MN471000, Pressure Safety Manual
Sponsor: Michael W. Hazen, 4000
Revision Date: October 7, 2007
Replaces Document Dated: August 29, 2007

This document is no longer a CPR. This document implements the requirements of Corporate procedure ESH100.2.PS.1, Control Pressure Safety Hazards.

IMPORTANT NOTICE: A printed copy of this document may not be the document currently in effect. The official version is the online version located on the Sandia Restricted Network (SRN).


Pressure Safety Manual

10. VACUUM SAFETY


Subject Matter Experts: Shane Page, and David Paoletta
Contributor: Pressure Safety Committee
MN471000, Issue R (Q not used)
Revision Date: October 8, 2007; Replaces Document Dated: August 29, 2007
Administrative Changes: November 21, 2007, January 28, 2008, December 17, 2009, June 8, 2010, and May 26, 2011, and January 19, 2012



INTRODUCTION

What Are Vacuum Systems?

Guidance

The term "vacuum" refers to a space that has gas pressure below ambient atmospheric pressure. These systems may present some hazards and employ components that are unique and separate from pressure systems where the gas-pressure is greater than ambient atmospheric pressure. A vacuum system includes all of the components, e.g., the main vacuum vessel, plumbing, and pumps.

Negative Internal Pressure

Guidance

Vacuum systems contain less than ambient atmospheric pressure, also referred to as "negative internal pressure." Measurements of the remaining gases in vacuum systems are referred to as pressure measurements (operating pressure or system ultimate pressure), and are typically in absolute units, such as microns, torr, millibar, or pascals.

Note:  The ASME Boiler and Pressure Vessel Code, Sec. VIII, Div. 1, Part UG-28 refers to these systems as being under "external pressure."

Positive Internal Pressure

Guidance

Systems containing pressures greater than ambient atmospheric are differentiated from negative internal pressure systems by referring to them as "positive internal pressure" systems. Pressure measurements for positive internal pressure systems are often not in absolute units but are commonly in gauge pressure units (typically, pounds per square inch gauge [psig]).

Vacuum-Only Systems

Guidance

"Vacuum-only" systems are systems in which all intended processes or experiments are conducted at pressures less than ambient atmospheric pressure. These systems are brought up to atmospheric pressure for backfill and venting operations. Minimal positive (greater than ambient atmospheric) internal pressures may be allowed for purge purposes when opening a system to the atmosphere.

In general, vacuum-only systems are designed for negative internal pressure and contain components and design concepts that make a positive internal overpressure test inappropriate. Therefore, other means may be used to determine the safety of these systems.

Vacuum-only systems must be protected from accidental overpressurization by applicable protective devices or techniques discussed in this appendix.

Pressure Sources Associated with Vacuum Systems

Requirements

System owners shall address the possible effects of any positive-pressure sources, such as process or backfill gases, connected to the system when considering the vacuum system's safety and approach to overpressure protection.

Vacuum Systems Used at Positive Internal Pressures

Requirements

System owners shall be aware that vacuum systems that are also used at positive internal pressures are subject to the requirements of the Pressure Safety Manual.

Pressure Safety Related to Vacuum Systems

Guidance

Vacuum systems, like all pressure systems, are required to be safe when used in occupied areas. A thorough approach to the pressure safety aspects of vacuum systems involves evaluating systems to ensure that they meet the following requirements:

Flowchart for Evaluating Vacuum Systems

Guidance

The following is a vacuum system design guidance flowchart that presents the suggested steps for evaluation of a vacuum system.


APPROVED AND REPUTABLE SUPPLIERS

Who Are Approved and Reputable Suppliers?

Guidance

The terms "approved" and "reputable" indicate suppliers who have a proven history of acceptable quality products and who adhere to industry standard design parameters with respect to the following:

Experience shows that vacuum systems (or components) fabricated by reputable manufacturers adhere to acceptable safety standards. The acceptance and documentation of these systems is therefore simpler than that of systems or components not fabricated by reputable manufacturers.

Criteria for an Approved Supplier

Guidance

A vacuum system meets the safety requirements of this manual if that system is purchased from an "approved" supplier, which includes systems assembled from commercially available components from approved suppliers. The following are factors for approving a supplier:

Who Approves Suppliers?

Requirements

The system owner shall approve the supplier, with the agreement of the SNL organization manager, pressure advisor or vacuum consultant, and any applicable SNL purchasing agent.

Note:  An SNL pressure advisor shall sign all purchase requisitions for vacuum systems and components in the special approval block of the Purchase Requisition Form as required by Supply Chain Management requirements.

Listing of Approved and Reputable Suppliers

Guidance

Vacuum system personnel should see the Pressure Safety homepage for a listing of reputable vacuum equipment manufacturers who may be approved for fabrication of a vacuum system. This list is not intended to be all inclusive; other suppliers may be approved by the SNL organization involved with the acceptance of the system.


ACCEPTABLE DESIGN AND SYSTEM SPECIFICATIONS

Steps for Designing, Fabricating, or Purchasing a Vacuum System

Guidance

Vacuum system personnel should use a step-by-step approach when specifying, designing, fabricating, or purchasing a vacuum system such as the following:
  1. Select a design concept.
  2. Specify and define the system requirements and operating conditions.
  3. Select or specify the materials and processes.
  4. Specify any leak rate testing or other certifications that may be required for acceptance of the system.

Selecting a Design Concept

Guidance

Vacuum system personnel should consider the following when selecting a design concept:

Specifying System Requirements and Operating Conditions

Guidance

Vacuum system personnel should consider the following when specifying and defining the system requirements and operating conditions:

Selecting or Specifying Materials and Processes

Guidance

Vacuum system personnel should consider the following when selecting or specifying materials and processes:


DESIGN AND SYSTEM REQUIREMENTS FOR SYSTEMS NOT FABRICATED BY AN APPROVED MANUFACTURER

Using Suppliers Who Are Not Listed as Approved and Reputable

Requirements

Vacuum system personnel shall:

Design and Processing Criteria

Requirements

Vacuum system personnel shall accept that a vacuum system not fabricated by an approved supplier meets the appropriate design and processing criteria if information from the supplier that describes materials of construction, welding, and system design parameters has been obtained and the system meets one of the following:

What the Safety Analysis Must Satisfy

Requirements

Vacuum system personnel shall ensure that a safety analysis for a vacuum system from a supplier who is not listed as approved and reputable satisfies both of the following:

Note:  An external overpressure test is not required.

Additional Analysis for Systems Not Meeting the Code

Requirements

Vacuum system personnel shall:

Systems Used in Harsh Environments

Requirements

Vacuum system personnel shall consult materials and metallurgy experts to ensure that those materials have sufficient ductility for the application, if system operation calls for harsh environments (e.g., containment of corrosives).

Specifying and Verifying Welds and Brazes

Guidance

When specifying and verifying welds and brazes, vacuum system personnel should consider the following guidelines:

Note:  ASME code calls for internal overpressure tests. However, most vacuum systems contain components designed for external pressure only, which makes an internal overpressure test inappropriate. External overpressure tests also may not be appropriate for some vacuum vessels.


VACUUM SYSTEM PRESSURE SOURCES AND OVERPRESSURE PROTECTION TECHNIQUES

Vacuum System Safety

Requirements

Vacuum system personnel shall provide overpressurization protection for vacuum systems which have identified pressure sources with a safety manifold as shown in Chapter 5 of this manual or shall otherwise adequately protect them by an alternate technique from overpressurization.

Vacuum Systems Versus Positive-Pressure Systems

Guidance

Vacuum systems meet the SNL definition of pressure systems; however, there are basic differences between vacuum systems and positive (greater than ambient atmospheric) internal pressure systems that should be recognized and appreciated to adequately address safety concerns and maintain vacuum system integrity.

Briefly stated, all plausible pressure sources of vacuum systems should be identified and adequate overpressure protection should be provided to protect the vacuum system and components from these pressure sources. Overpressure protection can be implemented using a variety of techniques.

Evaluation of all plausible pressure sources in any given system is necessary to adequately address overpressure protection.

Vacuum system personnel should be cognizant of the following vacuum system pressure sources and overpressure protection techniques.

Process and Backfill Gases

Guidance

Some common pressure sources associated with vacuum systems include process and backfill gases.

Process gases are typically gases supplied from high-pressure gas cylinders. Backfill gases are also supplied from gas cylinders or may be supplied from "house" sources, such as nitrogen gas from a liquid nitrogen tank.

Less Common Pressure Sources

Guidance

Additional types of pressure sources that are not as commonly recognized include the following:

Effects of Increasing Temperature

Guidance

Increasing temperature may affect system pressure in vacuum systems capable of operation above room temperature. Typically, systems are heated while under vacuum for degassing or process purposes. However, if a closed system is inadvertently backfilled and then heated, pressure could rise significantly. A vacuum system, closed and vented to 1 atm at room temperature, will see a pressure rise of nearly 20 psig when heated to 400°C. This obviously could present a significant hazard that should be mitigated through the use of a pressure relief device or other controls or interlocks.

Positive-Pressure Gas Sources in Vacuum-Only Systems

Guidance

It is common for vacuum-only systems to be connected to positive pressure gas sources in order to admit process or backfill or purge gases into the system. These gas sources typically include the following:

The vacuum system's safety and approach to overpressure protection should identify these positive pressure gas sources and their possible effects on the vacuum system.

Other System Pressure Sources

Guidance

Other system-specific pressure sources may exist (e.g., the mixing of reactive gases or other chemical reactions and the subsequent generation of high pressures).

Techniques for Overpressure Protection

Guidance

The following are means for providing overpressure protection for vacuum systems:


VACUUM APPLICATION PRESSURE RELIEF DEVICES

Requirements

Vacuum system personnel shall ensure that relief devices located directly on the vacuum chamber do not limit the vacuum integrity of the system. When relief devices are located on the associated gas supply lines, use relief devices on all pressure lines into the chamber and ensure that no unforeseen pressure sources exist in the chamber (such as the warming of cryogenic components).

Guidance

Vacuum system personnel should be cognizant of the following guidelines concerning vacuum application pressure relief devices.

Availability of Hardware

Guidance

Pressure relief devices specially intended for vacuum system applications that have the necessary low set pressure and high flow capacity and that provide reliable service (low leakage rates) are made by vacuum or cryogenic equipment manufacturers. They are available through the JIT or other vacuum component suppliers in the form of pressure relief valves and burst disks. The selection of a particular pressure relief device and its location on the system is dependent upon the specific system construction, system hazards, and vacuum requirements.

Hardware suitable for even the most stringent demands of ultra high-vacuum systems is commercially available, with typical ranges from 2 to 5 psig for pressure relief valves and 3 to 5 psig for burst disks.

Characteristics of Relief Devices

Guidance

There are three main characteristics of relief devices for vacuum applications:

Placement of the Relief Device

Guidance

Determine the correct placement of the pressure relief device according to the guidance in Chapter 5 of this manual. Generally, the relief device should be located on the vacuum system itself or on the pressure source line as it leads to the vacuum system. When located on the pressure source line, the device should relieve at a pressure low enough to protect the vacuum system.

Determining the Set Pressure

Guidance

Because a maximum allowable working pressure (MAWP) is generally not specified for a vacuum only system or component, use the "as low as reasonably achievable" (ALARA) principle to determine the set pressure of the pressure relief device.

Evaluate the following to determine the set pressure:

Flow Capacity Concerns

Guidance

Vacuum systems present special sizing problems (relief device flow capacity), and devices may be necessary to reduce the pressure source flow rate to a level compatible with the relief device capacity. Refer to Chapter 5 of the Pressure Safety Manual under "Protective Pressure Relieving Devices" for a discussion of special sizing problems.

Calculations should show a minimal and acceptable amount of accumulated pressure across the relief device during the worst-case overpressure scenario.

Devices for Limiting Flow Capacity

Guidance

Flow-restrictive components in the pressure supply line can be used to limit the flow capacity requirements for the pressure relief valve.

Excess flow valves should also be used to address the issue of flow capacity. In these cases, the relief device must have sufficient capacity to actuate the excess flow valve and thereby isolate the pressure source.

Excess flow valves used for this purpose should not be left in the locked or manually open position.

Leak Integrity

Guidance

The leak integrity of the relief device should be commensurate with the vacuum system requirements.

When selecting a pressure relief device, the leak integrity of both the mounting connection and valve closure seal should be evaluated.

For More Information on Pressure Relief Devices

Guidance

Seek advice from your pressure advisor, local vacuum consultant, or the Safety Engineering Department (4122) (Health & Safety Department [8517] at SNL/CA) on the selection and location of pressure relief devices for vacuum systems.

Vacuum component sales representatives can also supply information on pressure relief device characteristics.


GRAVITY/VACUUM CLOSURE DEVICES AND PROCEDURAL CONTROLS FOR OVERPRESSURE PROTECTION

Guidance

Vacuum system personnel should be cognizant of the following guidance.

Using Gravity/Vacuum Closure Devices

Guidance

Using a gravity closure device or a flange held in place merely by the vacuum pressure itself may be an acceptable overpressure protection technique. A gravity closure bell jar will lift and vent upon slight overpressures (typically around 2 psig).

In a similar approach, the closure hardware (for example, bolts or clamps) can be intentionally left off of a component, allowing the vacuum pressure alone to supply the sealing force to hold the flange in place and vent upon slight overpressure.

Precautions for Leaving Off Closure Hardware

Guidance

The following precautions should be taken when intentionally leaving closure hardware off of a component:

Volume Limitation

Guidance

Overpressure protection devices are not necessary for vacuum systems for which analysis shows that it is impossible to overpressurize the system by any credible accident scenario (e.g., a 2 ft3 [expanded gas volume] lecture bottle connected to a 6 ft3 volume vacuum chamber cannot overpressurize the chamber).

Procedural Controls

A small-volume chamber (e.g., a section of tubing) can be charged to a particular pressure by the pressure source. This chamber can then be isolated from the pressure source and used to supply gas into the vacuum system. In this approach, the volume limitation is supplied through procedural controls (proper valve sequencing).

The use of a checklist to assure proper sequencing is recommended.

Note:  Hardware controls are preferred over procedural controls.


PRECAUTIONS FOR GAUGES AND OTHER DEVICES

Requirements

Vacuum system personnel shall:

Guidance

Vacuum system personnel should be cognizant that:


USING BRITTLE MATERIALS

Note:  Brittle components (e.g., vacuum viewports, glass ion gauges, ceramic feedthroughs, and quartz reactor tubes) are commonly applied to vacuum systems. In some cases, the entire vacuum system may be constructed of brittle material (e.g., a laboratory glassware system commonly used in a chemistry lab). Adequate overpressure protection for systems employing these components is especially important, as is, the protection of personnel.

Precautions for Brittle Components

Requirements

Vacuum system personnel shall locate, shield, or position brittle systems or components away from personnel and equipment that could be damaged if the system or component fails.

Shielding Brittle Components or Using Personal Protective Equipment

Requirements

Vacuum system personnel shall shield brittle components to protect personnel from the fragments of a system failure, and to protect brittle or otherwise fragile components from accidental damage by personnel. Although shielding is the preferred method of protection, an acceptable alternative is to require personnel to wear safety glasses (or a face shield with safety glasses) when working around unshielded brittle components or looking through an unshielded vacuum viewport.

Obtaining Shields

Guidance

Lexan shields are available through the Just in Time (JIT) contract for standard vacuum viewport sizes. Metal shields are available for glass ion gauges.

Special Components Constructed of Brittle Materials

Requirements

Vacuum system personnel shall use the same shielding, isolation, and personal protection equipment when dealing with special components constructed of brittle materials as are required for routinely used components.


PRECAUTIONS FOR VACUUM VIEWPORTS AND NONRATED COMPONENTS

Operational Hazards for Vacuum Viewports

Note: Vacuum viewports have certain operational high-hazard conditions:

Minimizing Thermal Gradients

Guidance

Vacuum system personnel should use layers of aluminum foil across a vacuum viewport to minimize thermal gradients during the bakeout process.

Scratched or Damaged Viewports

Requirements

Vacuum system personnel shall:

Mounting Viewport Flanges

Guidance

Vacuum system personnel should:

Examples of Nonrated Components

Guidance

An example of a special (nonrated) component is the ultra-thin "window" used on X-ray tubes/detectors or on other detectors for activities such as optical experiments and particle beam analysis.

Determining Level of Rigor for Precautionary Measures

Requirements

Vacuum system personnel shall:


PRECAUTIONS FOR VACUUM PUMPING SYSTEMS

Evaluate Vacuum Pump Applications

Requirements

Vacuum system personnel shall closely scrutinize vacuum pump applications to ensure safe and reliable operations.

Special Precautions

Guidance

Vacuum system personnel should:

Informing Repair or Maintenance Personnel of Hazards

Requirements

Vacuum system personnel shall inform repair or maintenance personnel who may be exposed to hazardous residues of these hazards.

Form for Providing Information

Requirements

Vacuum system personnel shall use the SNL Vacuum Pump Repair Information Form (SF 2001-VPR [Word file/Acrobat file]) to identify hazards and solicit feedback from the repair facility for failure analysis.

Note: The form should accompany vacuum pumps sent out for repair.

Materials Compatibility

Requirements

Vaccum system personnel shall ensure the compatibility of the gases pumped with pump fluids and the pump's materials of construction.

Note: For example, special pump oils are needed to safely pump oxygen.

Pump Failure Modes

Requirements

Vacuum system personnel shall determine the vacuum pump failure modes and their ramifications on the vacuum system pressure if pump failure or improper pump connection could pressurize the vacuum system.

Take Additional Overpressure Protection Measures

Requirements

Vacuum system personnel shall:

Guidance

Vacuum system personnel should use appropriate overpressure protection measures that may include the following:


DATA PACKAGES

A data package:

Developing Data Packages

Requirements

Vacuum system personnel shall develop data packages applicable to vacuum systems according to Chapter 9 of the Pressure Safety Manual.

Maintaining and Referencing Operational Documents in Data Package

Guidance

Vacuum system personnel should consider that the data package is a good place to maintain or reference operational technical work documents (TWDs) such as the following:

Note: See ESH100.2.GEN.3, Develop and Use Technical Work Documents, for information on developing TWDs.

Review and Approval of Data Packages

Requirements

The responsible SNL manager, the Pressure Advisor, and the Pressure Installer shall determine the adequacy of and the level of approval for the Data Package.


DOCUMENTING VACUUM SYSTEMS

Identify and Characterize the System

Requirements

Vacuum system personnel shall identify and characterize the vacuum system in a Data Package including:

Guidance

Vacuum system personnel should use the manufacturer's catalog information or operators' manuals as sources of this information including:

Identify Component Automation and "Fail-Safe" Components

Requirements

Vacuum system personnel shall identify the consequences of failure in the data package for the following:

List Pressure Sources

Requirements

Vacuum system personnel shall list all plausible pressure sources in the data package. Include a listing of the pressure line components and their ratings (for example, DOT cylinders, regulators, valves, and piping or tubing).

Document Overpressure Protection

Requirements

Vacuum system personnel shall document the following in the data package:

Identify Nonrated Components

Requirements

Vacuum system personnel shall identify and give special attention to nonrated components in the data package. Indicate a safe failure mode or shielding provided.

Identify Brittle Materials

Requirements

Vacuum system personnel shall list components that contain brittle materials and document shielding or procedures that provide for personnel protection.

If the system is predominantly of brittle materials, document the design material specifications and mechanical containment or administrative controls, including physical barriers, to preclude access to the potential hazard.

Document Pump Information

Requirements

Vacuum system personnel shall describe the vacuum pump system and document the following information in the Data Package:

Include Warnings and Special Instructions

Requirements

Vacuum system personnel shall include warnings or special instructions for maintenance or reapplication personnel and identify any hazardous substances that may remain in the vacuum system pumps or components and associated piping.

Document Procedural Controls

Requirements

Vacuum system personnel shall, for procedural controls that provide overpressure protection, document the pressure/volume calculations (along with the proper valve sequencing information) in the data package.

Document Positive-Pressure Gas Supply Lines

Requirements

Vacuum system personnel shall document gas supply lines in the data package covering the overall system, and document the MAWP based on the ratings of the gas line components.


Shane Page, srpage@sandia.gov
Al Bendure, aobendu@sandia.gov


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