Publications

To overcome the heat deficit and oxidizing atmosphere problems and to reduce fuel consumption, a small gas forge furnace has been developed which incorporates recuperative heating; as the combustion air is drawn into the furnace it is preheated by passing it through a simple heat exchanger which is heated by the exhaust gases from the furnace. This recuperative heating principle is the same used by blast and open hearth furnaces but they typically employ complex heat exchangers, and extensive blowers and valving to direct the flow of the intake and exhaust gases. In the furnace described in this article a chimney is provided at the rear of the furnace and the air intake ducts pass through the chimney before reaching the venturi where the fuel gas is injected. Thermocouples were place in the air intake ducts and the temperature of the recuperated air was 1000 F. Based on data in the Mechanical Engineers Handbook (Industrial Heating Furnaces) fuel savings are directly related to the temperature of the preheated air. The theoretical saving in fuel with 800 F. combustion air is about 19%. The furnace is very quiet, since no blowers are used and the venturi is located in the center of a long tube. To control the furnace atmosphere and to help reduce heat loss, a close fitting swing away door has been incorporated, and the entire furnace is insulated with lightweight high performance ceramic insulation. The resulting furnace easily achieves forge welding temperatures, has an oxygen depleted atmosphere and has proven to be very effective and capable for small machine and hand forging operations. 6 figs.

Need for standardization has been discussed for years by many government agencies. In the past, every perimeter site upgrade resulted in the design, specification, procurement, and fabrication of a unique power and signal junction box. To save design and specification cost, a standard terminal panel and uninterruptible power supply (UPS) design for an exterior intrusion sensor detection system was developed for a security system within the Sandia National Laboratories complex at Albuquerque, New Mexico. In facilitating this requirement a design was sought that could easily be modified for other government or commercial applications and one that could easily be fabricated in the shop. Also of primary importance was the need for lightning protection for both the communications and voltage sources. A 12V dc UPS with a current capacity of up to 4 amperes complements the standard terminal design and allows uninterrupted sensor operation for a number of hours should the primary ac source be interrupted. This report encompasses the features of the designs. The designs are also being used and continuously evaluated in Sandia's Area III exterior test field. 7 figs.

Radiation effects on polymers in the presence of air are characterized by complicated phenomena such as dose-rate effects and post-irradiation degradation. These time-dependent effects can be understood in these terms: (1) features of the free radical chain-reaction chemistry underlying the oxidation, and (2) oxygen diffusion effects. A profiling technique has been developed to study heterogeneous degradation resulting from oxygen diffusion, and kinetic schemes have been developed to allow long-term aging predictions from short-term high dose-rate experiments. Low molecular weight additives which act either as free-radical scavengers or else as energy-scavengers are effective as stabilizers in radiation-oxidation environments. Non-radical oxidation mechanisms, involving species such as ozone, can also be important in the radiation-oxidation of polymers. 18 refs., 15 figs.

Introduced in 1951 and 1966 respectively, the field ion microscope and atom-probe mass spectrometer can hardly be considered new or emerging microprobes. Over the years, the ability to use these instruments to examine the structure and composition of various materials at the atomic level has been well established. However,recent advances in more conventional microanalytical techniques, particularly progress toward a higher degree of spatial resolution, has created renewed interest in all techniques capable of analysis on a very fine scale. Also, there has been an increased emphasis over the past several years in the application of the field ion microscope and atom-probe to problems of greater general interest in surface and materials science. It is therefore not totally inappropriate to discuss the field ion microscope and atom-probe within the context of ''emerging'' microprobes. The intent of this paper is to familiarize the reader with the techniques of field ion microscopy and atom-probe mass spectroscopy and describe several recent applications which demonstrate some of their unique attributes. 45 refs., 8 figs.

The Phase Doppler Particle Analyzer (PDPA) is an LDV-based instrument for simultaneous measurement of single particle size and velocity. A PDPA calibration was performed using well-characterized liquid droplets in the 4 to 80 ..mu..m diameter range. Two test liquids were used: oleic acid and kerosene. A standard PDPA instrument and a fiber-optic probe PDPA system were tested. The standard instrument measurements agreed with expected droplet diameters to within the droplet generation accuracy for droplets above 15 ..mu..m diameter, and had a measurement accuracy of about 2 ..mu..m for smaller droplets. The fiber-optic probe system exhibited similar behavior, although the 2 ..mu..m sizing uncertainty extended to droplets as large as 25 ..mu..m. The measurement uncertainties in the small diameter ranges are in qualitative agreement with the light-scattering computations of Al-Chalabi et al. (1988) and Saffman et al. (1984). 7 refs., 4 figs.

This paper reviews several techniques available to the experimenter to characterize the mechanical properties of near surface layers of engineering materials. The test methods examined are: micro-tensile testing, bulge testing, ultra-low load indentation testing, and microfabricated test structures. The applicability of these techniques as well as their advantages and difficulties are examined. Special emphasis is given to recent developments in ultra-low load indentation testing and microfabricated test structures. 61 refs., 2 figs.

The Department of Energy (DOE) established the seals task force in 1986 to scope the extent of seals problems, develop guidelines and criteria, and recommend improvements. Recent task force activities have been to update the Safeguards Seals Reference manual produced in 1986, lay the groundwork for seal standardization, and make recommendations for general and specific seals problems in the field. This paper will discuss the manual updates and other general task force activities. 5 refs.

For years the lighting industry has manually entered and manually performed calculations on the photometric data that is necessary for lighting designs. In the past few years many lighting manufacturers and private lighting design software companies have published computer programs to enter and perform these calculations. Sandia National Laboratories (SNL), and other interested organizations, are involved in outdoor lighting designs for Closed Circuit Television (CCTV) that require lighting design software programs. During the period when no commercial lighting design software programs existed, SNL first used a government agency's program and then developed an in-house program. The in-house program is very powerful but has limitations, so it is not feasible to distribute it to interested organizations. This program has been used extensively for many high security outdoor lighting design projects. There is still a demand for lighting design programs, so SNL has ordered several that are commercially available. These programs are being evaluated for two reasons: (1) to determine if their features are adequate to aid the user in lighting designs, and (2) to provide that information to SNL and other organizations. The information obtained in this paper is to be used to help an end user decide if a program is needed, and if so, to choose one. This paper presents the results of evaluations performed. 5 refs., 6 figs., 3 tabs.

Rigid, closed-cell, polyurethane foam is used in impact limiters in nuclear waste transport containers. During a hypothetical nuclear waste transport accident, the foam is expected to absorb a significant amount of impact energy by undergoing large inelastic volume reductions. Consequently, the crushing of polyurethane foams must be well characterized and accurately modeled to properly analyze a transport container accident. At the request of Sandia National Laboratories, a series of uniaxial, hydrostatic and triaxial compression tests on polyurethane foams were performed by the New Mexico Engineering Research Institute (NMERI). The combination of hydrostatic and triaxial tests was chosen to provide sufficient data to characterize both the volumetric and deviatoric behaviors of the foams and the coupling between the two responses. Typical results from the NMERI tests are included in this paper. A complete description of these tests can be found in Neilsen et al., 1987. Constitutive models that have been used in the past to model foam did not capture some important foam behaviors observed in the NMERI tests. Therefore, a new constitutive model for rigid, closed-cell, polyurethane foams was developed and implemented in two finite element codes. Development of the new model is discussed in this paper. Also, results from analyses with the new model and other constitutive models are presented to demonstrate differences between the various models. 4 refs., 6 figs., 1 tab.

There are many Safeguards applications which have a need for a reliable system that uses state-of-the-art processing techniques to detect and track targets moving through a scene. A general purpose Target Cueing and Tracking System (TCATS), which is independent of the application and the user interface, is under development. The TCATS algorithms were developed and evaluated with commercially available image processing boards and a VME bus based microcomputer. The TCATS algorithms have successfully demonstrated a high detection capability and the ability to ignore exterior environmental conditions, such as cloud shadows moving through the scene, snow, blowing dust, rain, and moderate camera motion. These algorithms remove camera motion. These algorithms remove camera motion and perform target detection and tracking at near real time. The algorithms can handle many targets and retain the identity of each object from one frame to the next. Special ruggedized hardware is also under development to reduce the size, cost, and power consumption, and to increase the processing rate, reliability, and environmental operating capability of the TCATS. Field evaluations are underway specifically for Exterior Fixed Site Security applications. Testing includes nuisance alarm data gathering and detection capability evaluation of human targets crossing perimeter zones. This paper describes the detection and tracking techniques, custom hardware, and future development plans for the TCATS. 5 refs., 9 figs.

The Outsider Analysis (Outsider) module is part of the Analytic System and Software for Evaluation of Safeguards and Security (ASSESS). Outsider and the ASSESS Facility Descriptor (Facility) module together supercede the Systematic Analysis of Vulnerability to Intrusion (SAVI) PC software package. Outsider calculates P(I), the probability that outsiders are interrupted during an attack on a facility by security forces at the facility, and P(W), the probability of security system win. SAVI exhaustively examines every possible path to find the ten most vulnerable paths. Exhaustive search is adequate if the number of paths to examine is small, but moderately complex facilities can have millions of paths, making exhaustive search too slow for practical purposes. Outsider has two new algorithms that generate paths in order of vulnerability, finishing in a fraction of the time required by SAVI. The new Outsider algorithms make containment analysis easier for analysts than ever before. We describe the new algorithms and show how much better they perform than the SAVI exhaustive search algorithm. 6 refs., 5 figs., 2 tabs.

This paper demonstrates the use of the Analytic System and Software for Evaluating Safeguards and Security. ASSESS is an integrated approach for evaluating the effectiveness of safeguards against theft of special nuclear material by different types of adversaries: insiders, outsiders, and colluding insiders and outsiders. ASSESS consists of six modules: System Manager, Facility Descriptor, Insider Analysis, Outsider Analysis, Neutralization Analysis, and Collusion Analysis. This paper introduces the modules, describes their scope, and highlights the interactions among them. Separate papers will provide detailed discussion and demonstration of each of the modules. The ASSESS code runs on the IBM PC family of computers with 640K RAM, the DOS operating system, and Microsoft Windows. The Windows environment provides a very efficient and convenient graphics user interface as well as drivers for many types of output devices. ASSESS is being developed jointly by Lawrence Livermore National Laboratory and Sandia National Laboratories under the sponsorship of the Department of Energy (DOE) Office of Safeguards and Security. The first version of the ASSESS code was delivered to DOE/OSS in March 1989. 7 refs., 4 figs.

Historically, large scale safeguards alarm and communication systems have required the expensive computational power of a mainframe of midsize computer. Due to the widespread availability and reduced cost of PC-based technology, this class of machine is a much preferred solution. This paper will discuss a development program integrating this technology with inexpensive local area network (LAN) hardware to support (1) many touch panel based operator graphics consoles, (2) redundant LAN communications, (3) fault-tolerant LAN communication, (4) redundancy in subsystem failure, (5) modularity in design, (6) fault-tolerant video communication, (7) inexpensive PC-based video annotation and switcher design, (8) inexpensive video replay capability, (9) use of fiber optic communication media, (10) distributed parallel processing, and (11) minimized overall system cost. The Intel BitBus architecture was selected for network communications between PC CPUs. The network supports both fiber optic and copper media and insures message integrity/receival. Custom boards have been developed to transform PCs modular expandable routing switchers with video presence detection and annotation. 1 fig.

The Outsider Analysis (Outsider) module is part of the Analytic System and Software for Evaluating Safeguards and Security (ASSESS). Outsider and the ASSESS Facility Descriptor (Facility) module together supersede the Systematic Analysis of Vulnerability to Intrusion (SAVI) software package. Outsider calculates P(I), the probability that outsiders are interrupted during an attack by security forces at the facility, and P(W), the probability of security system win, and has other features not found in SAVI. Analysts can select intruders from a set of ten reference threats, ranging from well-equipped terrorists to intruders with no equipment at all. New analysis algorithms run 60 to more than 100 times faster. New reports detail how safeguards are defeated at each element in a path and give other data critical to effective upgrade decisions. Outsider takes as input a facility security system defined in Facility and produces intermediate results for the ASSESS Collision module. 8 refs., 6 figs.

The feasibility of competitive, modular bulk electric power from the sun may be greatly enhanced by the use of a reflux heat pipe receiver to combine a heat engine such as Stirling with a paraboloidal dish concentrator. This combination represents a potential improvement over previous successful demonstrations of dish-electric technology in terms of enhanced performance, lower cost, longer life, and greater flexibility in engine design. There are, however, important issues and unknowns which must be addressed to determine engineering feasibility of these devices. In the pool boiler reflux receiver, concentrated solar radiation causes liquid metal (sodium or potassium) to boil. The vapor flows to the engine heater heads, where it condenses and releases the latent heat. The condensate is returned to the receiver absorber pool by gravity (refluxing). This is essentially an adaptation of heat pipe technology to the peculiar requirements of concentrated solar flux, and provides many advantages over conventional heated tube receiver technology. Boiling theory indicates that long-term stable boiling of liquid metal may be difficult to achieve. Laboratory scale experiments have been performed. Initial tests confirmed that boiling is unstable in a baseline boiler. Boiling stability was established after the addition of ''artificial cavities'' to the heated surface, and successful boiling of sodium was demonstrated for 100 hours. Other stabilizing influences may have been present, and will be discussed. The flux and geometry closely simulated a real receiver. The results of these tests are presented, along with the design of a full scale receiver for on-sun testing and considerations for long term operation. 15 refs., 10 figs.

Techniques are being developed to gain understanding of energy transport efficiencies through changes in pulsed power transmission line geometries. These techniques are being applied to design study of the PBFA-II accelerator which has the goal of increasing the energy available for ICF experiments. Transverse electromagnetic (TEM) wave analysis yields a simple circuit model of the new coax-to- parallel-plate transition. This simple model gives insight into the dominant physics of the device and suggests design improvements that will lead to the desired energy efficiencies. Insights gained by this simple model are confirmed and refined by 3-dimensional, time dependent computer simulations with the SOS code and scale model experiments. Simulations have predicted experimental results to high degree of accuracy which adds confidence in both the simulations and the scale model experiments. 1 ref., 11 figs., 1 tab.

Ion diode research on Sandia National Laboratories' Particle Beam Fusion Accelerator (PBFA) II has progressed significantly during the past two years as we have operated in the shot-a-day model with well-diagnosed proton and lithium ion diode loads. During this period, we have succeeded in demonstrating efficient proton beam generation and in focusing the beam to a full width at half maximum (FWHM) spot size of 5.2 mm. Power and energy densities equivalent to 5.4 (+0.9, /minus/0.8) TW/cm/sup 2/ and 73 kJ/cm/sup 2/, respectively, on a 6 mm diameter sphere from the full diode were obtained. Tests of ion diode operation with a simple Plasma Opening Switch (POS), opening at a current of 1-2 MA, indicate efficient energy coupling and a rapid turn on of iron when the POS opens. A model of diode operation has been developed which successfully describes the operating impedance of applied-B ion diodes on PBFA II, PBFA I, Proto II, and Proto I. In addition, we have developed the capability to perform particle simulations which have helped to determine optimized insulating magnetic field profiles and anode shapes for efficient ion beam generation and focusing. Lithium ion source experiments on PBFA II have succeeded in delivering 26 kJ of lithium ions to the axis using a field-enhanced LiF ion source. Several active lithium ion sources, which should allow improved lithium began generation and focusing, are now being prepared for testing on PBFA II. 11 refs., 10 figs., 2 tabs.

Personnel at Sandia National Laboratories, the Naval Research Laboratory, Cornell University, and Los Alamos National Laboratory are developing cost effective beams of lithium ions to bridge the energy gap between lasers and underground nuclear explosions in the national Inertial Fusion Program. We plan to probe the threshold for igniting thermonuclear fuel in the laboratory on the Particle Beam Fusion Accelerator II (PBFA II). We have met our April 1, 1989, milestone of 5 trillion watts per square centimeter power density on PBFA II. We wish to adapt the existing Hermes III accelerator at Sandia into a pre-prototype module of the DOE Laboratory Microfusion Facility for military applications in support of the DOE decision in the mid 90s on the best particle beam or laser for the facility. A German-American study concludes that our lithium ion approach offers the lowest cost option for fusion energy. 7 figs.

Superconducting polycrystalline thin films in the Tl-Ca-Bu-Cu-O system have been prepared by electron beam evaporation followed by appropriate sintering and annealing. Transition temperatures to 110 K and critical current densities to 600,000 A/cm/sup 2/ have been attained in oxygen annealed films. However, with only 16 minutes of air sintering and no oxygen anneal, oriented films have been obtained with T/sub c/'s to 107 K and J/sub c/'s to 450,000 A/cm/sup 2/. Single film devices utilizing a parallel array of weak links and a coplanar control line have been fabricated from the films. Oscillators as well as AM and FM modulators operating between 3 and 6 GHz have been demonstrated using this device concept. 24 refs., 4 figs.

A Personnel and Material Tracking System (PMTS) demonstrated at Argonne National Laboratories-West (ANL-W) in 1987 has resulted in the further development of this system. The results of the demonstration indicated immediate potential for the Material Monitoring/Tracking (MM) portion of the system. The MM system provides the separate functions of (1) observing all container movements, (2) authorized access approval,and (3) initiation and receipt of material transfers. All three functions are coordinated through a single computer which is known as the Computer Augmented Material Access (CAMA) computer. The Wireless Alarm Transmission of Container handling (WATCH) system provides Function 1, and the Mobile Accountability Verification Inventory Station (MAVIS) system provides Functions 2 and 3. Faster communications and the expanded and refined software package developed to provide Functions 2 and 3 stands out as the major accomplishment of this project. Increased functionality with enhanced protection against the insider threat in a more friendly operator interface is provided by this software. 3 refs., 2 figs.

In our instrumentation development efforts we find it necessary to be able to evaluate the performance of waveform digitizing systems with sampling rates from a few kilohertz to more than a gigahertz. Our goal has been to develop an integrated system which can provide quantitative results on the performance of systems and subsystems. Here we describe a system which is controlled by a Microvax II with instrumentation control through the IEEE-488 buss. The evaluation procedure is delineated in reference to a Trial Waveform Digitizer Standard generated by the Waveform Measurements and Analysis committee appointed by the Instrumentation and Measurement Society of IEEE. The standard has been recently accepted by the IEEE and will become a published standard. In this work, special focus is given to the accurate measurement of effective-bit performance and differential nonlinearity of waveform digitizers. 3 refs., 8 figs.

This paper presents some simple concepts for fixtures that can be used in two and three-axis vibration testing. Two, two-axis fixtures were built and tested in the laboratory. Test results are shown, and serve to confirm the validity of the concept. Simple methods for extending the concepts for three-axis testing are discussed. 6 refs., 9 figs.

This paper presents a combined analytical and experimental method for establishing a set of equations to evaluate the equivalent forces acting on a structure. The method requires that a finite element model of the structure be established. It further requires that the accelerator responses to the external forces be measured at a number of points on the structure. The equivalent forces established in the analysis are a representation of the actual forces. The equivalent forces concentrate the effects of the external forces at the degrees of freedom where the acceleration responses are measured. 6 refs., 4 figs., 1 tab.

Second harmonic generation was measured for a thin corona-poled film of a dicyanovinyl azo dye incorporated in the side-chain methacrylate polymer. Measurements were performed at a wavelength of 1.58 ..mu..m as a function of incident angle for both p- and s-polarized incident light. From these measurements the form and magnitude of the second harmonic coefficient tensor were determined. The molecular distribution implied by the data is consistent with a thermodynamic potential containing only the dipolar orienting energy acting during poling. We have also demonstrated anomalous-dispersion phase-matched second harmonic generation for the first time using electric field induced second harmonic generation (EFISH) in a liquid solution of Foron Brilliant Blue S-R (FBB). Results are described. 10 refs., 4 figs., 2 tabs.

We report on the first ferroelectric measurements of chemically prepared KNbO/sub 3/ thin films. Polycrystalline KNbO/sub 3/ thin films were fabricated by dip coating substrates with methanolic solutions of potassium hydroxide and niobium ethoxide. Perovskite KNbO/sub 3/ was obtained for both bulk gels and films by using 800/degree/C firing treatments. For films, the intermediate temperature processing schedule was critical for the complete conversion of low temperature phases to perovskite KNbO/sub 3/. Raman spectroscopy and x-ray diffraction analysis confirmed that properly processed films possessed the orthorhombic distortion of the perovskite structure at room temperature. In response to a 1 kHz, sinusoidal field of 300 kV/cm amplitude, we measured the following ferroelectric properties: (1) a remanent polarization of 4.5 ..mu..C/cm/sup 2/, (2) a spontaneous polarization of 8.3 ..mu..C/cm/sup 2/, and (3) a coercive field of 55 kV/cm.