Tg of partially cured samples at a given temp for various minutes measured with a TA Instruments Q2000 DSC and measured from peak in G” from previous rheometer data.
70C
| Time (min) | Tg (C) |
|---|---|
| 280 | 26 |
| 316 | 33 |
| 406 | 46 |
| 442 | 50 |
| 514 | 58 |
| 604 | 63 |
| 802 | 67 |
| 1090 | 70 |
90C
| Time (min) | Tg (C) |
|---|---|
| 188 | 22 |
| 278 | 34 |
| 422 | 44 |
| 566 | 48 |
| 782 | 54 |
| 1088 | 62 |
90C
| Time (min) | Tg (C) | Tg (C) -12 |
|---|---|---|
| 240 | 38 | 26 |
| 270 | 40 | 28 |
| 300 | 42 | 30 |
| 360 | 48 | 36 |
| 420 | 50 | 38 |
| 480 | 57 | 45 |
| 600 | 63 | 51 |
| 720 | 66 | 54 |
| 960 | 75 | 63 |
| 1200 | 80 | 68 |
| 1440 | 84 | 72 |
| 2880 | 95 | 83 |