in passivation, metallization, barrier metal, and interlevel dielectric and present some preliminary measurements here. We conclude that passivated metallization may contain as much as 0.1 atomic % hydrogen.

The current status of lifetime prediction under conditions of thermomechanical creep/fatigue is reviewed. Each method is summarized and the results of the application to solder joints is shown. While each method has been applied with some success, a predictive, phenomenological approach has not been developed and validated. A method which captures the response of a crack to steady-state and cycling environments appears to hold most the most promise to provide a useful design tool.

We present a simple and effective path planning algorithm, an essential component in facilitating robot programming, based on a series of plausible task restriction. It is designed to solve realistic'' problems very quickly, at the expense of not being able to solve every problem. First, the notion of realistic'' problems is motivated with heuristic arguments and formalized through task restrictions. Next, an algorithm solving the resulting tasks of interest is provided. We prove its corrections and theoretical efficiency, and demonstrate empirically its effectiveness and speed. We expect our algorithm to be of practical significance based on its simplicity and predicted performance. 9 refs., 7 figs.

To address the need of a practical motion planner for manipulators, we present an efficient and resolution-complete algorithm that has performance commensurate with task difficulty. The algorithm uses SANDROS, a new search strategy that combines hierarchical, nonuniform-multi-resolution, and best-fit search to find a near-optimal solution in the configuration space. This algorithm can be applied to any manipulator, and has been tested with 5 and 6-degree-of-freedom robots, with execution time ranging from 20 seconds to 10 minutes on a 16 MIPS workstation. 14 refs., 3 figs., 1 tab.

Activation procedures can have a dramatic effect on the activity of iron-based catalysts for Fischer-Tropsch (F-T) synthesis. CO conversion over a 100 Fe/3 Cu/0.2 K catalyst (parts by weight) can vary by nearly a factor of 3, depending on activation treatment. In contrast, a 100 Fe/5 Cu/4.2 K/25 SiO₂ catalyst displays little dependence of F-T activity on activation treatment. An ultra-high vacuum surface analysis chamber coupled to an atmospheric reactor has been used to measure the surface composition of these catalysts following activation in carbon monoxide at 280°C, while transmission electron microscopy (TEM) and BET surface area measurements have been used to investigate catalyst morphology. CO activation of the 100 Fe/5 Cu/4.2 K/25 SiO₂ catalyst at 280°C results in partial reduction of iron to a mixture of Fe_xO and Fe₃O₄, and an overall surface composition very similar to that obtained following hydrogen activation at 220 or 280°C, consistent with the invariance of F-T activity with activation treatment for this catalyst. Activation of the 100 Fe/3 Cu/0.2 K catalyst in CO at 280°C results in the formation of iron carbide particles, growth of graphitic carbon (C_g) filaments, and formation of a thick, porous, Cg layer covering the carbide particles. Differences in F-T activity between the hydrogen- and CO-activated 100 Fe/3 Cu/O.2 K catalyst are discussed in terms of surface composition and catalyst morphology. The difference in sensitivity of the two catalysts to activation conditions is related to differences in the extent of reduction of the catalysts.

HISPLT is a graphics postprocessor designed to plot time histories for wave propagation codes. HISPLT is available for CRAY UNICOS, CRAY CTSS, VAX VMS computer systems, and a variety of UNIX workstations. The original HISPLT code employs a database structure that allows the program to be used without modification to process data generated by many wave propagation codes. HISPLT has recently been modified to process time histories for the reactor safety analysis code, MELCOR. This report provides a complete set of input instructions for HISPLT and provides examples of the types of plotted output that can be generated using HISPLT. 6 refs., 8 figs., 5 tabs.

The purpose of this NUREG is to present technical information that should be useful to NRC licensees in designing closed-circuit television systems for video alarm assessment. There is a section on each of the major components in a video system: camera, lens, lighting, transmission, synchronization, switcher, monitor, and recorder. Each section includes information on component selection, procurement, installation, test, and maintenance. Considerations for system integration of the components are contained in each section. System emphasis is focused on perimeter intrusion detection and assessment systems. A glossary of video terms is included. 13 figs., 9 tabs.

Blade fatigue life is an important element in determining the economic viability of the Vertical-Axis Wind Turbine (VAWT). A principal source of blade fatigue is thought to be the stochastic (i.e., random) aerodynamic loads created by atmospheric turbulence. This report describes the theoretical background of the VAWT Stochastic Aerodynamic Loads (VAWT-SAL) computer code, whose purpose is to numerically simulate these random loads, given the rotor geometry, operating conditions, and assumed turbulence properties. A Double-Multiple-Stream Tube (DMST) analysis is employed to model the rotor's aerodynamic response. The analysis includes the effects of Reynolds number variations, different airfoil sections and chord lengths along the blade span, and an empirical model for dynamic stall effects. The mean ambient wind is assumed to have a shear profile which is described by either a power law or a logarithmic variation with height above ground. Superimposed on this is a full 3-D field of turbulence: i.e., in addition to random fluctuations in time, the turbulence is allowed to vary randomly in planes perpendicular to the mean wind. The influence of flow retardation on the convection of turbulence through the turbine is also modeled. Calculations are presented for the VAWT 34-m Test Bed currently in operation at Bushland, Texas. Predicted time histories of the loads, as well as their Fourier spectra, are presented and discussed. Particular emphasis is placed on the differences between so-called steady-state'' (mean wind only) predictions, and those produced with turbulence present. Somewhat surprisingly, turbulence is found to be capable of either increasing or decreasing the average output power, depending on the turbine's tip-speed ratio. A heuristic explanation for such behavior is postulated, and a simple formula is derived for predicting the magnitude of this effect without the need for a full stochastic simulation. 41 refs., 32 figs., 1 tab.

Division 2525 Battery Test Laboratory is a fully automated battery testing facility used in evaluating various battery technologies. The results of these tests are used to verify developers' claims, characterize prototypes, and assist in identifying the strengths and weaknesses of each technology. The Test Facility consists of a central computer and nine remote computer controlled battery test systems. Data acquired during the battery testing process is sent to the central computer system. The test data is then stored in a large database for future analysis. The central computer system is also used in configuring battery tests. These test configurations are then sent to their appropriate remote battery test sites. The Battery Test Facility can perform a variety of battery tests, which include the following: Life Cycle Testing; Parametric Testing at various temperature levels, cutoff parameters, charge rates, and discharge rates; Constant Power Testing at various power levels; Peak Power Testing at various State-of-Charge levels; Simplified Federal Urban Driving Schedule Tests (SFUDS79). The Battery Test Facility is capable of charging a battery either by constant current, constant voltage, step current levels, or any combination of them. Discharge cycles can be by constant current, constant resistance, constant power, step current levels, or also any combination of them. The Battery Test Facility has been configured to provide the flexibility to evaluate a large variety of battery technologies. These technologies include Lead-Acid, Sodium/Sulfur, Zinc/Bromine, Nickel/Hydrogen, Aluminum/Air, and Nickel/Cadmium batteries.

PRONTO 3D is a three-dimensional transient solid dynamics code for analyzing large deformations of highly nonlinear materials subjected to high strain rates. It is a Lagrangian finite element program with explicit integration of the equations of motion through time. This report documents the implementation of a four-scale quadrilateral shell element into Version 6.0 of PRONTO 3D. This report describes the theory, implementation and use of a four-node shell element. Also described are the required architectural changes made to PRONTO 3D to allow multiple element types. Several test problems are documented for verification of the PRONTO 3D implementation and for demonstration of computational savings using shell elements for thin structures. These problems also serve as examples for the user. A complete, updated list of the PRONTO 3D input commands is also included.

This purpose of this NUREG is to present technical information that should be useful to NRC licensees for understanding and applying line supervision techniques to security communication links. A review of security communication links is followed by detailed discussions of link physical protection and DC/AC static supervision and dynamic supervision techniques. Material is also presented on security for atmospheric transmission and video line supervision. A glossary of security communication line supervision terms is appended. 16 figs.

This report describes the ranges of the residual contamination that may build up in spent-fuel transport casks. These contamination ranges are calculated based on data taken from published reports and from previously unpublished data supplied by cask transporters. The data involve dose rate measurements, interior smear surveys, and analyses of water flushed out of cask cavities during decontamination operations. A methodology has been developed to estimate the effect of residual contamination on spent-fuel cask containment requirements. Factors in estimating the maximum permissible leak rates include the form of the residual contamination; possible release modes; internal gas-borne depletion; and the temperature, pressure, and vibration characteristics of the cask during transport under normal and accident conditions. 12 refs., 9 figs., 4 tabs.

Chromate conversion coatings such as Parker Company`s Alodine coatings are widely used to increase the corrosion resistance of aluminum and aluminum alloys. The primary disadvantage of chromate-based processes is that they use and produce as waste hexavalent chromium (Cr{sup 6+}). We have discovered that the corrosion resistance of Al can be increased by forming an inorganic barrier coating using chemicals that pose a relatively small environmental hazard. These new coatings are formed using a process that is procedurally identical to the basic chromate conversion process. We have prepared new and conventional coatings on 1100 (99.0 Al minimum), 2024-T3 (Al-Cu-Mg) and 7075-T6 (Al-Zn-Mg) commercial sheet stock for accelerated electrochemical testing and coating conductivity testing. Results show that the new coatings offer increased corrosion resistance compared to uncoated Al, but do not yet match the performance of the chromate conversion coatings. The conductivity of these new films on 1100 Al is comparable to that of Alodine coatings; however, the new coatings are more resistive than Alodine coatings on 2024-T3 and 7075-T6.

A novel technique to monitor thin film deposition has been developed using optical fibers. The system measures the optical thickness of a film and not the physical thickness which results in accurate film deposition for optical applications regardless of deposition conditions. A discussion of the mathematics necessary to understand the operation of the system is presented. The details of the circuitry and software are presented. The performance of the system is then demonstrated for the deposition of SnO{sub 2} on an optical fiber. An analysis of the inherent errors present in the monitor electronics and measurement system and their effects on the accuracy of the deposition is presented. The system is then applied to several practical situations. First, the system is used to monitor the deposition of SnO{sub 2} films on microscope slides. The films on the slides are then shown to have optical thicknesses which are within 1% of the expected values. The system is next used to deposit SiO anti-reflective coatings on Si. The system is then used to monitor the aging effects seen in SiO and SnO{sub 2}. Finally, a seven layer dielectric mirror made from SnO{sub 2} and MgF{sub 2} films is deposited using the monitor. 25 figs., 1 tabs.

The Heat Source/Radioisotopic Thermoelectric Generator shipping counter is a Type B packaging currently under development by Los Alamos National Laboratory. Type B packaging for transporting radioactive material is required to maintain containment and shielding after being exposed to normal and hypothetical accident environments defined in Title 10 of the Code of Federal Regulations Part 71. A combination of testing and analysis is used to verify the adequacy of this packaging design. This report documents the testing portion of the design verification. Six tests were conducted on a prototype package: a water spray test, a 4-foot normal conditions drop test, a 30-foot drop test, a 40-inch puncture test, a 30-minute thermal test, and an 8-hour immersion test.

The MELCOR code has been used to simulate LACE aerosol experiment LA4. In this test, the behavior of single- and double-component, hygroscopic and nonhygroscopic, aerosols in a condensing environment was monitored. Results are compared to experimental data, and to CONTAIN calculations. Sensitivity studies have been done on time step effects and machine dependencies; thermal/hydraulic parameters such as condensation on heat structures and on pool surface, and radiation heat transfer; and aerosol parameters such as number of MAEROS components and sections assumed, the degree to which plated aerosols are washed off heat structures by condensate film draining, and the effect of non-default values for shape factors and diameter limits. 9 refs., 50 figs., 13 tabs.

Early attempts at estimation of stress wave damage due to blasting by use of finite element calculations met with limited success due to numerical instabilities that prevented calculations from being carried past the fragmentation limit. More recently, the improved damage model PRONTO has allowed finite element calculations which remain stable and yield good agreement between calculated fragmented regions and excavated crater profiles for blasting experiments in granite. Application of this damage model to blast experiments at the Straight Creek Mine in Bell County, Kentucky were complicated by anisotropic conditions and uncertainties in material properties. It appears that significant modifications to the damage model and extensive material testing may be necessary in order to estimate damage in these anisotropic materials. 18 refs., 18 figs.

This paper presents a series of experiments in robotic sensori-motor control during grasping. The work utilizes a multifingered, dextrous robot hand equipped with a fingertip force sensor to explore dynamic grasp force adjustment during manipulation. The work is primarily concerned with the relationship between the weight of an object and the grasp force required to lift it. Too weak a grasp is unstable and the object will slip from the hand. Too strong a grasp may damage the object and/or the manipulator. An algorithm is presented which uses tactile information from the sensor to dynamically adjust the grasp force during lift. It is assumed that there is no a priori knowledge about the object to be manipulated. The effects of different arm/hand postures and object surfaces is explored. Finally, the use of sensory data to detect unexpected object motion and to signal transitions between manipulation phases -- with the coincident triggering of new motor programs -- is investigated. 15 refs., 12 figs.

The fabrication of electronic systems has relied upon eutectic tin-lead solder for the attachment of components to printed wiring boards. Higher service temperatures are approaching the durability limits of the eutectic solder. The tin-rich, lead-free solders are being actively studied as alternate alloys. Experiments that examined the wettability of 95Sn-5Sb (wt. %), 95.5Sn-4.0Cu0.5Ag, 96.5Sn-3.5Ag, and the control solder, 60Sn-40Pb, on oxygen-free, high conductivity copper were performed. A rosin based, mildly activated (RMA) flux and three water soluble, organic acid fluxes were used in the wetting balance/meniscometer measurements. The 95.5Sn-4.0Cu-0.5Ag and 95Sn-5Sb alloys exhibited good wetting, with contact angles of 35° < θ_c < 55° as compared to the excellent performance of the 60Sn-40Pb material (20°< θ_c <35°). The fair wettability observed with the 96.5Sn 3.5Ag solder (60° < θ_c <75°) was due in large part to the inability of the fluxes to significantly lower the solder-flux interfacial tension. The wetting rates of the 95.5Sn-4.0Cu-0.5Ag and 95Sn 5Sb solders were comparable to those of the control; the 96.5Sn 3.5Ag alloy wetting rate was slower than the other candidates. The solder film formed on the substrate surface by the 95.5Sn-4.0Cu0.5Ag alloy was very grainy. The water soluble fluxes exhibited a larger degree of residue formation than did the RMA flux.

A parabolized Navier-Stokes analysis of a turbulent, compressible, wake/boundary-layer flow field for a cable in tow is discussed. It is assumed that the cable is being towed by a missile-like configuration whose total drag coefficient is known. The cable is assumed to be perfectly aligned with the missile axis and is subjected to its wake. Modeled in the analysis is the far wake behind the missile, coupled with the turbulent boundary layer growth along the cable. An analytical starting solution for a parabolized Navier-Stokes code is presented. The starting solution is applicable downstream of the towing body's near wake and, therefore, circumvents the complex task of computing the towing body's flow field. An algebraic wake/boundary-layer turbulence model is used to simulate turbulent flow in both the decaying wake and growing boundary layer along the cable. Results are presented for a towing-body freestream Mach number of 5 and a Reynolds number of 36.0 x 10⁶ per ft at select distances along a thin cable.

Parachute system performance issues such as turnover and wake recontact may be influenced by velocities induced by the wake of the delivering aircraft. The magnitude and direction of these aircraft-induced velocities is dependent on the specific delivering aircraft (as characterized by its size, shape, and weight), the aircraft’s speed and flight path (including any maneuvers which it is performing), and the location on the aircraft from which the system is released. In addition, the parachute deployment sequence is of major importance. The most significant effects will tend to occur after parachute deployment since induced velocities from the aircraft may become significant when compared to the velocity of the parachute system. For example, any downwash behind an aircraft will tend to cause a parachute system, which is horizontally deployed, to fly at a more positive angle of attack. As the forward speed of the parachute system decreases after deployment, this induced angle of attack will tend to increase. This effect tends to retard the rate at which the parachute system “turns over” from a horizontal trajectory into a vertical one. On the other hand, a maneuvering aircraft might produce upwash in its wake which would produce an opposite effect. In this case, the turnover rate would be enhanced. Aircraft-induced velocities may also affect the process known as “wake recontact” in which the momentum of the parachute wake causes the wake itself to overtake the parachute. This sometimes causes severe collapse of the canopy such as reported by Spahr and Wolf. Wake recontact may be either hastened or delayed, depending upon the aircraft flight path and the parachute deployment sequence

This paper reviews some of the technical considerations and current practices for testing parachutes in conventional wind tunnels. Special challenges to the experimentalist caused by the fabric construction, flexible geometry, and bluff shape of parachutes are discussed. In particular, the topics of measurement technique, similarity considerations, and wall interference are addressed in a summary manner. Many references are cited which provide detailed coverage of the state of the art in testing methods.

Sandia National Laboratories has performed a series of experiments under the sponsorship of the US Nuclear Regulatory Commission (USNRC) to assess the fire performance of thermally aged electrical cables. Two measures of fire performance were evaluated, namely, (1) the vulnerability of cables to thermal damage and (2) the flammability of cables. In each case, direct comparisons were made between experiments involving unaged (i.e., new off the reel) cables and cables subjected to accelerated thermal aging. The results were evaluated from the perspective of fire risk. It was found that thermal aging did cause changes in the thermal damageability of the cables tested; however, the changes observed are not considered risk significant. Large-scale fire tests demonstrated a clear decrease in material flammability due to thermal aging. Thus, it was concluded that the use of cable thermal damage and flammability information based on the testing of unaged cable samples is an acceptable risk assessment practice. Indeed, in the case of flammability, this is a conservative practice.

Computer networks, supporting an organization's activities, are prevalent and very important to the organization's mission. Implementing a heterogenous organizational network allows the staff to select the computing environment that best supports their job requirements. This paper outlines the lessons learned implementing a heterogenous computer network based on networking standards such as TCP/IP and Ethernet. Such a network is a viable alternative to a proprietary, vendor supported network and can provide all the functionality customers expect in a computer network. 2 figs.

Two experiments, DCH-3 and DCH-4, were performed at the Surtsey test facility to investigate phenomena associated with a high-pressure melt ejection (HPME) reactor accident sequence resulting in direct containment heating (DCH). These experiments were performed using the same experimental apparatus with identical initial conditions, except that the Surtsey test vessel contained air in DCH-3 and argon in DCH-4. Inerting the vessel with argon eliminated chemical reactions between metallic debris and oxygen. Thus, a comparison of the pressure response in DCH-3 and DCH-4 gave an indication of the DCH contribution due to metal/oxygen reactions. 44 refs., 110 figs., 43 tabs.

This Manual is compiled from techniques used in the Industrial Hygiene Chemistry Laboratory of Sandia National Laboratories in Albuquerque, New Mexico. The procedures are similar to those used in other laboratories devoted to industrial hygiene practices. Some of the methods are standard; some, modified to suit our needs; and still others, developed at Sandia. The authors have attempted to present all methods in a simple and concise manner but in sufficient detail to make them readily usable. It is not to be inferred that these methods are universal for any type of sample, but they have been found very reliable for the types of samples mentioned.

The title of this paper might unfairly provoke readers if it conjures up visions of vast stores of high-tech gadgets in several hundred technology warehouses'' (also known as federal laboratories) around the country, open for browsing by those in search of a bargain. That vision, unfortunately, is a mirage. The term technology transfer'' is not really as accurate as is the term technology team-work,'' a process of sharing ideas and knowledge rather than widgets. In addition, instead of discussing the efforts of more than 700 federal labs in the US, I mean to address only those nine government-owned, contractor-operated multiprogram labs run by the Department of Energy. Nevertheless, the topic of technology team-work opportunities with DOE multiprogram national lab is of significance to those concerned with increasing economic competitiveness and finding technological solutions to a host of national problems. A significant fraction of US R D capabilities rests in the nine DOE multiprogram national laboratories -- and these labs have only just begun to join the other federal laboratories in these efforts due to the passage and recent implementation of the National Competitiveness Technology Transfer Act of 1989.

The case and junction temperatures of selected integrated circuits (ICs) on the processor module of the SANDAC V computer were calculated using BETAsoft-R,'' a personal computer, thermal analysis software program. The predicted data was then compared to corresponding IC case temperature measurements from laboratory tests of a functional SANDAC V computer. Although the difference between the actual and calculated values was somewhat higher than expected, the results of the analysis indicate that BETAsoft-R'' identified the critical ICs on the processor module and that it is capable of analyzing printed circuit boards for potential thermal problems before the design layout is finalized. 8 figs., 12 tabs.

Sandia National Laboratories, Albuquerque, may soon have more responsibility for the operation of its own telephone system. The processes that constitute providing telephone service can all be improved through the use of a central data information system. We studied these processes, determined the requirements for a database system, then designed the first stages of a system that meets our needs for work order handling, trouble reporting, and ISDN hardware assignments. The design was based on an extensive set of applications that have been used for five years to manage the Sandia secure data network. The system utilizes an Ingres database management system and is programmed using the Application-By-Forms tools.

Radio-frequency (rf) electrical sources are commonly used to generate plasmas for processing of industrial materials and for related experimental work. Published descriptions of such plasmas usually include generator-power measurements, and occasionally include plasma dc-bias measurements. One or both of these quantitites are also used in industrial feedback ccontrol systems for setpoint regulation. Recent work at Sandia an elsewhere with an experimental rf discharge device (the GEC RF Reference Cell'') has shown that power and dc-bias levels are often insufficient information for specifying the state of the plasma. The plasma can have nonlinear electrical characteristics that cause harmonic generation, and the harmonic levels can depend sensitively on the impedance of the external circuitry at harmonic frequencies. Even though the harmonics may be low in amplitude, they can be directly related to large changes in plasma power and to changes in optical emission from the plasma. Consequently, in order for a worker to truly master the plasma-generation process, it is necessary to understand, measure, and control electrical characteristics of the plamsa. In this paper we describe technique that have been developed from work with the Reference Cell for making electrical measurements on rf plasmas, and we describe surprising observations of harmonic behavior. 10 refs., 4 figs.

The catalytic hydropyrolysis tests performed on coals of varying rank clearly show that high conversions and tar yields can be achieved in a fixed-bed laboratory reactor system. Each of the three types of catalysts utilized, MoS{sub 2} derived from dioxydithiomolybdate, the metal HTO catalysts, and the Pd colloidal catalysts, were shown to be effective for the bituminous coals tested. For the lower rank coals, no significant increase in conversions or tar yields preliminary tests utilizing oil agglomeration as a pretreatment provided encouraging results, with conversions and tar yields achieved similar to using the metal HTO and colloid catalysts. This pretreatment process might be effective for use in catalyst dispersal and coal cleaning, and facilitating coal introduction into a high-pressure reactor. In summary, the data obtained show that catalytic hydropyrolysis on a laboratory scale can achieve the necessary conversions and tar yields to be considered as a potentially viable process for converting coal into liquid products. Through proper dispersal of selected catalysts onto bituminous coals, conversions greater than 80% and tar yields greater than 70% can be achieved at low active metal concentrations. 12 refs., 9 figs., 7 tabs.

Abstract not provided.

The objective of this review is to evaluate the South Texas Project (STP) Probabilistic Safety Analysis (PSA) for the USNRC. The PSA was reviewed for thoroughness of analysis, accuracy in plant modeling, legitimacy of assumptions, and overall quality of the work. The review is limited to the internal event analysis and the fire sequence analysis. This review is not a quantitative evaluation of the adequacy of the PSA. The adequacy of the PSA depends on the intended uses and must be addressed on a case-by-case basis by the licensee and the NRC. This review identifies strengths, weakness, and areas where additional clarification would assist the NRC in evaluating the PSA for specific regulatory purposes. The licensee, Houston Lighting and Power (HL P), reviewed a draft version of this report prior to its final release to the USNRC. The responses provided by HL P are provided in detail in appendices to this report, and they are summarized in the main body of the report. All issues raised during the review were adequately addressed by HL P in the responses. 27 refs., 4 tabs.

Pressure-pulse tests have been performed in bedded evaporites of the Salado Formation at the Waste Isolation Pilot Plant (WIPP) site to evaluate the hydraulic properties controlling brine flow through the Salado. Hydraulic conductivities ranging from about 10{sup {minus}14} to 10{sup {minus}11} m/s (permeabilities of about 10{sup {minus}21} to 10{sup {minus}18} m{sup 2}) have been interpreted from nine tests conducted on five stratigraphic intervals within eleven meters of the WIPP underground excavations. Tests of a pure halite layer showed no measurable permeability. Pore pressures in the stratigraphic intervals range from about 0.5 to 9.3 MPa. An anhydrite interbed (Marker Bed 139) appears to be one or more orders of magnitude more permeable than the surrounding halite. Hydraulic conductivities appear to increase, and pore pressures decrease, with increasing proximity to the excavations. These effects are particularly evident within two to three meters of the excavations. Two tests indicated the presence of apparent zero-flow boundaries about two to three meters from the boreholes. The other tests revealed no apparent boundaries within the radii of influence of the tests, which were calculated to range from about four to thirty-five meters from the test holes. The data are insufficient to determine if brine flow through evaporites results from Darcy-like flow driven by pressure gradients within naturally interconnected porosity or from shear deformation around excavations connecting previously isolated pores, thereby providing pathways for fluids at or near lithostatic pressure to be driven towards the low-pressure excavations. Future testing will be performed at greater distances from the excavations to evaluate hydraulic properties and processes beyond the range of excavation effects.

An all optical circuit in GaAs/AlGaAs for control of phased-array systems using a single photonic integrated circuit chip has the potential for high performance control of phasedarray systems from a small, lightweight, package. Such a circuit based exclusively on combinations of reverse-biased optical phase modulators, waveguide interconnects, corner reflectors, and power splitter combiners with optical-fiber output to the antenna elements has been designed at Sandia National Laboratories. This paper presents some basic features of optical phase modulators for photonic circuit applications and provide relevant performance data as achieved to date. Current structures have been shown to operate with a 76.5°/V-mm figure of merit at 1.06μm and losses as low as 2 cm-1. A novel digital phase shifter to allow direct digital control of phased arrays is also proposed and demonstrated.